# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_04skc0003p1 _shelx_title ' 04skc0003p1 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 191.23 _exptl_crystal_F_000 628.00 _reflns_d_resolution_high 0.7701 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.3454 _cell_length_b 9.3736 _cell_length_c 17.6236 _cell_angle_alpha 78.408 _cell_angle_beta 78.446 _cell_angle_gamma 89.855 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 285.13 264.30 18.27 o 7 0 0 63.31 79.70 23.90 o 10 0 0 10.76 22.05 36.08 o -10 1 0 34.83 19.65 33.28 o -9 1 0 47.37 60.10 25.12 o -8 1 0 27.21 85.01 66.56 o -7 1 0 143.32 167.16 24.46 o -6 1 0 53.89 67.88 21.59 o -5 1 0 291.10 301.51 20.02 o -1 1 0 111.05 103.36 6.75 o 1 1 0 31.31 25.30 8.84 o 3 1 0 2341.71 2087.52 107.52 o 5 1 0 332.55 298.94 24.89 o 6 1 0 104.62 78.43 16.80 o 7 1 0 1.50 171.88 65.74 o 8 1 0 265.61 262.98 54.29 o 9 1 0 18.35 43.69 28.57 o 10 1 0 4.21 33.67 51.31 o -9 2 0 0.99 -4.36 19.46 o -5 2 0 217.75 239.42 55.13 o -4 2 0 378.50 120.00 27.07 o -3 2 0 2600.25 2422.86 110.60 o -2 2 0 5.15 2.84 3.47 o 0 2 0 403.90 345.76 26.94 o 2 2 0 1571.38 1413.44 78.35 o 4 2 0 2247.25 2173.34 96.40 o 5 2 0 2.02 75.76 28.86 o 6 2 0 372.06 331.40 34.96 o 7 2 0 0.31 15.60 24.25 o 8 2 0 568.29 558.42 98.85 o 9 2 0 31.90 37.75 27.75 o 10 2 0 335.14 259.39 81.23 o -11 3 0 5.85 29.66 35.68 o -8 3 0 113.95 129.66 27.43 o -3 3 0 109.54 114.13 9.73 o -1 3 0 47.72 104.85 26.92 o 1 3 0 1929.44 1680.61 85.10 o 3 3 0 5.01 30.47 17.86 o 5 3 0 231.99 278.11 29.61 o 6 3 0 4.05 14.62 21.76 o 7 3 0 252.08 184.40 41.42 o 8 3 0 0.43 3.04 30.42 o 9 3 0 31.46 33.70 37.03 o 10 3 0 25.43 50.52 55.73 o 11 3 0 33.11 13.63 53.73 o -7 4 0 41.30 115.10 65.37 o -6 4 0 197.88 160.50 17.54 o -4 4 0 2.09 16.76 8.31 o -3 4 0 635.73 662.04 134.27 o -2 4 0 27.84 53.00 11.73 o -1 4 0 255.43 407.71 174.26 o 0 4 0 1143.00 2252.81 101.84 o 3 4 0 574.43 456.89 49.82 o 4 4 0 0.86 79.77 21.12 o 6 4 0 85.65 53.77 26.31 o 7 4 0 167.06 157.46 36.43 o 8 4 0 10.76 -10.05 34.48 o 9 4 0 37.03 31.87 36.21 o 10 4 0 87.34 105.91 64.59 o 11 4 0 1.40 -75.76 94.60 o -8 5 0 16.95 -3.15 9.13 o -7 5 0 8.92 28.86 44.50 o -6 5 0 441.32 396.58 31.48 o -5 5 0 122.60 122.61 17.49 o -3 5 0 154.91 163.34 15.05 o -2 5 0 398.65 399.74 24.10 o -1 5 0 285.23 302.58 25.27 o 0 5 0 182.46 235.12 23.84 o 2 5 0 90.30 108.27 26.92 o 3 5 0 424.91 350.56 49.43 o 5 5 0 112.52 130.86 32.40 o 7 5 0 148.88 200.08 48.99 o 8 5 0 3.77 -7.09 34.68 o 9 5 0 18.35 80.41 53.78 o 10 5 0 251.77 203.29 89.19 o -6 6 0 225.40 248.33 32.84 o -4 6 0 206.00 235.13 32.96 o -3 6 0 716.30 753.23 41.07 o -1 6 0 27.85 22.60 13.93 o 0 6 0 188.23 234.97 22.99 o 1 6 0 109.23 132.89 19.87 o 2 6 0 234.77 246.77 53.70 o 3 6 0 7.11 3.73 24.62 o 4 6 0 3.91 25.34 29.65 o 5 6 0 930.92 1076.97 206.31 o 6 6 0 100.98 131.07 49.41 o 7 6 0 25.83 25.29 38.89 o 8 6 0 15.45 35.40 41.66 o 9 6 0 66.55 170.07 86.64 o -8 7 0 26.69 14.84 8.82 o -7 7 0 0.94 6.92 15.28 o -5 7 0 149.71 150.58 22.60 o -4 7 0 282.80 281.86 24.16 o -2 7 0 399.62 436.04 31.15 o -1 7 0 261.20 289.06 28.28 o 0 7 0 6.00 -0.92 19.21 o 1 7 0 5.73 27.26 38.89 o 2 7 0 10.92 35.08 33.58 o 3 7 0 47.69 52.94 36.50 o 4 7 0 219.89 323.12 76.36 o 5 7 0 258.81 291.08 53.39 o 6 7 0 172.83 211.92 49.51 o 7 7 0 99.51 68.61 56.17 o 8 7 0 39.37 86.62 75.79 o 9 7 0 103.20 91.08 93.48 o -7 8 0 2.47 15.29 14.87 o -6 8 0 458.08 403.04 41.98 o -5 8 0 1.03 -2.68 17.16 o -4 8 0 486.49 538.25 38.16 o -3 8 0 59.59 114.02 20.26 o -2 8 0 1254.62 1267.53 73.29 o -1 8 0 222.06 256.53 25.63 o 0 8 0 92.49 111.80 27.94 o 3 8 0 0.06 7.72 43.49 o 4 8 0 21.07 62.91 49.72 o 5 8 0 30.09 24.06 45.71 o 6 8 0 3.94 15.63 68.15 o 7 8 0 143.73 73.05 81.88 o 8 8 0 2.72 -11.62 93.00 o -8 9 0 7.02 78.97 85.79 o -7 9 0 64.53 57.11 27.19 o -6 9 0 12.56 -7.37 27.26 o -5 9 0 122.16 125.25 29.70 o -4 9 0 162.44 153.80 27.94 o -3 9 0 0.66 35.28 64.14 o -2 9 0 4.68 3.14 24.37 o -1 9 0 90.81 92.38 27.15 o 0 9 0 334.52 342.00 44.99 o 1 9 0 249.43 220.65 48.79 o 2 9 0 112.98 113.16 39.52 o 3 9 0 98.74 162.91 75.44 o 4 9 0 3.27 8.82 60.13 o 5 9 0 1.33 -19.24 73.76 o 6 9 0 42.69 52.93 71.78 o 7 9 0 9.83 57.33 124.27 o -6 10 0 4.79 28.30 40.03 o -5 10 0 1.35 13.30 40.22 o -4 10 0 25.44 13.23 31.97 o -3 10 0 18.55 38.62 36.00 o -2 10 0 245.42 247.15 44.54 o -1 10 0 13.34 7.17 38.98 o 0 10 0 45.45 72.00 42.10 o 1 10 0 121.54 99.30 44.72 o 2 10 0 51.52 58.76 55.04 o 3 10 0 123.42 149.87 51.63 o 4 10 0 36.65 100.65 68.57 o 5 10 0 34.93 145.55 107.46 o -4 11 0 3.17 -17.88 42.85 o -3 11 0 60.70 82.65 46.02 o -2 11 0 24.15 49.74 40.96 o -1 11 0 0.14 29.16 64.94 o 0 11 0 30.57 19.60 40.76 o 1 11 0 13.52 -22.63 61.94 o 2 11 0 30.93 42.23 56.22 o 3 11 0 56.24 37.12 64.07 o 4 11 0 1.93 57.72 71.75 o -3 -11 1 6.65 2.48 65.87 o -2 -11 1 26.05 43.90 72.51 o -1 -11 1 23.06 -22.82 73.17 o 0 -11 1 41.30 84.04 66.08 o 1 -11 1 84.17 55.82 36.60 o 2 -11 1 120.62 182.37 64.56 o 3 -11 1 1.86 32.03 53.31 o 4 -11 1 7.16 22.48 43.56 o -5 -10 1 24.17 -1.60 81.79 o -4 -10 1 50.96 17.65 98.25 o -3 -10 1 40.62 74.19 83.81 o -2 -10 1 33.50 6.79 41.52 o -1 -10 1 0.43 34.01 44.59 o 0 -10 1 51.51 44.44 34.48 o 1 -10 1 0.71 10.58 32.55 o 2 -10 1 44.68 16.70 38.06 o 3 -10 1 148.75 207.91 43.07 o 4 -10 1 9.66 29.96 31.20 o 5 -10 1 385.36 337.24 98.76 o 6 -10 1 25.27 4.96 31.35 o -7 -9 1 20.47 168.79 144.33 o -6 -9 1 10.73 28.46 86.59 o -5 -9 1 6.26 -73.36 85.79 o -3 -9 1 76.51 89.06 79.03 o -2 -9 1 182.04 155.82 42.27 o -1 -9 1 123.74 127.61 39.07 o 0 -9 1 529.30 501.51 47.24 o 1 -9 1 132.59 130.50 33.19 o 2 -9 1 2.71 -6.45 25.32 o 3 -9 1 1.36 4.10 35.83 o 4 -9 1 122.26 135.69 61.12 o 5 -9 1 6.01 1.88 26.02 o 6 -9 1 30.56 12.04 30.99 o 7 -9 1 75.23 133.98 97.07 o 8 -9 1 19.25 88.20 72.17 o -8 -8 1 135.47 15.65 80.27 o -7 -8 1 101.22 29.69 73.02 o -6 -8 1 243.27 188.44 94.02 o -5 -8 1 10.14 -23.65 46.90 o -4 -8 1 434.83 502.91 140.34 o -3 -8 1 30.90 64.51 39.26 o -2 -8 1 20.97 -0.40 37.29 o -1 -8 1 235.86 303.91 46.82 o 0 -8 1 28.64 50.03 28.08 o 1 -8 1 87.50 64.81 24.14 o 2 -8 1 567.82 532.15 43.10 o 3 -8 1 199.25 183.71 26.41 o 4 -8 1 12.98 39.67 18.48 o 5 -8 1 0.02 23.28 17.20 o 6 -8 1 113.40 158.87 36.03 o 7 -8 1 0.01 12.67 21.39 o 8 -8 1 94.07 64.77 24.34 o -9 -7 1 83.77 64.18 83.84 o -8 -7 1 48.33 99.86 75.79 o -7 -7 1 1.01 -4.41 52.11 o -6 -7 1 1.98 28.72 42.25 o -5 -7 1 45.14 32.48 38.50 o -4 -7 1 63.03 41.78 47.37 o -3 -7 1 17.28 55.92 34.13 o -1 -7 1 69.14 58.74 27.12 o 0 -7 1 400.85 349.58 41.51 o 1 -7 1 20.41 31.84 22.24 o 2 -7 1 99.06 77.59 21.83 o 3 -7 1 436.84 525.38 37.99 o 4 -7 1 121.99 145.39 19.32 o 5 -7 1 266.87 313.65 38.27 o 6 -7 1 392.11 407.20 33.20 o 7 -7 1 109.68 104.05 24.86 o 8 -7 1 29.07 4.81 21.65 o -9 -6 1 555.64 470.55 170.41 o -8 -6 1 183.33 230.12 86.54 o -7 -6 1 0.02 3.53 34.31 o -6 -6 1 124.41 120.84 38.67 o -4 -6 1 112.36 101.51 27.52 o -3 -6 1 553.74 656.43 61.28 o -2 -6 1 202.46 171.84 27.74 o -1 -6 1 134.20 175.47 48.40 o 0 -6 1 50.29 53.79 17.21 o 1 -6 1 58.67 57.88 12.87 o 2 -6 1 50.84 68.62 16.16 o 3 -6 1 235.80 209.43 16.34 o 4 -6 1 121.59 84.29 14.31 o 5 -6 1 112.43 119.01 19.86 o 7 -6 1 0.01 20.42 13.93 o 8 -6 1 6.17 -3.48 14.03 o 9 -6 1 0.04 20.44 16.43 o -10 -5 1 15.95 -65.75 56.53 o -9 -5 1 17.87 52.79 42.01 o -8 -5 1 85.71 55.61 53.43 o -7 -5 1 11.33 0.36 35.38 o -5 -5 1 12.52 0.45 20.84 o -4 -5 1 361.66 405.39 45.65 o -2 -5 1 442.28 400.57 54.92 o 0 -5 1 1064.85 1288.64 64.74 o 1 -5 1 52.82 64.60 24.21 o 2 -5 1 894.45 994.65 58.92 o 3 -5 1 91.38 83.04 12.49 o 4 -5 1 379.91 381.86 22.25 o 5 -5 1 159.96 174.57 18.73 o 6 -5 1 222.00 185.71 19.49 o 7 -5 1 109.38 61.81 56.99 o 8 -5 1 1.62 -2.69 12.37 o -10 -4 1 53.84 64.17 52.14 o -9 -4 1 519.43 624.88 70.57 o -7 -4 1 48.50 79.72 31.06 o -6 -4 1 33.96 36.91 24.09 o -5 -4 1 415.96 383.46 71.37 o -4 -4 1 8.48 77.58 20.26 o -2 -4 1 564.30 657.99 63.23 o 0 -4 1 2913.47 4553.76 211.83 o 1 -4 1 6069.86 6421.70 257.84 o 2 -4 1 13.38 86.99 11.86 o 4 -4 1 128.28 114.24 22.20 o 5 -4 1 413.22 416.77 46.96 o 6 -4 1 3.78 103.83 55.32 o 7 -4 1 260.15 125.06 34.98 o 8 -4 1 1.08 15.49 11.40 o 10 -4 1 189.81 168.26 35.34 o -10 -3 1 72.74 0.80 79.42 o -9 -3 1 33.71 44.59 41.90 o -8 -3 1 96.20 170.89 34.77 o -7 -3 1 111.90 129.78 35.64 o -6 -3 1 415.36 440.36 38.24 o -3 -3 1 498.46 497.59 72.69 o 0 -3 1 1113.41 1283.91 78.83 o 2 -3 1 4509.59 3986.92 143.37 o 7 -3 1 45.96 36.29 15.10 o 8 -3 1 114.70 107.20 17.55 o 9 -3 1 161.65 187.08 34.64 o -10 -2 1 57.03 46.52 51.34 o -9 -2 1 12.20 34.71 34.14 o -8 -2 1 214.61 178.82 43.40 o -6 -2 1 76.77 146.09 26.64 o -2 -2 1 261.75 298.40 22.28 o -1 -2 1 3378.60 2908.96 147.71 o 0 -2 1 198.02 305.16 44.06 o 1 -2 1 21012.76 24964.85 870.14 o 2 -2 1 2521.80 2267.20 66.67 o 3 -2 1 964.99 1066.15 37.05 o 4 -2 1 84.77 158.22 39.35 o 5 -2 1 1.54 2.54 7.66 o 7 -2 1 282.29 286.23 25.62 o 8 -2 1 391.90 406.83 36.32 o 10 -2 1 0.20 -11.62 43.69 o -10 -1 1 0.11 10.02 56.52 o -9 -1 1 136.57 97.21 27.04 o -8 -1 1 254.21 167.69 38.63 o -7 -1 1 122.97 144.10 28.66 o -5 -1 1 633.36 529.72 36.30 o -3 -1 1 79.18 122.99 14.93 o -2 -1 1 5043.22 3739.10 215.22 o -1 -1 1 500.22 390.12 25.89 o 1 -1 1 1196.66 670.22 51.93 o 2 -1 1 215.68 217.13 15.53 o 3 -1 1 1219.59 1181.45 61.84 o 5 -1 1 14.03 38.00 8.94 o 6 -1 1 2.62 22.45 37.28 o 8 -1 1 263.85 287.68 49.06 o -10 0 1 4.44 37.68 66.54 o -8 0 1 161.75 174.49 27.40 o -7 0 1 185.43 243.70 33.76 o -6 0 1 79.05 66.97 17.46 o -4 0 1 6018.17 5823.66 344.03 o -3 0 1 1972.59 1521.10 69.24 o -2 0 1 574.92 415.03 23.84 o 2 0 1 1063.15 879.11 52.27 o 3 0 1 200.47 195.28 16.38 o 4 0 1 4319.26 5162.46 246.68 o 6 0 1 141.60 121.66 19.20 o 7 0 1 436.50 514.05 51.61 o 9 0 1 8.38 9.58 25.62 o 10 0 1 0.68 19.09 33.03 o -10 1 1 121.97 150.50 46.96 o -9 1 1 174.46 246.32 35.61 o -8 1 1 1.07 -5.16 16.59 o -7 1 1 28.81 26.10 11.68 o -5 1 1 1.00 9.21 7.15 o -1 1 1 888.65 655.21 35.59 o 2 1 1 328.28 266.80 20.68 o 5 1 1 7.37 10.02 11.34 o 6 1 1 128.34 141.38 32.13 o 8 1 1 8.17 54.03 34.88 o 10 1 1 124.18 119.69 46.64 o 11 1 1 9.04 -50.11 67.75 o -10 2 1 0.79 9.22 24.85 o -9 2 1 7.14 43.39 22.05 o -8 2 1 370.86 427.74 43.48 o -6 2 1 75.29 95.91 35.72 o -4 2 1 74.33 107.19 28.50 o -1 2 1 21.79 126.78 28.49 o 0 2 1 1081.06 956.20 40.67 o 1 2 1 528.54 352.08 21.87 o 2 2 1 920.30 715.41 69.78 o 7 2 1 71.06 34.41 27.04 o 8 2 1 1083.59 1081.70 100.49 o 9 2 1 0.84 33.16 38.70 o 10 2 1 34.87 24.61 43.77 o 11 2 1 4.16 39.29 78.97 o -10 3 1 197.05 167.47 38.96 o -9 3 1 39.78 36.29 12.64 o -8 3 1 3.27 95.41 65.34 o -6 3 1 240.17 257.69 15.07 o -5 3 1 38.23 41.98 6.70 o -4 3 1 263.03 238.95 12.17 o -3 3 1 200.39 230.96 15.41 o -2 3 1 1527.41 1353.75 82.46 o -1 3 1 1473.71 1223.25 54.07 o 0 3 1 288.79 240.49 20.63 o 1 3 1 1206.03 1018.55 55.18 o 2 3 1 602.03 500.45 33.42 o 3 3 1 760.34 657.15 44.42 o 5 3 1 162.30 160.76 34.16 o 6 3 1 197.94 189.57 27.62 o 7 3 1 537.49 585.96 93.62 o 8 3 1 18.48 8.29 22.64 o 9 3 1 9.45 -9.17 32.48 o 10 3 1 46.29 68.03 47.75 o 11 3 1 115.66 -10.03 65.81 o -8 4 1 48.38 32.11 12.16 o -6 4 1 133.56 135.27 13.93 o -4 4 1 61.74 54.87 9.51 o -3 4 1 105.28 209.71 12.63 o -2 4 1 31.51 48.63 8.85 o 0 4 1 3244.52 4177.14 169.47 o 4 4 1 4.51 37.86 20.85 o 5 4 1 541.94 445.43 75.35 o 6 4 1 153.49 162.50 29.28 o 8 4 1 164.53 129.25 36.76 o 9 4 1 73.30 85.57 49.62 o 10 4 1 8.47 90.20 91.80 o 11 4 1 8.48 15.23 102.63 o -5 5 1 298.39 249.51 34.95 o -3 5 1 334.31 298.35 33.34 o -2 5 1 0.04 5.33 8.31 o -1 5 1 3.29 -3.29 11.51 o 0 5 1 15.51 39.25 16.09 o 1 5 1 13.94 55.03 25.63 o 3 5 1 0.80 9.22 32.87 o 5 5 1 1.25 -15.96 29.09 o 6 5 1 728.35 792.40 81.32 o 7 5 1 47.27 3.39 23.70 o 8 5 1 6.70 33.95 32.46 o 9 5 1 0.31 71.04 46.50 o 10 5 1 1.43 25.25 63.74 o -6 6 1 480.22 493.77 92.30 o -5 6 1 366.97 297.12 56.01 o -4 6 1 234.33 237.25 17.63 o -3 6 1 992.84 948.46 161.80 o -1 6 1 173.62 119.65 15.56 o 0 6 1 84.12 105.05 21.56 o 2 6 1 288.45 284.12 32.79 o 3 6 1 345.12 373.00 71.30 o 4 6 1 7.10 30.07 23.81 o 6 6 1 203.09 122.84 67.30 o 7 6 1 0.70 8.21 37.81 o 8 6 1 43.62 86.47 55.72 o 9 6 1 71.98 6.82 81.03 o 10 6 1 5.06 -40.89 72.96 o -7 7 1 74.50 57.83 16.82 o -6 7 1 12.02 15.82 16.87 o -5 7 1 382.09 308.83 48.46 o -4 7 1 2.20 61.50 24.05 o -3 7 1 15.15 86.02 19.29 o -2 7 1 271.41 260.68 25.95 o 1 7 1 1374.90 1240.07 78.30 o 2 7 1 4.85 20.39 20.07 o 4 7 1 360.70 366.11 97.42 o 5 7 1 0.09 -13.81 39.23 o 6 7 1 136.29 109.77 52.19 o 7 7 1 67.55 85.04 61.77 o 8 7 1 8.84 -57.33 60.93 o 9 7 1 30.54 8.82 63.35 o -7 8 1 1.35 -12.10 9.39 o -6 8 1 27.01 20.67 14.33 o -5 8 1 23.84 27.58 22.13 o -4 8 1 0.23 1.42 13.93 o -3 8 1 0.32 18.04 41.29 o -2 8 1 504.89 492.89 41.41 o 1 8 1 57.95 35.21 24.36 o 2 8 1 921.16 973.15 93.99 o 3 8 1 5.19 10.02 35.72 o 4 8 1 168.57 265.85 78.31 o 5 8 1 119.08 171.38 53.38 o 6 8 1 64.32 37.70 53.35 o 7 8 1 0.75 38.08 63.74 o 8 8 1 0.19 14.03 70.95 o -7 9 1 34.27 -11.63 53.33 o -6 9 1 0.32 -7.21 47.70 o -5 9 1 4.00 28.21 21.53 o -4 9 1 138.30 166.84 24.67 o -3 9 1 18.04 -6.40 20.51 o -2 9 1 125.81 107.58 28.52 o -1 9 1 392.19 376.11 41.72 o 0 9 1 1.02 2.70 23.31 o 1 9 1 71.89 65.85 31.16 o 2 9 1 66.23 66.58 42.24 o 3 9 1 0.39 35.28 61.73 o 5 9 1 33.07 95.43 91.42 o 6 9 1 34.59 99.04 73.78 o 7 9 1 72.22 22.06 113.11 o -6 10 1 6.23 54.65 27.97 o -5 10 1 0.04 3.99 31.84 o -4 10 1 374.77 296.82 62.88 o -3 10 1 233.04 341.70 109.48 o -2 10 1 57.85 24.71 40.40 o -1 10 1 363.09 457.77 49.89 o 0 10 1 0.24 27.21 37.36 o 1 10 1 85.62 152.39 47.98 o 2 10 1 33.15 16.94 50.35 o 3 10 1 120.08 44.63 52.31 o 4 10 1 7.89 -31.27 70.15 o 5 10 1 0.03 35.28 86.18 o 6 10 1 5.34 -166.56 111.04 o -5 11 1 11.71 50.65 40.06 o -4 11 1 15.69 -30.51 74.77 o -3 11 1 25.52 49.69 41.50 o -2 11 1 64.15 12.26 45.22 o -1 11 1 3.87 11.35 41.46 o 0 11 1 20.77 20.51 58.32 o 1 11 1 8.83 -40.26 38.48 o 2 11 1 43.80 51.90 44.91 o 3 11 1 20.40 28.11 70.99 o 4 11 1 16.74 83.35 59.61 o -1 12 1 78.49 80.22 90.25 o 0 12 1 64.24 56.55 66.98 o -3 -11 2 3.52 -27.66 90.19 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