Sample Originator: Martin B. Smitha.

Data Collection: Mark E. Lightb and Michael B. Hursthouseb

Structure Determination: Mark E. Lightb.

Loughborough Universitya
University of Southamptonb



Controlled Keywords:polyphosphines
Date Created:13 June 2002
Deposited On:16 Feb 2010 14:33
Deposited By:Mr Steve Lamond

Depositor Comments

All hydrogen atoms were placed in idealised positions and refined using a riding model.

Data collection parameters

Chemical formulaC43 H43 Cl Ir N2 O P
Crystal morphology
Crystal systemTriclinic
Space group symbolp-1
Cell length a9.778(5)
Cell length b18.378(5)
Cell length c22.542(5)
Cell angle alpha75.970(5)
Cell angle beta78.762(5)
Cell angle gamma74.836(5)
Data collection temperature120(2)

Refinement results

Solution figure of merit
R Factor (Obs)0.0461
R Factor (All)0.0659
Weighted R Factor (Obs)0.1020
Weighted R Factor (All)0.1081

Citation: Smith, Martin B. and Light, Mark E. and Hursthouse, Michael B. (2002) University of Southampton, Crystal Structure Report Archive. (http://ecrystals.chem.soton.ac.uk/1144/)
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