# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_2008src0880 _shelx_title ' 2008src0880 in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 652.88 _exptl_crystal_F_000 2536.00 _reflns_d_resolution_high 0.7700 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 12.7644 _cell_length_b 11.9584 _cell_length_c 29.2566 _cell_angle_alpha 90.000 _cell_angle_beta 98.801 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 45585.39 42276.12 1856.33 o 3 0 0 2280.55 2136.59 181.45 o 4 0 0 204235.06 198234.73 8197.19 o 5 0 0 6108.37 5692.61 183.87 o 6 0 0 118191.42 110693.67 3148.90 o 7 0 0 757.22 741.81 128.24 o 8 0 0 232424.81 229977.53 5876.12 o 9 0 0 884.41 1018.89 137.34 o 10 0 0 111180.88 109282.31 3408.84 o 11 0 0 1116.49 1215.69 168.52 o 12 0 0 74517.50 74521.12 2430.88 o 13 0 0 269.75 528.67 313.71 o 14 0 0 59141.42 64636.59 2721.10 o 15 0 0 2661.74 3282.41 566.50 o 16 0 0 17388.44 15618.45 1068.70 o 2 1 0 88.45 26.45 21.33 o 3 1 0 36450.75 38535.04 631.90 o 4 1 0 5160.89 5482.30 117.56 o 5 1 0 416.22 744.18 70.40 o 6 1 0 1520.44 1646.53 97.14 o 7 1 0 4280.56 4314.58 135.93 o 8 1 0 1005.83 1234.80 91.58 o 9 1 0 28456.09 28617.94 629.43 o 10 1 0 84.98 182.37 91.91 o 11 1 0 480.04 530.85 112.62 o 12 1 0 43.66 259.44 114.22 o 13 1 0 2449.92 2428.66 276.25 o 14 1 0 1522.88 1863.87 319.48 o 15 1 0 1127.09 950.70 172.78 o 16 1 0 323.02 385.53 358.46 o 0 2 0 54670.96 51535.57 1399.53 o 1 2 0 32442.70 31100.11 591.39 o 2 2 0 205299.86 197091.84 3516.58 o 3 2 0 45718.33 46192.13 708.49 o 4 2 0 92082.63 91471.27 1383.78 o 5 2 0 91445.02 95683.59 1738.74 o 6 2 0 44264.59 43216.13 960.56 o 7 2 0 15749.50 14871.37 390.15 o 8 2 0 39578.56 37863.60 1382.39 o 9 2 0 20243.99 21037.91 534.15 o 10 2 0 57370.48 58438.62 1506.11 o 11 2 0 16227.38 16054.33 532.99 o 12 2 0 19866.45 20731.52 773.82 o 13 2 0 14808.59 15058.85 630.62 o 14 2 0 11094.63 11190.15 835.00 o 15 2 0 10595.01 12143.19 546.04 o 16 2 0 7699.58 7294.83 594.05 o 1 3 0 71948.15 72841.41 924.95 o 2 3 0 379.60 472.61 27.90 o 3 3 0 588.64 686.91 38.34 o 4 3 0 1444.30 1906.03 96.88 o 5 3 0 86.01 187.41 54.22 o 6 3 0 760.20 1034.74 69.91 o 7 3 0 2806.96 2986.55 199.27 o 8 3 0 948.73 1093.46 169.65 o 9 3 0 2.87 8.39 90.03 o 10 3 0 2900.92 2969.92 223.00 o 11 3 0 6.59 161.72 131.15 o 12 3 0 3465.31 3724.13 228.96 o 13 3 0 162.71 494.02 213.09 o 14 3 0 2099.96 2171.81 397.28 o 15 3 0 1018.17 1218.80 187.61 o 16 3 0 915.48 960.38 247.81 o 0 4 0 3151.84 3127.03 99.59 o 1 4 0 315445.28 305322.41 3785.94 o 2 4 0 12889.14 13310.43 274.29 o 3 4 0 388358.19 371085.06 6372.27 o 4 4 0 989.33 965.86 49.48 o 5 4 0 163262.80 156023.53 3155.34 o 6 4 0 3807.28 4068.75 129.90 o 7 4 0 100794.09 101014.34 2816.59 o 8 4 0 338.19 285.81 76.92 o 9 4 0 95155.35 95759.56 2535.31 o 10 4 0 3818.93 4217.09 284.29 o 11 4 0 102377.49 101471.92 3062.52 o 12 4 0 3700.98 4253.68 294.22 o 13 4 0 39166.49 40509.78 1297.07 o 14 4 0 1671.33 1643.16 210.29 o 15 4 0 23689.90 25359.21 1246.74 o 1 5 0 127.07 96.61 36.65 o 2 5 0 10802.06 11508.74 199.50 o 3 5 0 4446.66 4559.13 123.26 o 4 5 0 177.46 392.28 58.20 o 5 5 0 552.38 537.25 76.06 o 6 5 0 381.52 358.13 67.52 o 7 5 0 2046.09 2097.96 153.14 o 8 5 0 8923.29 9088.37 371.58 o 9 5 0 246.34 51.73 166.96 o 10 5 0 3611.32 3573.27 367.47 o 11 5 0 226.29 594.75 267.28 o 12 5 0 4938.21 4461.51 278.46 o 13 5 0 1886.21 1959.18 211.48 o 14 5 0 2837.08 2609.08 243.49 o 15 5 0 408.65 223.63 163.58 o 0 6 0 11725.05 12160.70 269.91 o 1 6 0 150207.16 152165.75 2163.37 o 2 6 0 19485.46 18683.58 351.42 o 3 6 0 46153.22 43509.76 945.04 o 4 6 0 10117.59 11032.51 352.20 o 5 6 0 53295.96 54938.38 1257.57 o 6 6 0 23749.00 24687.28 611.86 o 7 6 0 50749.00 50630.87 1215.14 o 8 6 0 9302.67 9607.78 323.37 o 9 6 0 46913.28 45931.57 1958.07 o 10 6 0 17540.23 17839.63 731.04 o 11 6 0 23292.59 22181.47 1060.32 o 12 6 0 8079.81 6911.09 1167.67 o 13 6 0 24542.31 26923.48 1020.31 o 14 6 0 4948.68 4885.35 525.07 o 15 6 0 7396.19 7380.84 411.73 o 1 7 0 1804.54 2091.33 81.83 o 2 7 0 1448.16 1468.58 89.85 o 3 7 0 1808.07 1676.98 87.03 o 4 7 0 4590.37 5026.72 185.23 o 5 7 0 1801.95 1658.23 114.84 o 6 7 0 1248.89 1488.97 93.63 o 7 7 0 921.19 715.01 126.48 o 8 7 0 34.92 261.52 104.55 o 9 7 0 3526.81 3569.08 190.36 o 10 7 0 4577.32 4530.75 250.08 o 11 7 0 266.03 372.84 101.30 o 12 7 0 2360.04 2480.20 261.39 o 13 7 0 520.77 708.69 222.01 o 14 7 0 168.51 180.00 159.35 o 0 8 0 267734.97 266527.09 5815.68 o 1 8 0 109.60 173.99 66.05 o 2 8 0 90138.99 88561.64 2323.97 o 3 8 0 659.17 911.70 85.38 o 4 8 0 95583.05 95675.22 1972.05 o 5 8 0 1070.02 1044.92 77.17 o 6 8 0 69153.50 69983.22 1613.95 o 7 8 0 136.47 135.83 111.51 o 8 8 0 82819.09 81703.72 2032.77 o 9 8 0 2.31 -67.77 130.94 o 10 8 0 31672.99 33037.13 1446.58 o 11 8 0 1322.64 1028.71 168.13 o 12 8 0 38519.82 37968.61 3571.69 o 13 8 0 270.07 326.33 214.51 o 14 8 0 27662.84 28373.35 1666.78 o 1 9 0 5402.04 5742.16 397.36 o 2 9 0 4774.18 4589.55 210.58 o 3 9 0 884.91 1180.85 121.85 o 4 9 0 711.60 721.57 97.44 o 5 9 0 1832.60 2010.61 172.98 o 6 9 0 86.96 208.69 84.01 o 7 9 0 916.67 1064.41 144.53 o 8 9 0 926.47 787.99 264.15 o 9 9 0 4868.39 5153.61 235.89 o 10 9 0 366.77 467.10 147.72 o 11 9 0 3225.13 2630.13 308.76 o 12 9 0 172.51 349.56 192.14 o 0 10 0 18468.21 18653.60 971.55 o 1 10 0 6779.17 6239.66 678.83 o 2 10 0 78675.74 84784.30 3291.37 o 3 10 0 6388.05 5634.98 863.76 o 4 10 0 47730.36 46497.35 2103.31 o 5 10 0 259.32 198.48 155.17 o 6 10 0 36250.78 36611.13 1033.13 o 7 10 0 4857.40 5651.95 266.41 o 8 10 0 23726.10 23586.53 837.79 o 9 10 0 2499.08 2062.91 203.81 o 10 10 0 27258.55 26525.85 2321.25 o 11 10 0 5716.68 5700.08 694.24 o 1 11 0 7217.69 6430.22 747.39 o 2 11 0 141.05 344.88 183.95 o 3 11 0 362.29 261.50 391.65 o 4 11 0 664.50 410.03 293.77 o 5 11 0 2555.07 2494.52 256.37 o 6 11 0 2246.89 2677.35 257.45 o 7 11 0 861.70 696.61 177.33 o 8 11 0 31.33 96.07 227.99 o 9 11 0 1121.16 1325.00 334.38 o 10 11 0 577.20 319.11 189.17 o 0 12 0 6064.52 5550.43 441.62 o 1 12 0 50640.35 53930.82 3535.79 o 2 12 0 2554.84 1671.51 532.29 o 3 12 0 40769.29 42147.23 2020.91 o 4 12 0 561.17 611.57 217.39 o 5 12 0 34128.15 33781.92 2429.78 o 6 12 0 80.86 169.38 222.71 o 7 12 0 17709.01 17539.27 768.81 o 8 12 0 0.51 -30.13 153.39 o 9 12 0 31622.63 26519.98 2252.95 o 1 13 0 1078.15 860.80 273.67 o 3 13 0 61.07 89.31 243.14 o 4 13 0 38.69 111.33 275.41 o 5 13 0 1173.57 1057.89 265.81 o 6 13 0 1591.70 141.48 713.33 o 7 13 0 160.20 -147.81 201.54 o 8 13 0 1742.26 1844.10 269.86 o 2 14 0 184.60 627.59 281.90 o 3 14 0 14350.46 14598.65 1416.55 o 4 14 0 29.96 -9.06 210.00 o 5 14 0 18082.65 16257.00 1658.83 o 6 14 0 521.67 929.71 291.67 o 1 15 0 1.34 -152.67 287.01 o 2 15 0 506.83 830.04 503.85 o 3 15 0 21.33 -136.83 452.89 o 4 15 0 5.67 294.66 292.55 o -16 1 1 1484.42 1871.62 299.67 o -15 1 1 96.57 235.25 187.53 o -14 1 1 9.89 -315.15 210.10 o -13 1 1 1804.32 2009.51 193.27 o -12 1 1 15041.85 13556.81 1034.26 o -11 1 1 480.54 509.78 151.09 o -10 1 1 1191.95 1446.33 168.58 o -9 1 1 3589.94 3816.01 139.65 o -8 1 1 2986.94 3213.26 230.60 o -7 1 1 1989.52 1852.86 125.30 o -6 1 1 76.65 255.45 57.36 o -5 1 1 5374.07 5468.92 173.08 o -4 1 1 1185.07 1111.71 56.95 o -3 1 1 23748.08 24318.77 386.06 o -2 1 1 162.60 226.87 18.23 o 2 1 1 9854.27 9849.97 218.53 o 3 1 1 23924.84 23880.88 401.44 o 4 1 1 1751.50 1825.35 52.28 o 5 1 1 2313.09 2505.20 89.84 o 6 1 1 5733.88 6118.04 189.35 o 7 1 1 16817.77 15790.51 332.28 o 8 1 1 12387.26 11515.87 274.02 o 9 1 1 17929.41 19046.54 414.48 o 10 1 1 5906.44 6095.72 262.35 o 11 1 1 17544.49 17100.20 493.26 o 12 1 1 4461.70 5185.95 300.26 o 13 1 1 5272.80 5593.22 354.31 o 14 1 1 2849.34 3108.05 269.64 o 15 1 1 5423.02 6023.57 333.12 o 16 1 1 4131.29 3279.70 875.98 o -16 2 1 6227.63 6505.61 763.59 o -15 2 1 10961.24 11199.68 414.37 o -14 2 1 11992.35 12107.77 697.71 o -13 2 1 23574.37 24267.49 815.64 o -12 2 1 6134.45 6283.87 271.93 o -11 2 1 18537.92 19604.59 682.34 o -10 2 1 42031.86 41199.46 1192.09 o -9 2 1 45063.39 46625.59 1037.79 o -8 2 1 32441.90 31642.13 738.21 o -7 2 1 22221.12 20493.20 455.38 o -6 2 1 37022.11 37659.17 793.11 o -5 2 1 153273.69 157600.89 2547.27 o -4 2 1 67050.45 67089.33 981.83 o -3 2 1 21292.06 21145.19 331.47 o -2 2 1 60009.96 58909.45 858.32 o -1 2 1 18898.51 18595.25 305.54 o 0 2 1 18731.45 18508.93 313.34 o 1 2 1 76765.17 72295.27 2057.35 o 2 2 1 69904.73 69274.11 1151.08 o 3 2 1 53709.19 52684.27 797.71 o 4 2 1 28628.10 28462.12 500.31 o 5 2 1 33930.24 34295.73 655.03 o 6 2 1 21476.44 21358.72 518.81 o 7 2 1 10927.46 10812.43 273.33 o 8 2 1 1569.05 1764.14 105.22 o 9 2 1 21928.05 22051.43 513.07 o 10 2 1 1985.79 2309.12 315.07 o 11 2 1 6414.38 7113.77 288.56 o 12 2 1 16220.49 16879.51 480.23 o 13 2 1 3387.32 3560.61 319.19 o 14 2 1 2574.76 2643.55 393.81 o 15 2 1 7734.55 7364.04 389.47 o 16 2 1 512.28 604.07 196.18 o -16 3 1 9.33 -43.35 168.98 o -15 3 1 770.03 770.60 218.09 o -14 3 1 81.33 5.81 198.64 o -13 3 1 44.37 176.11 149.10 o -12 3 1 16.50 17.57 124.22 o -11 3 1 4319.47 5200.19 477.26 o -10 3 1 2465.67 2180.73 190.48 o -9 3 1 18782.87 19228.68 486.27 o -8 3 1 61.79 200.41 63.51 o -7 3 1 527.96 848.94 68.51 o -6 3 1 4062.78 4157.67 162.91 o -5 3 1 10096.90 9774.25 231.33 o -4 3 1 8724.95 8420.11 154.23 o -3 3 1 2034.33 2124.52 76.85 o -2 3 1 2875.78 3029.55 75.68 o -1 3 1 91917.17 90786.30 1255.97 o 0 3 1 2790.90 2745.26 58.90 o 1 3 1 3770.30 3860.50 75.90 o 2 3 1 184.47 182.30 45.62 o 3 3 1 30333.43 30918.87 486.74 o 4 3 1 58961.43 58141.46 884.83 o 5 3 1 59421.76 60430.82 983.05 o 6 3 1 191.72 361.27 84.39 o 7 3 1 10043.93 10316.59 392.99 o 8 3 1 17165.33 17950.47 457.36 o 9 3 1 15218.22 14448.99 447.80 o 10 3 1 14308.18 13577.93 414.63 o 11 3 1 13770.53 15095.75 659.53 o 12 3 1 15695.46 15688.42 524.97 o 13 3 1 11276.25 12402.64 416.86 o 14 3 1 761.02 830.24 231.18 o 15 3 1 4574.03 5161.86 692.07 o 16 3 1 1289.09 1333.45 272.25 o -15 4 1 487.17 508.55 320.40 o -14 4 1 56.42 139.72 129.98 o -13 4 1 812.78 835.42 198.99 o -12 4 1 3.41 248.06 162.14 o -11 4 1 6781.44 6923.12 376.42 o -10 4 1 1339.30 1243.93 250.90 o -9 4 1 4934.89 4870.72 323.96 o -8 4 1 1394.21 1714.25 121.47 o -7 4 1 6620.23 7275.59 206.13 o -6 4 1 51.52 259.24 56.56 o -5 4 1 7637.43 7070.48 179.90 o -4 4 1 221.68 456.69 65.92 o -3 4 1 227.74 295.55 36.90 o -2 4 1 38.95 61.20 27.35 o -1 4 1 7166.37 7129.13 111.35 o 0 4 1 1492.29 1754.78 44.25 o 1 4 1 4356.64 4879.02 86.23 o 2 4 1 7654.51 7718.53 172.37 o 3 4 1 38331.39 38280.24 557.54 o 4 4 1 644.69 632.78 44.62 o 5 4 1 2236.47 2125.46 105.23 o 6 4 1 889.07 1142.60 71.27 o 7 4 1 530.76 617.05 100.48 o 8 4 1 0.53 -118.29 144.24 o 9 4 1 143.79 205.12 86.00 o 10 4 1 4.52 94.71 161.73 o 11 4 1 6015.55 6222.73 282.53 o 12 4 1 101.43 62.02 185.19 o 13 4 1 1150.57 1233.72 149.18 o 14 4 1 4.29 -35.77 159.58 o 15 4 1 959.15 1504.87 343.57 o -15 5 1 307.02 244.51 191.90 o -14 5 1 1581.93 1971.60 314.64 o -13 5 1 1771.00 2082.30 254.32 o -12 5 1 482.45 662.92 277.07 o -11 5 1 697.22 653.17 235.81 o -10 5 1 4439.91 5163.43 297.69 o -9 5 1 4555.53 4943.39 315.60 o -8 5 1 2368.46 2288.23 112.10 o -7 5 1 196.08 284.13 64.91 o -6 5 1 17579.57 17903.51 478.02 o -5 5 1 774.04 900.74 78.59 o -4 5 1 41388.60 41172.44 746.13 o -3 5 1 1243.42 1659.98 87.37 o -2 5 1 8536.71 8753.87 172.16 o -1 5 1 2416.73 2678.17 75.98 o 0 5 1 948.70 985.79 50.35 o 1 5 1 12563.53 13243.65 211.78 o 2 5 1 2615.38 2916.61 92.06 o 3 5 1 2092.98 2672.08 86.74 o 4 5 1 46743.63 46114.41 890.76 o 5 5 1 10414.85 10199.67 263.84 o 6 5 1 27201.67 28152.32 641.71 o 7 5 1 2356.46 2197.57 201.66 o 8 5 1 3275.65 3358.22 170.20 o 9 5 1 275.16 418.14 104.96 o 10 5 1 8929.93 8867.22 458.52 o 11 5 1 18.77 45.24 220.87 o 12 5 1 12315.38 12010.79 494.32 o 13 5 1 1116.32 2048.96 357.51 o 14 5 1 3283.36 3000.36 265.02 o 15 5 1 939.44 873.55 197.80 o -15 6 1 7095.43 6380.77 384.75 o -14 6 1 10878.98 10066.62 790.78 o -13 6 1 12370.02 12391.35 523.44 o -12 6 1 10962.89 11135.45 582.23 o -11 6 1 7538.88 8248.70 428.64 o -10 6 1 35236.30 34145.57 1312.35 o -9 6 1 4613.58 4547.90 257.69 o -8 6 1 14568.99 16320.72 455.78 o -7 6 1 14692.76 14538.99 398.37 o -6 6 1 53789.54 55643.63 1191.30 o -5 6 1 35494.04 35076.34 1176.17 o -4 6 1 34563.49 33172.46 742.66 o -3 6 1 14591.22 14493.87 391.22 o -2 6 1 120082.94 120364.58 1860.29 o -1 6 1 17153.13 16802.37 302.30 o 0 6 1 3850.61 3489.34 84.73 o 1 6 1 7460.55 7275.36 133.26 o 2 6 1 28099.43 27374.16 516.49 o 3 6 1 22583.62 22844.36 472.09 o 4 6 1 33811.79 33266.36 627.04 o 5 6 1 2709.17 3115.13 121.68 o 6 6 1 11167.56 10932.45 318.17 o 7 6 1 6478.74 7096.82 257.81 o 8 6 1 18264.75 18426.79 689.71 o 9 6 1 2726.60 2844.23 210.94 o 10 6 1 9957.77 11402.32 602.28 o 11 6 1 774.40 866.93 276.59 o 12 6 1 9148.40 7619.89 571.23 o 13 6 1 140.85 -140.44 154.19 o 14 6 1 1795.98 1737.40 441.32 o 15 6 1 1159.74 1600.63 216.76 o -14 7 1 2305.91 2109.69 391.80 o -13 7 1 1317.98 1243.23 202.55 o -12 7 1 3937.74 4121.23 427.52 o -11 7 1 1331.45 1438.20 166.62 o -10 7 1 2829.49 3204.59 291.29 o -9 7 1 66.68 70.53 199.10 o -8 7 1 14193.00 14247.77 502.39 o -7 7 1 73.14 117.80 66.92 o -6 7 1 22449.19 21987.44 511.72 o -5 7 1 6903.38 7118.98 346.15 o -4 7 1 19651.21 19930.37 464.21 o -3 7 1 34.18 -8.72 49.35 o -2 7 1 9617.14 9433.87 233.97 o -1 7 1 6042.74 6294.12 142.53 o 0 7 1 36770.13 37519.18 595.05 o 1 7 1 502.64 663.25 67.68 o 2 7 1 43043.73 42234.78 890.87 o 3 7 1 2879.86 2966.91 124.86 o 4 7 1 46894.40 48724.89 1225.43 o 5 7 1 4847.59 5440.04 178.31 o 6 7 1 18852.43 19120.29 441.18 o 7 7 1 10399.69 10749.83 356.06 o 8 7 1 28717.85 29222.88 918.26 o 9 7 1 5141.83 5129.75 251.56 o 10 7 1 22487.44 21532.45 795.03 o 11 7 1 1152.34 803.51 194.17 o 12 7 1 18595.32 20310.13 836.03 o 13 7 1 3453.11 2917.12 307.82 o 14 7 1 12528.42 10858.41 633.95 o -14 8 1 8876.41 7366.63 684.25 o -13 8 1 226.07 274.66 202.02 o -12 8 1 3441.19 3438.97 307.97 o -11 8 1 58.32 199.39 282.13 o -10 8 1 5986.87 6148.75 806.91 o -9 8 1 1417.38 1510.49 140.64 o -8 8 1 7118.98 6792.69 348.87 o -7 8 1 160.33 325.57 89.47 o -6 8 1 7013.67 7278.49 306.82 o -5 8 1 210.10 289.93 74.61 o -4 8 1 21574.53 21981.72 572.48 o -3 8 1 3745.62 3719.63 140.50 o -2 8 1 12993.49 12688.60 294.57 o -1 8 1 162.23 101.00 78.55 o 0 8 1 29768.20 29919.43 535.05 o 1 8 1 47.33 33.36 81.83 o 2 8 1 2782.37 2956.49 143.32 o 3 8 1 1186.82 1090.96 157.89 o 4 8 1 1010.49 1339.93 93.72 o 5 8 1 803.11 827.56 88.52 o 6 8 1 19334.27 19210.70 596.27 o 7 8 1 1606.30 1458.54 119.44 o 8 8 1 3026.53 2954.23 196.78 o 9 8 1 751.84 674.10 101.84 o 10 8 1 3571.45 3456.26 551.38 o 11 8 1 168.91 386.61 170.72 o 12 8 1 1035.55 967.58 199.60 o 13 8 1 227.33 290.95 160.35 o -13 9 1 2308.31 1455.27 292.88 o -12 9 1 38.04 394.32 198.98 o -11 9 1 2563.78 2883.68 300.70 o -10 9 1 631.52 578.14 159.74 o -9 9 1 6363.48 6746.36 460.82 o -8 9 1 940.49 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