C~66~H~58~N~2~O~6~P~4~Pd, Cl~2~

Sample Originator: Martin B. Smitha.

Data Collection: Peter N. Hortonb and Michael B. Hursthouseb

Structure Determination: Peter N. Hortonb.

Loughborough Universitya
University of Southamptonb



Controlled Keywords:polyphosphines
Date Created:04 September 2002
Deposited On:16 Feb 2010 14:43
Deposited By:Mr Steve Lamond

Depositor Comments

One of the chloride ions (Cl2) is disordered over two independent sites. All the hydrogen atoms were fixed.

Data collection parameters

Chemical formulaC66 H58 Cl2 N2 O6 P4 Pd
Crystal morphology
Crystal systemTetragonal
Space group symbolI4(1)/acd
Cell length a33.788(6)
Cell length b33.788(6)
Cell length c22.014(7)
Cell angle alpha90.000
Cell angle beta90.000
Cell angle gamma90.000
Data collection temperature120(2)

Refinement results

Solution figure of merit0.4840
R Factor (Obs)0.0801
R Factor (All)0.2565
Weighted R Factor (Obs)0.1689
Weighted R Factor (All)0.2391

Citation: Smith, Martin B. and Horton, Peter N. and Hursthouse, Michael B. (2002) University of Southampton, Crystal Structure Report Archive. (http://ecrystals.chem.soton.ac.uk/1149/)
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