Symmetry used in scalepack | p2 |
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a (Angstrom) | 7.1328 +/- 0.0002 |
b (Angstrom) | 20.6990 +/- 0.0005 |
c (Angstrom) | 7.1455 +/- 0.0002 |
alpha (°) | 90.000 |
beta (°) | 116.1729 +/- 0.0009 |
gamma (°) | 90.000 |
Volume (A**3) | 946.81 +/- 0.04 |
Mosaicity (°) | 0.655 +/- 0.002 |
Total number of images collected | 203 |
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Total exposure time | 54.0 minutes |
Data collection exposure time | 52.7 minutes |
Data collection wall-clock time | 77.8 minutes |
Wavelength | 0.71073 A |
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Generator setting | 50.00kV 70.00mA |
Crystal to detector distance | 30.00 mm |
Type | Name | # images | Total Rotation | Per frame Rotation | Exposure per frame | Used in scaling |
---|---|---|---|---|---|---|
data collection | s01f | 69 | 110.4° omega | 1.600° | 16 seconds | Yes |
data collection | s02f | 68 | 108.8° omega | 1.600° | 16 seconds | Yes |
data collection | s03f | 58 | 92.8° omega | 1.600° | 16 seconds | Yes |
Zero sigma or profile test | 4 |
---|---|
Overload or incomplete profile | 501 |
Sigma cutoff | 75 |
Low resolution limit | 7 |
High resolution limit | 1489 |
Scale factor | 10.00 |
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Number of 'full' reflections | 4414 |
Number of 'partial' reflections | 15627 |
Total number of integrated reflections | 10274 |
Total number of unique reflections | 2236 |
Data completeness | 99.6% |
Resolution range | 7.00-0.77 A |
Theta range | 2.91°-27.48° |
Average Intensity | 139.1 |
Average Sigma(I) | 3.7 |
Overall R-merge (linear) | 0.056 |
Collection Temperature | 150 K |
Crystal Size | x x |
Crystal Colour | |
Crystal Shape |
R(merge) on F2 |
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R |
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Rw |
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Max Transmission Factor |
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Min Transmission Factor |
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