2010src0042 CD68 C40H34Cl2P2Pd

Sample Originator: Stuart L. Jamesa.

Data Collection: Peter N. Hortonb and Michael B. Hursthouseb

Structure Determination: Peter N. Hortonb.

Queen's University, Belfasta
University of Southamptonb


Controlled Keywords:palladium compounds, organophosphorus ligands
Date Created:19 March 2010
Deposited On:19 Mar 2010 11:22
Deposited By:Dr Peter N Horton

Depositor Comments

User Redcode:- CD68 The styrene group was disordered over two sites.

Data collection parameters

Chemical formulaC40 H34 Cl2 P2 Pd
Crystal morphologyPlate
Crystal systemtriclinic
Space group symbolP-1
Cell length a9.9242(4)
Cell length b9.9428(4)
Cell length c10.4323(3)
Cell angle alpha86.305(2)
Cell angle beta67.758(2)
Cell angle gamma62.176(2)
Data collection temperature120(2)

Refinement results

Solution figure of merit34.99
R Factor (Obs)0.0382
R Factor (All)0.0531
Weighted R Factor (Obs)0.0799
Weighted R Factor (All)0.0867

Citation: James, Stuart L. and Horton, Peter N. and Hursthouse, Michael B. (2010) University of Southampton, Crystal Structure Report Archive. (http://ecrystals.chem.soton.ac.uk/1262/)
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