03SRC188 - C74H52Cl3N17Ni4O22

Sample Originator: Craig J. Matthewsa.

Data Collection: Peter N. Hortonb and Michael B. Hursthouseb

Structure Determination: Peter N. Hortonb.

Nottingham Trent Universitya
University of Southamptonb



Identification Number:10.5258/ecrystals/974
Controlled Keywords:zinc compounds, nickel compounds, supramolecular assemblies
Date Created:23 March 2003
Deposited On:08 Nov 2013 16:26
Deposited By:Mr Steve Lamond

Data collection parameters

Chemical formulaC74 H52 Cl3 N17 Ni4 O22
Crystal morphology
Crystal systemMonoclinic
Space group symbolP2(1)/n
Cell length a17.5385(2)
Cell length b23.9347(3)
Cell length c19.7227(3)
Cell angle alpha90.00
Cell angle beta93.9730(10)
Cell angle gamma90.00
Data collection temperature120(2)

Refinement results

Solution figure of merit0.0962
R Factor (Obs)0.0762
R Factor (All)0.1201
Weighted R Factor (Obs)0.1911
Weighted R Factor (All)0.2125

Citation: Matthews, Craig J. and Horton, Peter N. and Hursthouse, Michael B. (2003) University of Southampton, Crystal Structure Report Archive. (doi:10.5258/ecrystals/974)
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