C~57~H~54~F~9~N~30~O~19~Pb~4~S~3~, 3(CF~3~O~3~S), 6(H~2~O)

Sample Originator: Craig J. Matthewsa and Lisa Davisa.

Data Collection: Peter N. Hortonb and Michael B. Hursthouseb

Structure Determination: Peter N. Hortonb.

Nottingham Trent Universitya
University of Southamptonb



Identification Number:10.5258/ecrystals/971
Controlled Keywords:lead compounds, supramolecular assemblies
Date Created:12 June 2003
Deposited On:17 Feb 2010 16:35
Deposited By:Mr Steve Lamond

Data collection parameters

Chemical formulaC60 H66 F18 N30 O34 Pb4 S6
Crystal morphology
Crystal systemTriclinic
Space group symbolP-1
Cell length a12.7864(5)
Cell length b17.1825(7)
Cell length c22.7443(8)
Cell angle alpha99.355(2)
Cell angle beta99.419(3)
Cell angle gamma99.681(4)
Data collection temperature120(2)

Refinement results

Solution figure of merit0.0399
R Factor (Obs)0.0321
R Factor (All)0.0358
Weighted R Factor (Obs)0.0783
Weighted R Factor (All)0.0802

Citation: Matthews, Craig J. and Davis, Lisa and Horton, Peter N. and Hursthouse, Michael B. (2003) University of Southampton, Crystal Structure Report Archive. (doi:10.5258/ecrystals/971)
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