C~32~H~46~ClFeN~2~O~2~, CH~2~Cl~2~

Sample Originator: Robin B. Bedforda.

Data Collection: Peter N. Hortonb and Michael B. Hursthouseb

Structure Determination: Peter N. Hortonb.

Bristol Universitya
University of Southamptonb



Controlled Keywords:catalysis, iron compounds
Date Created:01 February 2005
Deposited On:17 Feb 2010 13:06
Deposited By:Mr Steve Lamond

Depositor Comments

All hydrogen atoms were fixed. There is a disordered molecule of DCM in the asymmetric unit.

Data collection parameters

Chemical formulaC33 H48 Cl3 Fe N2 O2
Crystal morphologyCut Shard
Crystal systemmonoclinic
Space group symbolP2(1)/c
Cell length a11.2450(7)
Cell length b9.0486(8)
Cell length c34.6489(18)
Cell angle alpha90.00
Cell angle beta97.632(5)
Cell angle gamma90.00
Data collection temperature120(2)

Refinement results

Solution figure of merit0.0810
R Factor (Obs)0.0552
R Factor (All)0.1069
Weighted R Factor (Obs)0.1150
Weighted R Factor (All)0.1325

Citation: Bedford, Robin B. and Horton, Peter N. and Hursthouse, Michael B. (2005) University of Southampton, Crystal Structure Report Archive. (http://ecrystals.chem.soton.ac.uk/1094/)
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