C~52~H~47~O~3~P~4~Pd, F~6~Sb, CHCl~3~

Sample Originator: Robin B. Bedforda.

Data Collection: Peter N. Hortonb and Michael B. Hursthouseb

Structure Determination: Peter N. Hortonb.

Bristol Universitya
University of Southamptonb



Controlled Keywords:organic compounds, catalysis
Date Created:02 November 2004
Deposited On:16 Feb 2010 16:06
Deposited By:Mr Steve Lamond

Depositor Comments

All hydrogen atoms were fixed. There is a molecule of chloroform in the asymmetric unit which is disordered over 4 main sites.

Data collection parameters

Chemical formulaC53 H48 Cl3 F6 O3 P4 Pd Sb
Crystal morphologyCut Block
Crystal systemmonoclinic
Space group symbolP2(1)/c
Cell length a12.677(4)
Cell length b26.381(11)
Cell length c16.334(5)
Cell angle alpha90.00
Cell angle beta95.89(3)
Cell angle gamma90.00
Data collection temperature120(2)

Refinement results

Solution figure of merit0.0467
R Factor (Obs)0.0951
R Factor (All)0.1514
Weighted R Factor (Obs)0.2105
Weighted R Factor (All)0.2409

Citation: Bedford, Robin B. and Horton, Peter N. and Hursthouse, Michael B. (2004) University of Southampton, Crystal Structure Report Archive. (http://ecrystals.chem.soton.ac.uk/1092/)
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