Sample Originator: Jim A. S. Howella.
Data Collection: Peter N. Hortonb and Michael B. Hursthouseb
Structure Determination: Peter N. Hortonb.
University of Keelea
University of Southamptonb
C11H15AuClNOSi
InChI=1/C11H16NOSi.Au.ClH/c1-12-11-8-6-5-7-10(11)9-13-14(2,3)4;;/h5-8,12H,9H2,2-4H3;;1H/q;+1;/p-1
| Identification Number: | 10.5258/ecrystals/891 |
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| Controlled Keywords: | metal carbenes, gold compounds |
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| Date Created: | 14 May 2002 |
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| Deposited On: | 14 Aug 2013 22:44 |
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| Deposited By: | Mr Steve Lamond |
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Depositor Comments
All hydrogen atoms were fixed.
The collection was carried out at room temperature since the crystals tended to splay under the low temperatures of the cryostream.
Data collection parameters
| Chemical formula | C11 H15 Au Cl N O Si |
| Crystal morphology | |
| Crystal system | Monoclinic |
| Space group symbol | P2(1)/n |
| Cell length a | 12.3830(12) |
| Cell length b | 6.2820(4) |
| Cell length c | 18.9017(16) |
| Cell angle alpha | 90.00 |
| Cell angle beta | 92.669(3) |
| Cell angle gamma | 90.00 |
| Data collection temperature | 120(2) |
Refinement results
| Solution figure of merit | |
| R Factor (Obs) | 0.0534 |
| R Factor (All) | 0.1374 |
| Weighted R Factor (Obs) | 0.0897 |
| Weighted R Factor (All) | 0.1090 |
Citation: Howell, Jim A. S. and Horton, Peter N. and Hursthouse, Michael B. (2002) University of Southampton, Crystal Structure Report Archive. (doi:10.5258/ecrystals/891)
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