Logo

C~24~H~20~P, B~3~H~8~

Sample Originator: Mike A Becketta.

Data Collection: Peter N. Hortonb, Michael B. Hursthouseb and Simon J. Colesb

Structure Determination: Peter N. Hortonb.

University College of North Walesa
University of Southamptonb

C24H28B3P

InChI=1/5C24H21P.4B3H3.BH3/c5*1-5-13-21(14-6-1)25(22-15-7-2-8-16-22,23-17-9-3-10-18-23)24-19-11-4-12-20-24;4*1-2-3-1;/h5*1-20,25H;4*1-3H;1H3

Controlled Keywords:borosilicates, glasses, coatings
Date Created:06 January 2006
Deposited On:03 Sep 2015 16:41
Deposited By:Mr Steve Lamond

Depositor Comments

All hydrogen atoms were fixed. The B3H8 groups were disordered

Data collection parameters

Chemical formulaC24 H28 B3 P
Crystal morphologyRod
Crystal systemtetragonal
Space group symbolI-4
Cell length a27.593(2)
Cell length b27.593(2)
Cell length c7.0313(5)
Cell angle alpha90.00
Cell angle beta90.00
Cell angle gamma90.00
Data collection temperature120(2)

Refinement results

Solution figure of merit0.7235
R Factor (Obs)0.1292
R Factor (All)0.1533
Weighted R Factor (Obs)0.3403
Weighted R Factor (All)0.3675

Citation: Beckett, Mike A and Horton, Peter N. and Hursthouse, Michael B. and Coles, Simon J. (2006) University of Southampton, Crystal Structure Report Archive. (http://ecrystals.chem.soton.ac.uk/1086/)
Export as: oreChem EndNote BibTeX ASCII Citation

Warning

This item is embargoed, The embargo will be lifted on 01 August 2022. This is only viewable by the authors and respository staff, If you would like to show this item to a guest, share this url: http://ecrystals.chem.soton.ac.uk/1086/?key=a36b92379c02372a4542801c61c0da0d

Repository Staff Only: item control page