Sample Originator: Martin B. Smitha.
Data Collection: Simon J. Colesb and Michael B. Hursthouseb
Structure Determination: Simon J. Colesb.
Loughborough Universitya
University of Southamptonb
C29H28Cl2N2PRhSSe
InChI=1/C19H16ClN2PSSe.C10H15.ClH.Rh/c20-14-11-12-17-18(13-14)24-19(21-17)22-23(25,15-7-3-1-4-8-15)16-9-5-2-6-10-16;1-6-7(2)9(4)10(5)8(6)3;;/h1-13,23,25H,(H,21,22);1-5H3;1H;
| Controlled Keywords: | polyphosphines |
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| Date Created: | 11 October 2002 |
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| Deposited On: | 16 Feb 2010 14:44 |
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| Deposited By: | Mr Steve Lamond |
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Data collection parameters
| Chemical formula | C29 H28 Cl2 N2 P Rh S Se |
| Crystal morphology | |
| Crystal system | Monoclinic |
| Space group symbol | P2(1)/n |
| Cell length a | 7.9701(3) |
| Cell length b | 16.3122(8) |
| Cell length c | 21.5858(13) |
| Cell angle alpha | 90.00 |
| Cell angle beta | 90.811(2) |
| Cell angle gamma | 90.00 |
| Data collection temperature | 120(2) |
Refinement results
| Solution figure of merit | |
| R Factor (Obs) | 0.0529 |
| R Factor (All) | 0.1068 |
| Weighted R Factor (Obs) | 0.0927 |
| Weighted R Factor (All) | 0.1076 |
Citation: Smith, Martin B. and Coles, Simon J. and Hursthouse, Michael B. (2002) University of Southampton, Crystal Structure Report Archive. (http://ecrystals.chem.soton.ac.uk/1145/)
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