C~44~H~36~N~16~Ni~2~, 4(ClO~4~), 5(O)

Sample Originator: Craig J. Matthewsa.

Data Collection: Peter N. Hortonb and Michael B. Hursthouseb

Structure Determination: Peter N. Hortonb.

Nottingham Trent Universitya
University of Southamptonb



Identification Number:10.5258/ecrystals/989
Controlled Keywords:nickel compounds, supramolecular assemblies
Date Created:06 April 2004
Deposited On:28 Mar 2012 12:53
Deposited By:Mr Steve Lamond

Data collection parameters

Chemical formulaC44 H46 Cl4 N16 Ni2 O21
Crystal morphology
Crystal systemOrthorhombic
Space group symbolPna2(1)
Cell length a25.809(5)
Cell length b11.899(5)
Cell length c17.357(5)
Cell angle alpha90.00
Cell angle beta90.00
Cell angle gamma90.00
Data collection temperature120(2)

Refinement results

Solution figure of merit0.2028
R Factor (Obs)0.0810
R Factor (All)0.1288
Weighted R Factor (Obs)0.1720
Weighted R Factor (All)0.1905

Citation: Matthews, Craig J. and Horton, Peter N. and Hursthouse, Michael B. (2004) University of Southampton, Crystal Structure Report Archive. (doi:10.5258/ecrystals/989)
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