# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_2008src0881 _shelx_title ' 2008src0881 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 499.89 _exptl_crystal_F_000 1364.00 _reflns_d_resolution_high 0.7700 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.1958 _cell_length_b 13.3800 _cell_length_c 14.7281 _cell_angle_alpha 94.551 _cell_angle_beta 95.856 _cell_angle_gamma 94.182 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 12258.78 12205.33 331.00 o 3 0 0 457.91 538.20 17.67 o 4 0 0 189.06 252.67 21.18 o 5 0 0 314.35 367.94 26.98 o 6 0 0 1942.25 2323.25 57.17 o 7 0 0 19369.41 19003.55 354.93 o 8 0 0 7979.55 8082.75 180.03 o 9 0 0 14430.07 14362.95 360.08 o 10 0 0 18033.18 18285.75 466.21 o 11 0 0 5082.28 5394.76 199.43 o 12 0 0 954.75 1047.52 107.23 o 13 0 0 3103.27 2916.90 174.55 o 14 0 0 100.58 71.87 98.56 o 15 0 0 4186.14 4119.99 496.55 o -15 1 0 18.00 253.12 128.48 o -14 1 0 3776.71 4004.41 423.25 o -13 1 0 1865.64 1831.61 122.87 o -12 1 0 15546.11 16644.76 672.68 o -11 1 0 104.87 130.87 57.21 o -10 1 0 5328.51 5290.07 221.36 o -9 1 0 9268.33 8703.10 208.13 o -8 1 0 7999.94 7580.81 178.75 o -7 1 0 2296.19 2081.43 63.28 o -6 1 0 9698.48 9930.91 217.59 o -5 1 0 55828.18 55396.65 1145.42 o -4 1 0 9538.38 9392.89 201.35 o -3 1 0 146585.44 140875.73 2953.22 o -2 1 0 2078.37 2021.08 54.49 o 2 1 0 301.97 296.43 15.15 o 3 1 0 14551.54 14096.29 262.98 o 4 1 0 10916.30 10750.56 188.74 o 5 1 0 72572.40 70579.09 1013.34 o 6 1 0 1870.66 1804.91 42.84 o 7 1 0 13267.40 13232.57 272.66 o 8 1 0 669.54 797.68 36.30 o 9 1 0 656.70 662.66 33.02 o 10 1 0 1007.29 930.72 59.39 o 11 1 0 4799.92 5398.37 233.56 o 12 1 0 8395.84 8845.08 511.21 o 13 1 0 134.85 382.98 87.93 o 14 1 0 13738.25 14040.68 1055.47 o 15 1 0 2540.89 2802.67 293.05 o -15 2 0 1621.55 1763.29 181.64 o -14 2 0 102.25 59.92 123.39 o -13 2 0 322.11 280.83 64.94 o -12 2 0 2582.86 2563.67 165.16 o -11 2 0 13780.71 13625.71 430.96 o -10 2 0 3462.10 3679.31 146.46 o -9 2 0 36237.36 36092.98 853.86 o -8 2 0 23444.91 22224.96 934.89 o -7 2 0 3469.74 3218.92 161.70 o -6 2 0 9932.65 10358.33 187.53 o -5 2 0 1173.64 1328.79 41.61 o -4 2 0 23179.36 23589.27 443.31 o -3 2 0 2959.32 3096.03 86.39 o -2 2 0 38167.95 37872.83 906.52 o -1 2 0 111.27 95.46 16.15 o 0 2 0 9990.78 9463.45 343.20 o 1 2 0 72.27 85.41 18.09 o 2 2 0 80023.75 75359.81 1658.65 o 3 2 0 3316.40 3469.92 70.47 o 4 2 0 48110.09 48380.46 814.56 o 5 2 0 121.27 130.04 20.37 o 6 2 0 50040.89 52166.85 878.80 o 7 2 0 14380.88 14477.27 252.48 o 8 2 0 28229.24 28052.10 726.16 o 9 2 0 11026.04 11610.82 360.40 o 10 2 0 2921.05 2987.14 124.73 o 11 2 0 8640.27 9015.47 420.66 o 12 2 0 43.32 36.42 59.67 o 13 2 0 1121.57 1013.84 141.57 o 14 2 0 144.66 50.18 95.19 o 15 2 0 4629.74 4536.06 653.68 o -15 3 0 114.66 144.81 175.62 o -14 3 0 10112.25 9925.60 565.95 o -13 3 0 17.36 81.97 87.78 o -12 3 0 17959.35 19254.71 819.06 o -11 3 0 3487.08 3635.57 160.24 o -10 3 0 910.95 939.78 90.59 o -9 3 0 16.26 -5.67 27.28 o -8 3 0 2886.85 2734.38 89.43 o -7 3 0 20141.27 20757.64 494.41 o -6 3 0 13685.84 13450.03 335.94 o -5 3 0 59062.87 60124.10 1214.13 o -4 3 0 62919.30 64682.07 1226.81 o -3 3 0 17617.00 17440.89 363.61 o -2 3 0 1363.75 1510.05 44.16 o -1 3 0 16708.07 16493.20 386.75 o 0 3 0 96.73 87.55 10.61 o 1 3 0 1490.72 1612.68 43.51 o 2 3 0 304.61 345.17 14.38 o 3 3 0 59855.00 59001.83 1264.84 o 4 3 0 7018.40 7161.13 136.60 o 5 3 0 38829.40 37892.90 643.96 o 6 3 0 1105.07 1175.05 41.81 o 7 3 0 1951.93 1902.28 56.05 o 8 3 0 1407.23 1444.97 60.33 o 9 3 0 769.11 944.96 89.38 o 10 3 0 1784.19 1651.15 78.40 o 11 3 0 9420.60 9035.95 476.87 o 12 3 0 7472.34 7011.86 497.70 o 13 3 0 6197.31 7059.59 502.84 o 14 3 0 8066.13 7929.60 632.60 o 15 3 0 170.48 179.88 262.87 o -15 4 0 447.07 541.61 114.77 o -14 4 0 117.46 127.49 160.95 o -13 4 0 6858.84 6773.88 350.36 o -12 4 0 290.71 248.34 137.48 o -11 4 0 7271.04 6921.56 442.64 o -10 4 0 1332.01 1271.44 68.37 o -9 4 0 16633.20 17247.90 438.33 o -8 4 0 11519.21 11511.67 357.32 o -7 4 0 20118.48 20064.49 402.77 o -6 4 0 737.72 807.25 37.36 o -5 4 0 150.44 116.02 20.10 o -4 4 0 77.74 122.51 16.57 o -3 4 0 22044.02 22162.75 481.55 o -2 4 0 54556.25 53139.40 1042.86 o -1 4 0 14699.00 14603.41 297.37 o 0 4 0 44559.79 43754.27 1025.18 o 1 4 0 3010.04 3037.64 79.34 o 2 4 0 6242.09 6041.14 122.12 o 3 4 0 1527.17 1625.12 40.43 o 4 4 0 1768.24 1932.96 43.08 o 5 4 0 200.93 256.84 15.29 o 6 4 0 16409.80 16071.34 293.96 o 7 4 0 2525.40 2502.93 110.33 o 8 4 0 17771.60 18761.65 473.75 o 9 4 0 1880.84 1966.89 84.37 o 10 4 0 17074.48 16597.69 733.09 o 11 4 0 1204.56 1362.49 191.27 o 12 4 0 346.39 364.23 60.73 o 13 4 0 304.69 321.73 197.74 o 14 4 0 4802.82 4996.36 677.43 o -15 5 0 1033.64 899.32 215.95 o -14 5 0 13450.45 13016.31 667.11 o -13 5 0 190.56 161.84 80.45 o -12 5 0 5429.24 5505.83 282.90 o -11 5 0 604.83 643.00 81.03 o -10 5 0 194.10 163.50 41.56 o -9 5 0 171.94 130.34 59.95 o -8 5 0 3001.45 3197.28 143.91 o -7 5 0 137.94 109.35 29.94 o -6 5 0 25609.57 25230.38 622.89 o -5 5 0 13754.47 13686.18 363.35 o -4 5 0 10571.77 9871.78 360.09 o -3 5 0 26723.48 26826.19 757.12 o -2 5 0 2860.78 2882.20 86.15 o -1 5 0 417.91 413.55 24.30 o 0 5 0 91.24 74.28 22.98 o 1 5 0 15792.10 16001.73 394.01 o 2 5 0 15130.18 15804.02 276.10 o 3 5 0 109143.38 102241.48 2848.59 o 4 5 0 918.29 1065.95 34.30 o 5 5 0 6841.69 6332.50 127.23 o 6 5 0 2550.22 2747.30 59.18 o 7 5 0 10708.20 10935.42 263.69 o 8 5 0 2607.49 2592.60 91.47 o 9 5 0 2141.96 2216.21 102.24 o 10 5 0 1357.77 1316.88 115.51 o 11 5 0 16474.13 16830.17 975.88 o 12 5 0 2019.37 2134.83 160.35 o 13 5 0 6683.95 6424.61 445.50 o 14 5 0 2162.41 1984.69 207.01 o -15 6 0 909.08 736.78 173.53 o -14 6 0 921.08 844.93 165.45 o -13 6 0 3205.89 2931.03 263.95 o -12 6 0 279.31 116.30 99.90 o -11 6 0 15058.08 15618.52 664.04 o -10 6 0 1428.11 1351.77 111.78 o -9 6 0 26806.59 27593.40 1437.46 o -8 6 0 1020.76 765.27 119.06 o -7 6 0 1469.85 1264.07 71.77 o -6 6 0 1634.63 1683.84 84.54 o -5 6 0 779.81 692.20 60.70 o -4 6 0 86.01 125.08 23.90 o -3 6 0 1053.53 1075.45 39.86 o -2 6 0 36068.75 36136.95 719.05 o -1 6 0 24198.57 24088.38 479.46 o 0 6 0 21475.83 21556.26 428.73 o 1 6 0 13276.18 13070.65 313.81 o 2 6 0 22555.11 22823.25 398.66 o 3 6 0 1506.72 1180.70 167.87 o 4 6 0 6675.84 6751.29 147.07 o 5 6 0 2129.48 2202.62 55.36 o 6 6 0 31431.70 31126.03 627.51 o 7 6 0 177.51 172.53 31.49 o 8 6 0 30005.27 29942.20 912.65 o 9 6 0 421.82 397.78 43.91 o 10 6 0 9152.69 8339.94 435.07 o 11 6 0 934.49 796.54 102.56 o 12 6 0 2159.47 2230.05 179.67 o 13 6 0 1710.40 1528.21 174.16 o 14 6 0 522.43 422.57 144.66 o -14 7 0 7425.62 7223.46 444.95 o -13 7 0 825.24 660.26 90.70 o -12 7 0 4482.04 5490.94 476.32 o -11 7 0 607.50 531.73 78.57 o -10 7 0 1470.01 1470.35 109.23 o -9 7 0 322.19 223.45 73.36 o -8 7 0 8015.03 7787.36 565.62 o -7 7 0 3420.16 3548.19 149.84 o -6 7 0 41173.04 40266.68 1068.03 o -5 7 0 2806.36 2918.00 89.01 o -4 7 0 9120.54 8727.55 264.52 o -3 7 0 96.98 97.88 22.60 o -2 7 0 136.57 274.32 29.95 o -1 7 0 103.50 183.87 21.00 o 0 7 0 3677.35 3833.53 97.81 o 1 7 0 8433.29 8115.60 238.44 o 2 7 0 4803.84 4471.56 108.01 o 3 7 0 73740.29 72201.80 2662.75 o 4 7 0 10215.45 10226.86 355.18 o 5 7 0 14942.93 15567.64 346.50 o 6 7 0 2864.70 2941.32 88.62 o 7 7 0 5516.58 5427.55 160.07 o 8 7 0 394.15 387.76 58.55 o 9 7 0 9379.71 9329.03 552.65 o 10 7 0 2695.21 2694.23 157.88 o 11 7 0 7698.80 7480.16 518.71 o 12 7 0 496.87 442.79 94.62 o 13 7 0 9570.54 9065.82 757.62 o -14 8 0 205.01 95.94 114.55 o -13 8 0 1955.08 2076.75 159.33 o -12 8 0 353.40 436.76 104.18 o -11 8 0 13833.08 14618.23 583.59 o -10 8 0 67.62 5.63 67.99 o -9 8 0 22866.70 23859.79 867.29 o -8 8 0 848.44 973.65 88.76 o -7 8 0 3581.06 3636.29 209.58 o -6 8 0 1392.25 1293.59 115.86 o -5 8 0 9201.32 9024.76 238.38 o -4 8 0 716.86 815.42 60.06 o -3 8 0 32122.18 31420.98 717.06 o -2 8 0 28507.02 28356.16 533.18 o -1 8 0 40142.39 39163.98 776.76 o 0 8 0 29765.54 29781.38 621.64 o 1 8 0 3383.46 3390.91 124.55 o 2 8 0 2276.23 2379.22 63.87 o 3 8 0 1715.56 1856.14 98.93 o 4 8 0 1635.06 1966.82 87.74 o 5 8 0 1054.49 1250.82 70.26 o 6 8 0 12779.26 13828.46 500.85 o 7 8 0 1069.24 1049.70 78.73 o 8 8 0 33116.80 33672.32 1028.45 o 9 8 0 1845.78 1828.88 194.98 o 10 8 0 6033.17 5368.50 384.33 o 11 8 0 171.01 215.14 59.85 o 12 8 0 163.30 318.90 104.85 o 13 8 0 118.50 269.44 690.14 o -14 9 0 1296.59 1046.99 180.06 o -13 9 0 1809.53 1388.87 142.44 o -12 9 0 2106.45 2149.27 148.11 o -11 9 0 492.72 388.36 85.18 o -10 9 0 712.58 1096.38 133.07 o -9 9 0 327.04 386.43 89.47 o -8 9 0 9427.88 8604.69 347.07 o -7 9 0 35.31 10.51 45.51 o -6 9 0 29830.50 29047.00 818.20 o -5 9 0 2821.49 2757.48 105.41 o -4 9 0 18290.31 17810.49 539.35 o -3 9 0 2587.04 2546.55 95.26 o -2 9 0 3530.80 3604.68 109.78 o -1 9 0 310.25 423.56 30.05 o 0 9 0 26275.73 27231.44 526.01 o 1 9 0 16542.05 16885.45 455.90 o 2 9 0 11034.29 11521.20 283.79 o 3 9 0 15787.03 16675.37 521.95 o 4 9 0 9127.80 9712.68 384.83 o 5 9 0 18845.98 18894.51 761.96 o 6 9 0 1235.30 1266.31 90.21 o 7 9 0 5599.88 5789.48 257.90 o 8 9 0 1698.06 1525.84 156.49 o 9 9 0 11530.52 10988.17 585.65 o 10 9 0 42.31 -23.96 180.90 o 11 9 0 5353.71 5348.95 514.12 o 12 9 0 777.34 510.42 224.60 o -13 10 0 2680.44 2300.19 206.43 o -12 10 0 2892.99 3126.82 310.91 o -11 10 0 15257.36 16146.25 835.32 o -10 10 0 1195.11 1386.13 117.98 o -9 10 0 6396.77 7002.31 605.12 o -8 10 0 265.46 413.77 72.87 o -7 10 0 54.78 49.36 31.83 o -6 10 0 29.75 91.89 37.70 o -5 10 0 130.31 99.50 34.02 o -4 10 0 3251.23 3061.47 218.78 o -3 10 0 28535.18 29582.29 898.45 o -2 10 0 12200.07 12387.72 360.44 o -1 10 0 50834.17 51133.16 1363.02 o 0 10 0 1526.02 1479.04 55.99 o 1 10 0 4562.73 4468.20 141.12 o 2 10 0 7001.63 7507.62 275.20 o 3 10 0 1637.57 1735.99 92.05 o 4 10 0 79.62 128.43 40.65 o 5 10 0 4869.27 5516.16 280.94 o 6 10 0 39776.57 40896.86 1744.80 o 7 10 0 437.17 478.16 60.03 o 8 10 0 10896.30 10856.02 695.95 o 9 10 0 108.37 165.16 101.72 o 10 10 0 3594.49 3267.99 283.66 o 11 10 0 276.08 270.93 118.23 o 12 10 0 84.57 87.80 189.20 o -12 11 0 856.02 614.35 222.60 o -11 11 0 400.72 327.39 103.07 o -10 11 0 4486.72 4607.05 261.86 o -9 11 0 216.72 5.00 170.41 o -8 11 0 7208.65 7781.49 350.14 o -7 11 0 50.39 56.75 50.36 o -6 11 0 22012.87 23285.37 765.59 o -5 11 0 826.71 811.93 75.86 o -4 11 0 15970.34 15852.33 616.22 o -3 11 0 708.53 708.20 56.45 o -2 11 0 3812.60 3775.88 158.49 o -1 11 0 3661.28 3679.31 143.95 o 0 11 0 517.18 510.91 52.35 o 1 11 0 9318.16 9448.23 255.75 o 2 11 0 8170.98 9278.11 318.74 o 3 11 0 13168.06 13541.85 423.54 o 4 11 0 15338.16 15902.10 552.09 o 5 11 0 5733.88 5308.78 276.60 o 6 11 0 406.04 443.58 58.70 o 7 11 0 4.96 -64.62 43.08 o 8 11 0 166.61 116.50 63.64 o 9 11 0 1383.11 1282.98 224.60 o 10 11 0 16.44 -9.51 92.83 o 11 11 0 12358.20 12257.30 956.15 o -12 12 0 4340.36 4067.30 371.47 o -11 12 0 7579.90 7842.21 447.70 o -10 12 0 787.26 755.48 103.92 o -9 12 0 8007.52 8821.05 417.92 o -8 12 0 1943.36 1970.41 149.08 o -7 12 0 1114.84 1206.48 117.21 o -6 12 0 159.42 176.55 79.92 o -5 12 0 5770.74 5458.25 219.10 o -4 12 0 38.61 81.62 41.83 o -3 12 0 14026.81 14895.94 502.99 o -2 12 0 368.94 403.50 45.69 o -1 12 0 3539.15 3640.22 183.84 o 0 12 0 2146.70 2120.27 105.33 o 1 12 0 8756.16 8428.91 349.41 o 2 12 0 197.07 247.94 79.95 o 3 12 0 389.33 403.15 67.46 o 4 12 0 6920.81 6679.00 290.21 o 5 12 0 5403.93 5650.02 240.25 o 6 12 0 5270.56 5626.29 277.57 o 7 12 0 3166.79 3235.53 168.22 o 8 12 0 6201.24 6146.47 417.02 o 9 12 0 818.08 898.04 138.45 o 10 12 0 9665.27 9259.74 814.50 o -11 13 0 14.28 2.64 116.77 o -10 13 0 640.39 498.83 119.03 o -9 13 0 159.27 156.71 68.64 o -8 13 0 11229.47 10311.92 601.56 o -7 13 0 4143.23 3980.27 266.83 o -6 13 0 13385.30 14102.39 589.24 o -5 13 0 18.75 -91.50 150.00 o -4 13 0 650.76 789.79 147.34 o -3 13 0 1227.41 1212.44 194.01 o -2 13 0 19.01 61.56 55.97 o -1 13 0 91.14 51.91 70.69 o 0 13 0 6644.95 6708.33 413.47 o 1 13 0 4831.21 4640.72 208.05 o 2 13 0 15802.29 16354.97 728.79 o 3 13 0 1421.47 1370.54 96.09 o 4 13 0 3161.01 3638.36 179.57 o 5 13 0 6612.43 6582.41 322.56 o 6 13 0 572.63 584.63 68.48 o 7 13 0 76.31 -5.44 103.58 o 8 13 0 164.12 221.67 78.72 o 9 13 0 4322.36 3755.09 354.19 o -10 14 0 3075.22 2533.58 224.20 o -9 14 0 4090.18 3742.39 386.81 o -8 14 0 1080.45 1020.67 157.85 o -7 14 0 217.73 269.18 89.44 o -6 14 0 581.12 419.47 126.57 o -5 14 0 820.69 692.71 216.71 o -4 14 0 164.89 598.06 172.67 o -3 14 0 14312.64 14340.89 769.41 o -2 14 0 79.12 11.25 67.19 o -1 14 0 12447.67 12200.69 651.06 o 0 14 0 136.41 160.82 60.53 o 1 14 0 990.78 886.28 70.83 o 2 14 0 1207.88 1528.51 152.45 o 3 14 0 5043.68 5821.81 390.23 o 4 14 0 781.45 749.97 84.00 o 5 14 0 2021.17 2195.93 135.23 o 6 14 0 8863.84 8866.08 466.51 o 7 14 0 8651.80 8490.95 606.18 o 8 14 0 2870.83 2118.93 345.79 o -8 15 0 4518.95 4562.10 366.03 o -7 15 0 261.08 208.42 108.10 o -6 15 0 2593.62 2123.46 220.69 o -5 15 0 2569.57 2104.80 213.40 o -4 15 0 2175.42 2205.81 182.95 o -3 15 0 420.92 396.04 117.71 o -2 15 0 924.70 696.98 95.46 o -1 15 0 631.20 487.65 118.53 o 0 15 0 11158.95 12361.63 827.66 o 1 15 0 677.64 559.68 194.48 o 2 15 0 19239.61 19904.11 936.62 o 3 15 0 955.77 760.91 87.51 o 4 15 0 1380.07 1515.56 177.53 o 5 15 0 2013.83 1971.71 170.82 o 6 15 0 1742.19 1560.23 215.44 o -7 16 0 399.48 454.94 157.29 o -6 16 0 796.96 723.20 293.27 o -5 16 0 3189.32 2900.01 238.32 o -4 16 0 1415.73 1249.19 474.40 o -3 16 0 12743.50 13368.52 835.66 o -2 16 0 450.01 322.48 88.37 o -1 16 0 4523.02 3872.46 398.47 o 0 16 0 33.31 30.29 203.22 o 1 16 0 1829.65 1543.38 172.38 o 2 16 0 0.20 8.17 87.54 o 3 16 0 2333.28 2151.16 217.20 o 4 16 0 838.17 702.39 122.74 o -4 17 0 559.26 371.84 152.28 o -3 17 0 438.68 -427.12 910.72 o -2 17 0 2046.76 2086.18 419.35 o -1 17 0 64.26 -28.87 159.16 o 0 17 0 3594.54 2528.75 272.83 o 1 17 0 12.43 134.31 106.83 o -2 -17 1 2.76 62.82 120.42 o -1 -17 1 3037.52 2527.02 209.19 o 0 -17 1 10.39 38.25 143.26 o 1 -17 1 9153.60 9834.60 776.71 o 2 -17 1 125.55 -101.80 123.52 o 3 -17 1 111.78 135.18 100.78 o 4 -17 1 233.11 84.53 126.23 o -5 -16 1 1994.86 2169.94 232.05 o -4 -16 1 5837.66 5150.37 405.92 o -3 -16 1 311.15 159.73 105.56 o -2 -16 1 69.23 -45.73 115.13 o -1 -16 1 35.51 92.13 74.16 o 0 -16 1 730.87 692.99 146.73 o 1 -16 1 2100.42 2533.62 294.13 o 2 -16 1 19899.51 21298.49 944.01 o 3 -16 1 380.81 359.75 92.13 o 4 -16 1 5439.33 4893.25 418.88 o 5 -16 1 1187.25 1256.66 135.13 o 6 -16 1 1718.34 1487.97 346.86 o 7 -16 1 518.82 815.20 256.30 o -6 -15 1 72.45 25.37 150.31 o -5 -15 1 401.46 542.88 145.03 o -4 -15 1 796.89 593.00 72.54 o -3 -15 1 8651.05 8544.12 490.16 o -2 -15 1 58.32 223.39 96.59 o -1 -15 1 16948.34 16857.08 944.93 o 0 -15 1 19.20 22.26 53.16 o 1 -15 1 12763.96 12587.60 501.07 o 2 -15 1 8.22 -66.07 44.05 o 3 -15 1 177.65 267.80 77.40 o 4 -15 1 577.62 562.93 188.60 o 5 -15 1 147.98 185.84 96.66 o 6 -15 1 962.75 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