# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_2009src0359 _shelx_title ' 2009src0359 in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 364.72 _exptl_crystal_F_000 1048.00 _reflns_d_resolution_high 0.7701 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 13.2510 _cell_length_b 8.7390 _cell_length_c 17.9308 _cell_angle_alpha 90.000 _cell_angle_beta 110.145 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 48503.95 47234.02 1337.37 o 4 0 0 26553.49 25970.36 719.89 o 5 0 0 57481.80 55700.91 1499.55 o 6 0 0 5010.66 5033.78 132.06 o 7 0 0 41375.55 41736.68 983.18 o 8 0 0 49040.34 49849.50 1161.01 o 9 0 0 8452.80 8462.33 200.66 o 10 0 0 27123.86 27545.18 695.37 o 11 0 0 457.64 481.49 55.44 o 12 0 0 32944.73 34120.98 1102.48 o 13 0 0 5694.94 5302.57 222.60 o 14 0 0 13980.20 13921.01 799.98 o 15 0 0 10685.69 10473.59 804.85 o 16 0 0 197.92 187.17 71.25 o 2 1 0 20901.59 19468.65 435.13 o 3 1 0 17929.77 17027.40 333.87 o 4 1 0 17647.49 17112.83 349.43 o 5 1 0 4835.18 5000.56 91.17 o 6 1 0 43706.39 43902.84 719.67 o 7 1 0 10658.09 10843.55 170.80 o 8 1 0 17198.59 17056.39 289.86 o 9 1 0 20156.02 20639.82 391.43 o 10 1 0 1344.79 1309.76 44.98 o 11 1 0 29354.54 29975.78 755.67 o 12 1 0 934.61 903.58 38.37 o 13 1 0 16878.29 16566.37 604.39 o 14 1 0 4831.39 5155.62 299.43 o 15 1 0 5183.41 5178.04 274.96 o 16 1 0 10370.38 9400.86 1077.54 o 0 2 0 133019.91 120789.81 3353.46 o 1 2 0 127.86 109.17 11.33 o 2 2 0 4590.24 4469.66 92.65 o 3 2 0 3009.22 2812.22 59.37 o 4 2 0 9896.85 9969.79 185.52 o 5 2 0 30588.86 30243.83 540.17 o 6 2 0 10.58 43.70 17.46 o 7 2 0 34325.24 34172.81 574.50 o 8 2 0 11223.76 11319.46 210.22 o 9 2 0 14439.72 14795.68 286.99 o 10 2 0 10957.38 11196.01 217.05 o 11 2 0 6.89 23.79 18.69 o 12 2 0 15432.58 15159.40 406.97 o 13 2 0 3754.90 3580.44 179.65 o 14 2 0 7790.56 8002.75 344.97 o 15 2 0 7270.65 7006.09 441.62 o 1 3 0 59253.38 59163.16 1216.68 o 2 3 0 26606.52 25893.90 519.20 o 3 3 0 17430.70 17484.51 290.28 o 4 3 0 39989.51 38817.02 679.91 o 5 3 0 2044.88 2186.86 48.37 o 6 3 0 87470.64 87946.09 1266.62 o 7 3 0 7088.00 7415.02 114.43 o 8 3 0 25431.55 25823.17 397.61 o 9 3 0 15345.02 15784.82 301.80 o 10 3 0 1946.44 2031.45 56.19 o 11 3 0 19599.90 19791.45 676.69 o 12 3 0 2959.02 2904.33 123.95 o 13 3 0 7598.01 7513.83 386.30 o 14 3 0 11049.00 11989.00 565.54 o 15 3 0 1568.17 1539.79 145.29 o 0 4 0 43481.32 45479.23 1298.59 o 1 4 0 5862.98 5973.81 131.08 o 2 4 0 32304.15 33064.22 587.42 o 3 4 0 22157.58 21648.78 367.67 o 4 4 0 2891.93 2949.30 54.83 o 5 4 0 60772.32 62498.91 926.78 o 6 4 0 2814.20 2931.00 64.31 o 7 4 0 30862.65 31078.52 469.29 o 8 4 0 6928.03 6923.61 142.52 o 9 4 0 10857.54 10985.26 255.04 o 10 4 0 11523.39 12165.50 399.19 o 11 4 0 130.45 191.73 59.88 o 12 4 0 9382.81 9433.32 433.68 o 13 4 0 6540.77 6579.50 401.83 o 14 4 0 3082.87 2953.49 285.66 o 15 4 0 7910.20 7377.06 517.44 o 1 5 0 13469.62 13892.24 281.68 o 2 5 0 5677.58 5787.34 138.71 o 3 5 0 5591.25 5820.86 113.43 o 4 5 0 8227.88 8261.72 141.07 o 5 5 0 120.96 154.73 31.24 o 6 5 0 16689.59 17002.80 391.35 o 7 5 0 949.78 991.19 56.31 o 8 5 0 4826.04 4981.88 120.69 o 9 5 0 1279.07 1463.95 71.22 o 10 5 0 2416.34 2472.01 131.92 o 11 5 0 7181.14 7502.46 379.77 o 12 5 0 40.87 117.32 72.42 o 13 5 0 4918.49 5000.34 311.18 o 14 5 0 2965.80 3138.64 238.17 o 0 6 0 15888.34 15236.23 495.48 o 1 6 0 878.74 823.12 38.70 o 2 6 0 17992.45 19030.50 417.94 o 3 6 0 2625.21 2546.89 77.45 o 4 6 0 1755.46 1902.94 79.11 o 5 6 0 10412.49 10399.22 254.59 o 6 6 0 1200.84 1013.20 57.02 o 7 6 0 5228.78 5207.64 172.71 o 8 6 0 1537.10 1620.33 85.99 o 9 6 0 3022.44 2844.75 134.86 o 10 6 0 5849.70 6120.20 264.49 o 11 6 0 186.10 48.16 64.89 o 12 6 0 7769.79 7918.69 464.11 o 13 6 0 980.16 783.25 134.52 o 1 7 0 16769.86 17771.57 460.42 o 2 7 0 951.71 981.06 64.05 o 3 7 0 10387.62 10222.63 279.80 o 4 7 0 7384.71 7349.78 228.59 o 5 7 0 23.16 29.95 16.52 o 6 7 0 7783.49 7652.75 316.46 o 7 7 0 2871.32 2611.19 126.75 o 8 7 0 3151.53 3090.82 192.00 o 9 7 0 5418.18 6058.98 315.29 o 10 7 0 505.96 773.28 98.38 o 11 7 0 10196.02 10571.41 743.54 o 12 7 0 1152.89 980.48 190.62 o 0 8 0 2949.99 3053.40 231.66 o 1 8 0 14.99 94.71 46.91 o 2 8 0 2696.97 2624.43 128.97 o 3 8 0 112.87 140.81 36.35 o 4 8 0 1283.31 1172.32 66.50 o 5 8 0 1415.70 1459.41 66.12 o 6 8 0 276.91 185.92 49.44 o 7 8 0 2278.13 2191.11 146.57 o 8 8 0 559.09 521.62 117.57 o 9 8 0 720.61 685.11 108.43 o 10 8 0 2348.00 2249.79 183.29 o 11 8 0 33.09 -92.39 82.24 o 1 9 0 103.45 108.96 34.75 o 2 9 0 168.80 262.15 55.26 o 3 9 0 183.23 225.27 47.02 o 4 9 0 276.81 313.30 49.52 o 5 9 0 2.32 -66.03 60.69 o 6 9 0 279.31 411.11 164.18 o 7 9 0 31.52 41.22 85.99 o 8 9 0 755.09 576.65 115.70 o 9 9 0 22.12 147.80 107.04 o 0 10 0 488.67 516.06 97.00 o 1 10 0 153.33 67.34 52.91 o 2 10 0 99.80 119.92 55.79 o 3 10 0 826.17 974.69 87.78 o 4 10 0 19.36 -70.50 63.28 o 5 10 0 888.13 882.12 144.22 o 6 10 0 180.61 272.31 108.83 o 7 10 0 646.71 646.76 133.52 o 1 11 0 6.53 115.64 126.73 o 2 11 0 121.42 101.04 100.95 o 3 11 0 271.17 138.77 78.81 o -16 1 1 89.94 67.06 81.56 o -15 1 1 14.70 -42.74 37.42 o -14 1 1 297.52 267.38 44.52 o -13 1 1 714.77 696.38 41.77 o -12 1 1 31.96 94.75 23.28 o -11 1 1 2439.30 2570.94 76.37 o -10 1 1 1376.19 1388.02 41.87 o -9 1 1 4043.45 4212.48 80.04 o -8 1 1 2069.34 2069.89 47.30 o -7 1 1 147.25 117.99 12.13 o -6 1 1 4151.96 4186.64 89.32 o -5 1 1 178.61 234.71 13.66 o -4 1 1 31.02 23.62 7.40 o -3 1 1 2049.32 1917.26 56.10 o -2 1 1 1938.03 1928.72 63.14 o 1 1 1 2765.51 2926.72 73.23 o 2 1 1 2264.39 2412.52 51.80 o 3 1 1 11374.74 11724.81 232.92 o 4 1 1 3726.17 3679.44 76.78 o 5 1 1 24.52 32.58 13.26 o 6 1 1 432.31 490.43 23.12 o 7 1 1 946.60 994.04 41.60 o 8 1 1 332.39 351.69 26.53 o 9 1 1 2165.59 2303.22 61.04 o 10 1 1 2831.90 2825.89 85.97 o 11 1 1 1144.39 1284.97 52.93 o 12 1 1 2724.63 2705.33 93.00 o 13 1 1 62.92 3.62 30.21 o 14 1 1 581.50 575.59 57.21 o 15 1 1 13.09 109.09 55.29 o -16 2 1 168.72 65.19 98.31 o -15 2 1 34.58 116.82 81.09 o -14 2 1 373.08 517.13 84.19 o -13 2 1 281.61 193.75 47.57 o -12 2 1 3100.67 2951.27 101.73 o -11 2 1 4902.80 5124.18 145.55 o -10 2 1 1452.22 1536.80 44.25 o -9 2 1 3742.55 3745.95 84.73 o -8 2 1 195.27 189.92 29.90 o -7 2 1 2787.06 2799.48 54.08 o -6 2 1 108.56 140.75 17.52 o -5 2 1 999.08 1012.05 31.10 o -4 2 1 6471.18 6685.34 125.35 o -3 2 1 17160.17 17186.31 365.80 o -2 2 1 11446.19 10996.05 239.22 o -1 2 1 17.04 -12.71 8.47 o 0 2 1 209.69 256.91 17.82 o 1 2 1 12334.70 11903.09 261.83 o 2 2 1 36450.32 36200.13 787.96 o 3 2 1 6752.62 6698.47 125.07 o 4 2 1 534.65 591.52 34.98 o 5 2 1 1775.50 1932.33 44.17 o 6 2 1 35.27 30.14 16.65 o 7 2 1 582.34 560.57 26.32 o 8 2 1 1159.96 1198.69 39.29 o 9 2 1 1321.88 1305.82 43.50 o 10 2 1 5283.57 5251.91 154.36 o 11 2 1 2672.41 2546.59 95.53 o 12 2 1 665.87 621.78 46.49 o 13 2 1 2275.50 2147.14 110.49 o 14 2 1 485.38 398.84 49.14 o 15 2 1 873.30 782.22 138.49 o -15 3 1 2081.15 1870.82 282.40 o -14 3 1 2.59 73.70 57.55 o -13 3 1 3086.24 3036.99 166.87 o -12 3 1 2651.97 2687.51 120.55 o -11 3 1 1336.27 1320.25 65.79 o -10 3 1 5011.77 4972.60 184.61 o -9 3 1 211.11 183.94 25.89 o -8 3 1 2120.75 2273.28 62.38 o -7 3 1 1347.44 1347.71 44.80 o -6 3 1 6311.65 6259.69 123.62 o -5 3 1 1128.15 985.22 28.80 o -4 3 1 140.15 193.53 13.00 o -3 3 1 16967.21 16874.23 353.93 o -2 3 1 3447.82 3602.86 80.70 o -1 3 1 3656.52 3233.56 110.54 o 0 3 1 3836.34 3731.46 76.75 o 1 3 1 4147.57 4071.29 88.07 o 2 3 1 12809.55 12538.19 239.76 o 3 3 1 2167.61 2133.15 52.35 o 4 3 1 6294.60 6071.80 114.63 o 5 3 1 2048.96 2195.46 49.76 o 6 3 1 129.25 111.28 22.60 o 7 3 1 1292.22 1320.52 55.66 o 8 3 1 272.61 321.40 25.33 o 9 3 1 3755.94 3937.35 93.10 o 10 3 1 557.89 534.74 34.72 o 11 3 1 4940.90 4896.79 148.61 o 12 3 1 1681.60 1721.18 105.59 o 13 3 1 665.92 583.45 53.90 o 14 3 1 1862.98 1781.40 182.02 o 15 3 1 95.63 -12.93 70.43 o -15 4 1 2379.53 1782.07 199.01 o -14 4 1 3138.15 2939.10 232.02 o -13 4 1 61.63 27.94 58.53 o -12 4 1 5906.38 5876.16 281.26 o -11 4 1 2176.25 2133.31 129.14 o -10 4 1 2569.68 2584.19 174.24 o -9 4 1 3251.77 3387.85 128.16 o -8 4 1 8.36 18.97 20.19 o -7 4 1 12104.14 12241.94 318.13 o -6 4 1 377.94 366.51 23.91 o -5 4 1 12632.73 12855.78 270.85 o -4 4 1 21505.64 21552.20 339.92 o -3 4 1 3205.50 3390.15 134.00 o -2 4 1 35047.54 35342.41 684.28 o -1 4 1 41.08 68.22 15.64 o 0 4 1 5154.11 4993.73 105.52 o 1 4 1 14097.73 14274.18 275.87 o 2 4 1 8259.97 8344.90 152.07 o 3 4 1 18421.49 18468.13 303.68 o 4 4 1 12998.86 13448.27 209.35 o 5 4 1 7203.29 7126.47 128.74 o 6 4 1 8449.21 8439.45 152.57 o 7 4 1 1627.39 1637.79 44.10 o 8 4 1 7107.49 7237.92 153.82 o 9 4 1 44.45 46.79 20.13 o 10 4 1 8910.30 8973.38 276.67 o 11 4 1 1737.37 1663.26 74.48 o 12 4 1 1005.65 1002.97 168.08 o 13 4 1 3822.47 3822.97 284.24 o 14 4 1 3.42 156.17 76.54 o -14 5 1 1895.51 1975.18 174.16 o -13 5 1 8416.33 8569.24 477.00 o -12 5 1 146.31 187.04 52.24 o -11 5 1 5936.50 6051.96 279.82 o -10 5 1 4127.19 4085.21 238.47 o -9 5 1 475.79 450.33 51.28 o -8 5 1 8441.71 8598.37 238.15 o -7 5 1 1643.48 1624.31 73.85 o -6 5 1 20374.91 20086.98 428.64 o -5 5 1 14938.60 14890.80 314.07 o -4 5 1 12378.00 12131.99 214.04 o -3 5 1 34588.67 35644.44 646.50 o -2 5 1 74.74 102.01 25.94 o -1 5 1 17907.56 18409.82 360.51 o 0 5 1 2190.51 2203.14 54.31 o 1 5 1 9725.85 10111.85 180.30 o 2 5 1 22929.32 22836.83 506.92 o 3 5 1 406.03 415.01 30.20 o 4 5 1 22184.59 21986.03 339.43 o 5 5 1 10953.62 11164.36 201.42 o 6 5 1 5266.87 5187.21 98.42 o 7 5 1 15019.56 15179.45 264.91 o 8 5 1 2831.25 2937.85 85.13 o 9 5 1 17456.31 18299.43 466.41 o 10 5 1 1049.30 942.89 56.25 o 11 5 1 4688.81 4631.28 216.07 o 12 5 1 3943.62 3683.44 252.13 o 13 5 1 321.23 493.34 90.23 o 14 5 1 4083.03 3434.11 315.16 o -13 6 1 104.57 88.00 78.73 o -12 6 1 7128.52 7170.85 429.44 o -11 6 1 3935.96 4090.92 450.38 o -10 6 1 2583.50 2661.19 249.38 o -9 6 1 8800.55 8687.74 340.33 o -8 6 1 1611.18 1620.61 75.80 o -7 6 1 14774.51 14956.47 508.36 o -6 6 1 7961.36 7554.75 201.43 o -5 6 1 3017.05 3090.06 66.37 o -4 6 1 26079.38 26849.19 594.29 o -3 6 1 1433.91 1395.98 61.11 o -2 6 1 16258.10 16386.49 392.90 o -1 6 1 1657.33 1638.58 77.85 o 0 6 1 5525.14 5804.06 135.77 o 1 6 1 5405.07 5202.95 128.70 o 2 6 1 1886.32 2047.90 64.57 o 3 6 1 13820.87 13579.68 281.86 o 4 6 1 3022.06 3004.28 78.27 o 5 6 1 14338.77 14769.39 289.32 o 6 6 1 7917.78 8157.24 169.14 o 7 6 1 6236.02 6375.59 215.85 o 8 6 1 13678.30 14194.91 414.30 o 9 6 1 96.61 147.79 37.96 o 10 6 1 10981.12 10878.36 658.26 o 11 6 1 2005.78 1849.10 165.03 o 12 6 1 1830.84 2130.14 171.86 o 13 6 1 5032.27 4838.35 319.41 o -12 7 1 1014.86 842.13 223.48 o -11 7 1 7196.56 6674.06 439.28 o -10 7 1 8450.55 8767.61 462.59 o -9 7 1 1201.31 1023.02 112.73 o -8 7 1 12991.26 12311.80 522.67 o -7 7 1 1461.59 1365.76 94.58 o -6 7 1 10073.19 10225.90 438.82 o -5 7 1 13917.23 14122.98 343.95 o -4 7 1 3766.88 3912.98 105.15 o -3 7 1 15663.58 16354.09 419.92 o -2 7 1 922.08 929.86 49.38 o -1 7 1 12812.92 12683.17 314.31 o 0 7 1 4776.06 4675.18 123.47 o 1 7 1 7143.74 7464.78 195.61 o 2 7 1 16576.46 16727.54 391.05 o 3 7 1 2.14 -14.95 24.11 o 4 7 1 17212.21 17402.30 453.70 o 5 7 1 2050.58 2127.58 128.84 o 6 7 1 6333.74 6640.23 216.07 o 7 7 1 11333.88 10920.02 377.75 o 8 7 1 1095.53 879.89 159.38 o 9 7 1 15651.00 16590.64 773.89 o 10 7 1 2322.56 2329.41 210.42 o 11 7 1 3472.50 3413.84 242.11 o 12 7 1 5043.47 4649.78 374.77 o -11 8 1 4213.02 4234.95 269.89 o -10 8 1 8123.00 8325.20 438.68 o -9 8 1 12022.20 12654.48 633.25 o -8 8 1 1080.14 1117.89 119.89 o -7 8 1 18062.30 18492.79 1115.33 o -6 8 1 1859.68 1867.62 144.61 o -5 8 1 8206.10 8369.49 322.38 o -4 8 1 16342.54 16122.22 657.13 o -3 8 1 1677.76 1808.18 84.44 o -2 8 1 24918.35 25150.12 921.69 o -1 8 1 4668.12 5104.50 204.67 o 0 8 1 20503.46 20628.63 721.22 o 1 8 1 20383.65 20828.70 722.17 o 2 8 1 4010.81 3905.54 178.13 o 3 8 1 26825.42 26777.10 911.68 o 4 8 1 883.10 860.27 98.14 o 5 8 1 14896.10 14964.01 573.03 o 6 8 1 6949.89 7035.09 252.89 o 7 8 1 3135.56 3237.00 262.56 o 8 8 1 16006.30 16677.71 726.47 o 9 8 1 1475.64 1520.62 148.70 o 10 8 1 10427.57 10483.34 713.79 o 11 8 1 5332.41 5258.04 422.86 o -10 9 1 8740.54 8901.57 592.33 o -9 9 1 2771.63 2709.53 270.65 o -8 9 1 12945.70 12788.25 892.70 o -7 9 1 315.58 266.84 78.89 o -6 9 1 8710.52 8663.61 875.40 o -5 9 1 6626.80 6750.30 580.67 o -4 9 1 4197.07 4295.11 240.96 o -3 9 1 13705.69 14729.26 686.19 o -2 9 1 627.91 640.11 70.07 o -1 9 1 21659.37 21552.18 849.40 o 0 9 1 11927.37 11558.16 457.28 o 1 9 1 7296.16 7376.43 321.73 o 2 9 1 22567.29 22935.21 1212.21 o 3 9 1 92.83 80.34 55.05 o 4 9 1 15810.93 15933.72 610.47 o 5 9 1 1589.17 1484.19 110.94 o 6 9 1 5220.59 4781.50 325.80 o 7 9 1 9165.50 10181.04 549.75 o 8 9 1 57.26 13.84 89.66 o 9 9 1 11199.55 11201.19 591.48 o -7 10 1 7684.62 7959.08 501.29 o -6 10 1 3306.33 2891.93 243.71 o -5 10 1 4053.24 3719.75 253.28 o -4 10 1 8061.30 8004.18 555.56 o -3 10 1 61.82 114.13 48.66 o -2 10 1 11334.11 11764.27 583.79 o -1 10 1 2061.08 1758.59 133.74 o 0 10 1 7290.93 7286.00 344.52 o 1 10 1 11164.37 11170.58 635.77 o 2 10 1 919.25 916.17 96.63 o 3 10 1 10646.70 10618.74 517.67 o 4 10 1 490.97 323.42 74.59 o 5 10 1 6231.74 6083.67 393.38 o 6 10 1 2497.35 2358.53 187.62 o 7 10 1 2229.96 2027.24 166.27 o -4 11 1 3072.41 2668.10 257.07 o -3 11 1 9816.54 9239.25 717.43 o -2 11 1 6.10 -43.93 96.32 o -1 11 1 10892.01 11131.70 833.70 o 0 11 1 4169.80 3654.24 259.37 o 1 11 1 3058.33 2679.86 249.43 o 2 11 1 9496.44 9209.76 689.24 o 3 11 1 29.19 30.57 69.41 o -16 0 2 10119.07 8797.23 761.05 o -15 0 2 831.76 900.91 96.30 o -14 0 2 8950.00 9199.24 430.05 o -13 0 2 4654.23 4716.95 206.28 o -12 0 2 3510.37 3659.37 136.88 o -11 0 2 28162.10 28198.15 791.69 o -10 0 2 43.39 92.42 21.51 o -9 0 2 53957.64 54059.79 1048.17 o -8 0 2 9830.48 9619.16 207.34 o -7 0 2 34835.44 34044.29 800.06 o -6 0 2 32966.25 32761.81 778.18 o -5 0 2 16522.07 16773.32 413.91 o -4 0 2 82613.59 78781.20 2142.08 o -3 0 2 9815.39 9815.09 232.12 o 1 0 2 89035.05 80595.48 3189.61 o 2 0 2 44841.34 43363.98 1190.54 o 3 0 2 120015.40 115588.88 2546.70 o 4 0 2 49125.56 48487.19 1173.81 o 5 0 2 21213.49 21052.89 492.77 o 6 0 2 68628.77 68196.05 1579.47 o 7 0 2 1642.78 1691.39 92.92 o 8 0 2 20989.66 21411.96 524.16 o 9 0 2 16265.46 15944.62 517.68 o 10 0 2 5573.70 5589.84 192.45 o 11 0 2 44020.62 43474.48 1809.91 o 12 0 2 1.99 9.79 42.55 o 13 0 2 23300.21 23963.74 1472.38 o 14 0 2 5441.40 5735.51 446.48 o 15 0 2 10104.51 10395.65 1051.99 o -16 1 2 26.86 127.23 78.73 o -15 1 2 11830.40 11028.57 500.01 o -14 1 2 3888.64 3664.16 188.01 o -13 1 2 7966.05 7797.54 247.80 o -12 1 2 14235.04 14864.36 374.03 o -11 1 2 41.35 43.68 19.32 o -10 1 2 33282.07 32557.13 500.36 o -9 1 2 11451.96 11701.46 206.12 o -8 1 2 46632.30 45439.08 652.16 o -7 1 2 18107.86 18053.08 283.29 o -6 1 2 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