 
data_s92 
 
_audit_creation_method            SHELXL 
_chemical_name_systematic 
; 
 ? 
; 
_chemical_name_common             ? 
_chemical_formula_moiety          ? 
_chemical_formula_structural      ? 
_chemical_formula_analytical      ? 
_chemical_formula_sum             'C35 H30 Cl4 Fe P2 Pd' 
_chemical_formula_weight          816.58 
_chemical_melting_point           ? 
_chemical_compound_source         ? 
 
loop_ 
 _atom_type_symbol 
 _atom_type_description 
 _atom_type_scat_dispersion_real 
 _atom_type_scat_dispersion_imag 
 _atom_type_scat_source 
 'C'  'C'   0.0033   0.0016 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'H'  'H'   0.0000   0.0000 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'P'  'P'   0.1023   0.0942 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'Cl'  'Cl'   0.1484   0.1585 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'Fe'  'Fe'   0.3463   0.8444 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'Pd'  'Pd'  -0.9988   1.0072 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 
_symmetry_cell_setting            Monoclinic 
_symmetry_space_group_name_H-M    P2(1)/c 
 
loop_ 
 _symmetry_equiv_pos_as_xyz 
 'x, y, z' 
 '-x, y+1/2, -z+1/2' 
 '-x, -y, -z' 
 'x, -y-1/2, z-1/2' 
 
_cell_length_a                    9.770(3) 
_cell_length_b                    18.093(5) 
_cell_length_c                    19.001(3) 
_cell_angle_alpha                 90.00 
_cell_angle_beta                  102.61(2) 
_cell_angle_gamma                 90.00 
_cell_volume                      3277.7(15) 
_cell_formula_units_Z             4 
_cell_measurement_temperature     150(2) 
_cell_measurement_reflns_used     ? 
_cell_measurement_theta_min       ? 
_cell_measurement_theta_max       ? 
 
_exptl_crystal_description        ? 
_exptl_crystal_colour             ? 
_exptl_crystal_size_max           0.25
_exptl_crystal_size_mid           0.21
_exptl_crystal_size_min           0.18
_exptl_crystal_density_meas       ? 
_exptl_crystal_density_diffrn     1.655 
_exptl_crystal_density_method     ? 
_exptl_crystal_F_000              1640 
_exptl_absorpt_coefficient_mu     1.440 
_exptl_absorpt_correction_type    ? 
_exptl_absorpt_correction_T_min   ? 
_exptl_absorpt_correction_T_max   ? 
 
_exptl_special_details 
; 
 ? 
; 
 
_diffrn_ambient_temperature       150(2) 
_diffrn_radiation_wavelength      0.71069 
_diffrn_radiation_type            MoK\a 
_diffrn_radiation_source          'fine-focus sealed tube' 
_diffrn_radiation_monochromator   graphite 
_diffrn_measurement_device        ? 
_diffrn_measurement_method        ? 
_diffrn_standards_number          ? 
_diffrn_standards_interval_count  ? 
_diffrn_standards_interval_time   ? 
_diffrn_standards_decay_%         ? 
_diffrn_reflns_number             8631 
_diffrn_reflns_av_R_equivalents   0.1021 
_diffrn_reflns_av_sigmaI/netI     0.1018 
_diffrn_reflns_limit_h_min        -10 
_diffrn_reflns_limit_h_max        10 
_diffrn_reflns_limit_k_min        -19 
_diffrn_reflns_limit_k_max        19 
_diffrn_reflns_limit_l_min        -16 
_diffrn_reflns_limit_l_max        21 
_diffrn_reflns_theta_min          2.20 
_diffrn_reflns_theta_max          25.01 
_reflns_number_total              4091 
_reflns_number_observed           3310 
_reflns_observed_criterion        >2sigma(I) 
 
_computing_data_collection        ? 
_computing_cell_refinement        ? 
_computing_data_reduction         ? 
_computing_structure_solution     'SHELXS-86 (Sheldrick, 1990)' 
_computing_structure_refinement   'SHELXL-92 (Sheldrick, 1993)' 
_computing_molecular_graphics     ? 
_computing_publication_material   ? 
 
_refine_special_details 
; 
 Refinement on F² for ALL reflections except for 8 with very negative F² 
 or flagged by the user for potential systematic errors.  Weighted R-factors 
 wR and all goodnesses of fit S are based on F², conventional R-factors R 
 are based on F, with F set to zero for negative F². The observed criterion 
 of F² > 2sigma(F²) is used only for calculating _R_factor_obs etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
; 
 
_refine_ls_structure_factor_coef  Fsqd  
_refine_ls_matrix_type            full 
_refine_ls_weighting_scheme 
 'calc w=1/[\s^2^(Fo^2^)+(0.0527P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' 
_atom_sites_solution_primary      direct 
_atom_sites_solution_secondary    difmap 
_atom_sites_solution_hydrogens    geom 
_refine_ls_hydrogen_treatment     ? 
_refine_ls_extinction_method      none 
_refine_ls_extinction_coef        ? 
_refine_ls_number_reflns          4083 
_refine_ls_number_parameters      388 
_refine_ls_number_restraints      0 
_refine_ls_R_factor_all           0.0596 
_refine_ls_R_factor_obs           0.0460 
_refine_ls_wR_factor_all          0.1160 
_refine_ls_wR_factor_obs          0.1056 
_refine_ls_goodness_of_fit_all    1.008 
_refine_ls_goodness_of_fit_obs    1.105 
_refine_ls_restrained_S_all       1.082 
_refine_ls_restrained_S_obs       1.105 
_refine_ls_shift/esd_max          0.001 
_refine_ls_shift/esd_mean         0.000 
 
loop_ 
 _atom_site_label 
 _atom_site_type_symbol 
 _atom_site_fract_x 
 _atom_site_fract_y 
 _atom_site_fract_z 
 _atom_site_U_iso_or_equiv 
 _atom_site_thermal_displace_type 
 _atom_site_occupancy 
 _atom_site_calc_flag 
 _atom_site_refinement_flags 
 _atom_site_disorder_group 
Pd1 Pd 0.76891(5) 0.77874(2) 0.19553(2) 0.0119(2) Uani 1 d . . 
Fe1 Fe 0.49817(10) 0.80225(4) -0.01043(4) 0.0148(2) Uani 1 d . . 
Cl1 Cl 0.9592(2) 0.84473(7) 0.26261(7) 0.0237(4) Uani 1 d . . 
Cl2 Cl 0.7304(2) 0.72382(6) 0.30193(6) 0.0185(4) Uani 1 d . . 
Cl3 Cl 0.6001(3) 0.94083(11) 0.2701(2) 0.0895(10) Uani 1 d . . 
Cl4 Cl 0.7507(3) 0.97417(11) 0.41708(15) 0.0924(11) Uani 1 d . . 
P1 P 0.5974(2) 0.69925(6) 0.13990(7) 0.0141(4) Uani 1 d . . 
P2 P 0.8153(2) 0.83228(7) 0.09500(7) 0.0149(4) Uani 1 d . . 
C1 C 0.6606(7) 0.8658(2) 0.0337(3) 0.015(2) Uani 1 d . . 
C2 C 0.6284(7) 0.8750(3) -0.0437(3) 0.019(2) Uani 1 d . . 
H2 H 0.6886(7) 0.8653(3) -0.0744(3) 0.023 Uiso 1 calc R . 
C3 C 0.4912(8) 0.9011(3) -0.0644(3) 0.022(2) Uani 1 d . . 
H3 H 0.4447(8) 0.9113(3) -0.1115(3) 0.027 Uiso 1 calc R . 
C4 C 0.4333(8) 0.9097(3) -0.0029(3) 0.026(2) Uani 1 d . . 
H4 H 0.3433(8) 0.9260(3) -0.0023(3) 0.031 Uiso 1 calc R . 
C5 C 0.5381(7) 0.8887(3) 0.0575(3) 0.020(2) Uani 1 d . . 
H5 H 0.5288(7) 0.8897(3) 0.1051(3) 0.024 Uiso 1 calc R . 
C6 C 0.3644(7) 0.7260(3) 0.0182(3) 0.020(2) Uani 1 d . . 
H6 H 0.2965(7) 0.7339(3) 0.0449(3) 0.024 Uiso 1 calc R . 
C7 C 0.5103(7) 0.7075(3) 0.0458(3) 0.0147(14) Uani 1 d . . 
C8 C 0.5740(7) 0.6989(3) -0.0152(3) 0.018(2) Uani 1 d . . 
H8 H 0.6669(7) 0.6861(3) -0.0133(3) 0.022 Uiso 1 calc R . 
C9 C 0.4715(8) 0.7132(3) -0.0783(3) 0.022(2) Uani 1 d . . 
H9 H 0.4855(8) 0.7118(3) -0.1251(3) 0.026 Uiso 1 calc R . 
C10 C 0.3455(8) 0.7297(3) -0.0587(3) 0.023(2) Uani 1 d . . 
H10 H 0.2618(8) 0.7413(3) -0.0906(3) 0.027 Uiso 1 calc R . 
C11 C 0.9056(7) 0.7661(3) 0.0501(3) 0.0171(15) Uani 1 d . . 
C12 C 0.9292(8) 0.7770(3) -0.0183(3) 0.031(2) Uani 1 d . . 
H12 H 0.9051(8) 0.8218(3) -0.0418(3) 0.037 Uiso 1 calc R . 
C13 C 0.9889(8) 0.7211(4) -0.0523(3) 0.035(2) Uani 1 d . . 
H13 H 1.0015(8) 0.7279(4) -0.0990(3) 0.042 Uiso 1 calc R . 
C14 C 1.0289(9) 0.6565(4) -0.0167(4) 0.040(2) Uani 1 d . . 
H14 H 1.0688(9) 0.6193(4) -0.0396(4) 0.048 Uiso 1 calc R . 
C15 C 1.0113(9) 0.6454(3) 0.0522(4) 0.040(2) Uani 1 d . . 
H15 H 1.0406(9) 0.6014(3) 0.0760(4) 0.048 Uiso 1 calc R . 
C16 C 0.9502(8) 0.6995(3) 0.0859(3) 0.024(2) Uani 1 d . . 
H16 H 0.9384(8) 0.6919(3) 0.1326(3) 0.029 Uiso 1 calc R . 
C17 C 0.9281(8) 0.9142(3) 0.1073(3) 0.021(2) Uani 1 d . . 
C18 C 0.8678(8) 0.9826(3) 0.1172(3) 0.028(2) Uani 1 d . . 
H18 H 0.7728(8) 0.9857(3) 0.1171(3) 0.034 Uiso 1 calc R . 
C19 C 0.9500(10) 1.0451(3) 0.1269(3) 0.035(2) Uani 1 d . . 
H19 H 0.9097(10) 1.0905(3) 0.1329(3) 0.042 Uiso 1 calc R . 
C20 C 1.0889(11) 1.0411(3) 0.1278(3) 0.042(2) Uani 1 d . . 
H20 H 1.1433(11) 1.0838(3) 0.1351(3) 0.050 Uiso 1 calc R . 
C21 C 1.1505(10) 0.9737(4) 0.1180(4) 0.046(2) Uani 1 d . . 
H21 H 1.2457(10) 0.9708(4) 0.1185(4) 0.056 Uiso 1 calc R . 
C22 C 1.0661(9) 0.9101(3) 0.1074(3) 0.033(2) Uani 1 d . . 
H22 H 1.1057(9) 0.8647(3) 0.1004(3) 0.040 Uiso 1 calc R . 
C23 C 0.6639(7) 0.6048(3) 0.1429(3) 0.017(2) Uani 1 d . . 
C24 C 0.7878(7) 0.5838(3) 0.1896(3) 0.020(2) Uani 1 d . . 
H24 H 0.8382(7) 0.6182(3) 0.2215(3) 0.024 Uiso 1 calc R . 
C25 C 0.8366(8) 0.5124(3) 0.1891(3) 0.024(2) Uani 1 d . . 
H25 H 0.9206(8) 0.4990(3) 0.2199(3) 0.028 Uiso 1 calc R . 
C26 C 0.7613(9) 0.4606(3) 0.1432(3) 0.031(2) Uani 1 d . . 
H26 H 0.7935(9) 0.4122(3) 0.1437(3) 0.037 Uiso 1 calc R . 
C27 C 0.6382(9) 0.4805(3) 0.0965(3) 0.031(2) Uani 1 d . . 
H27 H 0.5877(9) 0.4457(3) 0.0653(3) 0.037 Uiso 1 calc R . 
C28 C 0.5901(7) 0.5521(3) 0.0961(3) 0.021(2) Uani 1 d . . 
H28 H 0.5074(7) 0.5654(3) 0.0643(3) 0.025 Uiso 1 calc R . 
C29 C 0.4503(7) 0.6998(3) 0.1831(3) 0.0157(14) Uani 1 d . . 
C30 C 0.3866(8) 0.6360(3) 0.2005(3) 0.028(2) Uani 1 d . . 
H30 H 0.4219(8) 0.5903(3) 0.1906(3) 0.033 Uiso 1 calc R . 
C31 C 0.2733(9) 0.6385(3) 0.2318(3) 0.037(2) Uani 1 d . . 
H31 H 0.2333(9) 0.5947(3) 0.2431(3) 0.044 Uiso 1 calc R . 
C32 C 0.2176(8) 0.7052(3) 0.2466(3) 0.030(2) Uani 1 d . . 
H32 H 0.1389(8) 0.7066(3) 0.2667(3) 0.037 Uiso 1 calc R . 
C33 C 0.2805(8) 0.7700(3) 0.2311(3) 0.029(2) Uani 1 d . . 
H33 H 0.2453(8) 0.8154(3) 0.2419(3) 0.035 Uiso 1 calc R . 
C34 C 0.3940(8) 0.7676(3) 0.2002(3) 0.024(2) Uani 1 d . . 
H34 H 0.4351(8) 0.8116(3) 0.1902(3) 0.028 Uiso 1 calc R . 
C35 C 0.7202(13) 0.9137(4) 0.3472(4) 0.070(3) Uani 1 d . . 
 
 
_geom_special_details 
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
; 
 
loop_ 
 _geom_bond_atom_site_label_1 
 _geom_bond_atom_site_label_2 
 _geom_bond_distance 
 _geom_bond_site_symmetry_2 
 _geom_bond_publ_flag 
Pd1 P2 2.2737(14) . ? 
Pd1 P1 2.285(2) . ? 
Pd1 Cl1 2.339(2) . ? 
Pd1 Cl2 2.3556(13) . ? 
Fe1 C1 1.990(6) . ? 
Fe1 C7 2.009(5) . ? 
Fe1 C5 2.011(5) . ? 
Fe1 C8 2.021(5) . ? 
Fe1 C2 2.026(6) . ? 
Fe1 C9 2.045(5) . ? 
Fe1 C10 2.048(6) . ? 
Fe1 C6 2.054(6) . ? 
Fe1 C3 2.055(5) . ? 
Fe1 C4 2.059(5) . ? 
Cl3 C35 1.736(9) . ? 
Cl4 C35 1.696(8) . ? 
P1 C29 1.804(7) . ? 
P1 C7 1.811(5) . ? 
P1 C23 1.824(5) . ? 
P2 C1 1.800(6) . ? 
P2 C11 1.808(6) . ? 
P2 C17 1.832(6) . ? 
C1 C5 1.429(9) . ? 
C1 C2 1.446(7) . ? 
C2 C3 1.394(9) . ? 
C3 C4 1.413(9) . ? 
C4 C5 1.412(8) . ? 
C6 C10 1.433(8) . ? 
C6 C7 1.447(9) . ? 
C7 C8 1.438(8) . ? 
C8 C9 1.408(8) . ? 
C9 C10 1.395(10) . ? 
C11 C12 1.384(9) . ? 
C11 C16 1.405(7) . ? 
C12 C13 1.395(9) . ? 
C13 C14 1.365(9) . ? 
C14 C15 1.372(10) . ? 
C15 C16 1.375(9) . ? 
C17 C22 1.350(10) . ? 
C17 C18 1.399(8) . ? 
C18 C19 1.376(9) . ? 
C19 C20 1.355(12) . ? 
C20 C21 1.390(11) . ? 
C21 C22 1.404(9) . ? 
C23 C24 1.389(8) . ? 
C23 C28 1.393(7) . ? 
C24 C25 1.379(7) . ? 
C25 C26 1.379(8) . ? 
C26 C27 1.377(10) . ? 
C27 C28 1.377(7) . ? 
C29 C30 1.385(8) . ? 
C29 C34 1.411(8) . ? 
C30 C31 1.367(10) . ? 
C31 C32 1.377(9) . ? 
C32 C33 1.386(9) . ? 
C33 C34 1.363(10) . ? 
 
loop_ 
 _geom_angle_atom_site_label_1 
 _geom_angle_atom_site_label_2 
 _geom_angle_atom_site_label_3 
 _geom_angle 
 _geom_angle_site_symmetry_1 
 _geom_angle_site_symmetry_3 
 _geom_angle_publ_flag 
P2 Pd1 P1 98.05(5) . . ? 
P2 Pd1 Cl1 87.70(5) . . ? 
P1 Pd1 Cl1 171.39(5) . . ? 
P2 Pd1 Cl2 177.72(6) . . ? 
P1 Pd1 Cl2 83.86(5) . . ? 
Cl1 Pd1 Cl2 90.27(5) . . ? 
C1 Fe1 C7 108.6(2) . . ? 
C1 Fe1 C5 41.9(3) . . ? 
C7 Fe1 C5 110.0(2) . . ? 
C1 Fe1 C8 106.7(3) . . ? 
C7 Fe1 C8 41.8(2) . . ? 
C5 Fe1 C8 136.6(2) . . ? 
C1 Fe1 C2 42.2(2) . . ? 
C7 Fe1 C2 138.8(3) . . ? 
C5 Fe1 C2 69.4(2) . . ? 
C8 Fe1 C2 109.0(3) . . ? 
C1 Fe1 C9 134.5(3) . . ? 
C7 Fe1 C9 69.4(2) . . ? 
C5 Fe1 C9 176.2(3) . . ? 
C8 Fe1 C9 40.5(2) . . ? 
C2 Fe1 C9 108.5(3) . . ? 
C1 Fe1 C10 174.2(3) . . ? 
C7 Fe1 C10 69.1(2) . . ? 
C5 Fe1 C10 143.7(3) . . ? 
C8 Fe1 C10 68.0(3) . . ? 
C2 Fe1 C10 136.3(2) . . ? 
C9 Fe1 C10 39.9(3) . . ? 
C1 Fe1 C6 140.5(2) . . ? 
C7 Fe1 C6 41.7(3) . . ? 
C5 Fe1 C6 113.5(2) . . ? 
C8 Fe1 C6 69.6(3) . . ? 
C2 Fe1 C6 177.1(2) . . ? 
C9 Fe1 C6 68.7(2) . . ? 
C10 Fe1 C6 40.9(2) . . ? 
C1 Fe1 C3 69.2(2) . . ? 
C7 Fe1 C3 177.6(2) . . ? 
C5 Fe1 C3 67.9(2) . . ? 
C8 Fe1 C3 139.1(3) . . ? 
C2 Fe1 C3 39.9(3) . . ? 
C9 Fe1 C3 112.7(2) . . ? 
C10 Fe1 C3 113.2(2) . . ? 
C6 Fe1 C3 139.7(3) . . ? 
C1 Fe1 C4 69.8(3) . . ? 
C7 Fe1 C4 138.7(2) . . ? 
C5 Fe1 C4 40.6(2) . . ? 
C8 Fe1 C4 176.5(3) . . ? 
C2 Fe1 C4 68.4(3) . . ? 
C9 Fe1 C4 142.1(2) . . ? 
C10 Fe1 C4 115.5(3) . . ? 
C6 Fe1 C4 113.1(3) . . ? 
C3 Fe1 C4 40.2(2) . . ? 
C29 P1 C7 101.5(3) . . ? 
C29 P1 C23 107.8(3) . . ? 
C7 P1 C23 101.3(2) . . ? 
C29 P1 Pd1 111.2(2) . . ? 
C7 P1 Pd1 122.9(2) . . ? 
C23 P1 Pd1 110.8(2) . . ? 
C1 P2 C11 110.2(2) . . ? 
C1 P2 C17 101.9(3) . . ? 
C11 P2 C17 104.7(3) . . ? 
C1 P2 Pd1 113.2(2) . . ? 
C11 P2 Pd1 108.7(2) . . ? 
C17 P2 Pd1 117.5(2) . . ? 
C5 C1 C2 106.1(5) . . ? 
C5 C1 P2 122.4(4) . . ? 
C2 C1 P2 131.5(5) . . ? 
C5 C1 Fe1 69.8(3) . . ? 
C2 C1 Fe1 70.2(3) . . ? 
P2 C1 Fe1 123.9(2) . . ? 
C3 C2 C1 107.9(6) . . ? 
C3 C2 Fe1 71.1(4) . . ? 
C1 C2 Fe1 67.6(3) . . ? 
C2 C3 C4 109.8(5) . . ? 
C2 C3 Fe1 68.9(3) . . ? 
C4 C3 Fe1 70.1(3) . . ? 
C5 C4 C3 107.0(7) . . ? 
C5 C4 Fe1 67.9(3) . . ? 
C3 C4 Fe1 69.8(3) . . ? 
C4 C5 C1 109.3(5) . . ? 
C4 C5 Fe1 71.5(3) . . ? 
C1 C5 Fe1 68.3(3) . . ? 
C10 C6 C7 106.1(6) . . ? 
C10 C6 Fe1 69.3(3) . . ? 
C7 C6 Fe1 67.5(3) . . ? 
C8 C7 C6 107.4(5) . . ? 
C8 C7 P1 126.4(5) . . ? 
C6 C7 P1 126.2(5) . . ? 
C8 C7 Fe1 69.5(3) . . ? 
C6 C7 Fe1 70.8(3) . . ? 
P1 C7 Fe1 123.8(3) . . ? 
C9 C8 C7 108.3(6) . . ? 
C9 C8 Fe1 70.6(3) . . ? 
C7 C8 Fe1 68.7(3) . . ? 
C10 C9 C8 108.5(5) . . ? 
C10 C9 Fe1 70.2(3) . . ? 
C8 C9 Fe1 68.8(3) . . ? 
C9 C10 C6 109.7(6) . . ? 
C9 C10 Fe1 70.0(4) . . ? 
C6 C10 Fe1 69.8(3) . . ? 
C12 C11 C16 118.6(5) . . ? 
C12 C11 P2 123.2(4) . . ? 
C16 C11 P2 118.2(4) . . ? 
C11 C12 C13 120.2(6) . . ? 
C14 C13 C12 119.8(6) . . ? 
C13 C14 C15 121.0(6) . . ? 
C14 C15 C16 119.9(6) . . ? 
C15 C16 C11 120.4(6) . . ? 
C22 C17 C18 119.9(6) . . ? 
C22 C17 P2 121.9(5) . . ? 
C18 C17 P2 118.2(6) . . ? 
C19 C18 C17 119.6(8) . . ? 
C20 C19 C18 120.8(7) . . ? 
C19 C20 C21 120.4(6) . . ? 
C20 C21 C22 118.7(9) . . ? 
C17 C22 C21 120.7(7) . . ? 
C24 C23 C28 118.5(5) . . ? 
C24 C23 P1 122.1(4) . . ? 
C28 C23 P1 119.4(5) . . ? 
C25 C24 C23 120.5(5) . . ? 
C26 C25 C24 120.3(6) . . ? 
C27 C26 C25 120.0(5) . . ? 
C26 C27 C28 119.9(5) . . ? 
C27 C28 C23 120.8(6) . . ? 
C30 C29 C34 116.8(6) . . ? 
C30 C29 P1 123.2(5) . . ? 
C34 C29 P1 120.0(4) . . ? 
C31 C30 C29 121.6(6) . . ? 
C30 C31 C32 120.8(6) . . ? 
C31 C32 C33 118.9(7) . . ? 
C34 C33 C32 120.3(6) . . ? 
C33 C34 C29 121.5(6) . . ? 
Cl4 C35 Cl3 116.7(4) . . ? 
 
_refine_diff_density_max    1.009 
_refine_diff_density_min   -0.864 
_refine_diff_density_rms    0.141 
