C~30~H~26~Cl~2~N~2~PdS~4~, 2(C~2~H~3~N)

Sample Originator: Robin B. Bedforda.

Data Collection: Peter N. Hortonb and Michael B. Hursthouseb

Structure Determination: Peter N. Hortonb.

Bristol Universitya
University of Southamptonb



Controlled Keywords:palladium
Date Created:03 July 2002
Deposited On:08 Nov 2013 15:25
Deposited By:Mr Steve Lamond

Depositor Comments

The thiophene rings are both disordered. All hydrogen atoms are fixed. There is a molecule of acetonitrile in the asymmetric unit that is disordered over two sites.

Data collection parameters

Chemical formulaC34 H32 Cl2 N4 Pd S4
Crystal morphology
Crystal systemTriclinic
Space group symbolP-1
Cell length a6.2568(3)
Cell length b11.4708(5)
Cell length c12.9370(9)
Cell angle alpha100.823(2)
Cell angle beta94.201(2)
Cell angle gamma105.230(2)
Data collection temperature120(2)

Refinement results

Solution figure of merit0.1144
R Factor (Obs)0.0463
R Factor (All)0.0648
Weighted R Factor (Obs)0.1021
Weighted R Factor (All)0.1083

Citation: Bedford, Robin B. and Horton, Peter N. and Hursthouse, Michael B. (2002) University of Southampton, Crystal Structure Report Archive. (http://ecrystals.chem.soton.ac.uk/1087/)
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