# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_06skc0071p-1 _shelx_title ' 06skc0071p-1 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 188.15 _exptl_crystal_F_000 656.00 _reflns_d_resolution_high 0.7703 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.3001 _cell_length_b 11.9247 _cell_length_c 15.4496 _cell_angle_alpha 76.199 _cell_angle_beta 74.813 _cell_angle_gamma 89.758 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 71.08 45.39 19.78 o 3 0 0 1355.81 1702.10 57.21 o 4 0 0 1635.17 1859.91 66.68 o 5 0 0 628.16 748.96 47.36 o 6 0 0 65.21 34.20 23.17 o 7 0 0 345.60 200.27 43.47 o 8 0 0 77.07 118.02 34.20 o 9 0 0 13.45 -30.01 32.35 o 10 0 0 2.69 29.36 58.39 o 11 0 0 0.21 -104.97 166.41 o -11 1 0 0.23 33.99 126.24 o -10 1 0 34.25 35.51 57.51 o -9 1 0 0.24 59.54 30.37 o -8 1 0 346.72 344.89 48.72 o -7 1 0 64.63 145.62 33.43 o -6 1 0 1245.10 1254.39 57.42 o -5 1 0 99.87 128.47 19.40 o -4 1 0 36.33 -16.03 38.77 o -3 1 0 965.94 919.09 51.70 o -2 1 0 15753.03 16284.06 396.14 o 2 1 0 30007.78 29089.12 742.18 o 3 1 0 652.06 724.81 32.60 o 4 1 0 6.02 75.30 26.52 o 5 1 0 8.26 87.36 25.51 o 6 1 0 628.45 614.23 40.23 o 7 1 0 241.02 228.52 85.92 o 8 1 0 24.26 39.13 28.07 o 9 1 0 222.70 167.20 45.36 o 10 1 0 64.96 1.12 156.96 o 11 1 0 2.75 -1.74 87.52 o -11 2 0 22.84 35.55 94.94 o -10 2 0 0.00 -44.35 34.54 o -9 2 0 15.29 -6.84 35.83 o -8 2 0 104.81 40.04 26.48 o -7 2 0 205.35 172.96 83.08 o -6 2 0 352.43 313.94 40.43 o -5 2 0 322.33 352.95 35.38 o -4 2 0 225.93 180.74 30.89 o -3 2 0 1416.36 1611.27 83.43 o -2 2 0 1461.18 1611.62 79.03 o -1 2 0 590.06 610.84 34.89 o 0 2 0 20964.85 19249.10 912.84 o 1 2 0 92.83 140.88 18.76 o 2 2 0 1.41 38.12 23.51 o 3 2 0 30.94 60.91 20.67 o 4 2 0 1216.54 1031.79 61.48 o 5 2 0 559.02 456.67 35.44 o 6 2 0 10.58 -16.41 20.36 o 7 2 0 602.72 520.68 69.46 o 8 2 0 489.65 466.55 54.20 o 9 2 0 0.21 169.54 56.78 o 10 2 0 0.45 205.08 66.84 o 11 2 0 88.42 -200.73 133.82 o -11 3 0 1.87 78.80 50.99 o -10 3 0 0.01 -23.81 33.57 o -9 3 0 21.06 82.50 33.14 o -8 3 0 53.53 42.77 28.53 o -7 3 0 29.99 122.71 41.77 o -6 3 0 40.09 93.60 26.74 o -5 3 0 337.26 377.18 27.57 o -4 3 0 277.30 229.96 35.08 o -3 3 0 1016.87 1279.84 96.65 o -2 3 0 1598.68 1554.91 98.69 o -1 3 0 849.44 935.27 66.66 o 0 3 0 237.98 259.10 26.05 o 1 3 0 15.36 106.29 17.48 o 2 3 0 126.14 53.32 25.22 o 3 3 0 1573.87 1442.18 56.69 o 4 3 0 565.01 515.98 31.39 o 5 3 0 474.41 504.84 37.63 o 6 3 0 54.69 63.66 25.89 o 7 3 0 85.59 111.71 33.15 o 8 3 0 6.91 -17.84 37.36 o 9 3 0 74.99 59.37 86.90 o 10 3 0 79.05 101.94 73.65 o 11 3 0 19.75 213.99 84.48 o -11 4 0 64.73 12.63 143.54 o -10 4 0 35.51 76.72 36.95 o -9 4 0 3.59 82.97 34.57 o -8 4 0 237.34 333.88 33.56 o -7 4 0 93.42 145.96 25.99 o -6 4 0 245.15 212.76 33.18 o -5 4 0 121.87 91.38 27.03 o -4 4 0 264.71 378.12 43.62 o -3 4 0 835.99 738.27 89.90 o -2 4 0 6195.40 7098.82 353.39 o -1 4 0 952.56 912.81 52.56 o 0 4 0 8063.57 8279.34 241.17 o 1 4 0 4016.57 4025.83 122.01 o 2 4 0 951.96 921.88 41.97 o 3 4 0 123.80 39.26 35.79 o 4 4 0 212.69 300.74 36.68 o 5 4 0 2.80 -5.68 26.97 o 6 4 0 35.84 74.28 38.67 o 7 4 0 247.94 222.29 35.41 o 8 4 0 20.18 36.19 38.82 o 9 4 0 27.29 77.79 37.44 o 10 4 0 18.03 157.54 81.62 o 11 4 0 8.16 -38.06 80.71 o -11 5 0 40.10 103.70 58.11 o -10 5 0 50.88 9.07 42.79 o -9 5 0 267.22 237.40 49.13 o -8 5 0 0.05 -23.78 36.56 o -7 5 0 139.12 134.14 47.56 o -6 5 0 428.08 221.85 45.11 o -5 5 0 25.59 42.20 25.84 o -4 5 0 701.44 825.72 51.72 o -3 5 0 781.32 840.43 62.35 o -2 5 0 662.09 903.27 63.21 o -1 5 0 1234.88 1475.04 73.97 o 0 5 0 57.64 11.49 28.09 o 1 5 0 0.17 -24.39 25.78 o 2 5 0 894.01 903.03 37.18 o 3 5 0 345.23 328.62 31.37 o 4 5 0 474.39 463.75 47.62 o 5 5 0 1094.58 994.98 61.81 o 6 5 0 34.13 103.89 37.77 o 7 5 0 103.80 82.94 52.31 o 8 5 0 8.88 65.22 53.52 o 9 5 0 172.99 51.67 62.54 o 10 5 0 1.93 68.06 91.50 o -10 6 0 11.83 -20.23 49.11 o -9 6 0 22.80 -53.45 35.63 o -8 6 0 92.02 165.10 61.48 o -7 6 0 122.80 115.82 39.46 o -6 6 0 21.16 124.71 26.50 o -5 6 0 121.88 101.03 23.23 o -4 6 0 193.94 178.38 36.72 o -3 6 0 499.24 675.03 54.36 o -2 6 0 18.22 -23.13 33.21 o -1 6 0 100.97 154.84 29.45 o 0 6 0 1742.79 1718.93 83.83 o 1 6 0 26.57 18.66 29.17 o 2 6 0 0.26 19.56 22.15 o 3 6 0 0.27 64.68 24.30 o 4 6 0 1425.91 1592.80 84.96 o 5 6 0 25.95 -14.39 26.56 o 6 6 0 163.56 106.87 33.26 o 7 6 0 509.03 445.56 60.88 o 8 6 0 1.51 66.43 65.22 o 9 6 0 52.20 157.80 67.08 o 10 6 0 84.37 142.47 91.84 o -10 7 0 0.18 62.20 45.07 o -9 7 0 3.82 -15.05 41.58 o -8 7 0 0.58 24.91 52.81 o -7 7 0 143.62 301.94 52.58 o -6 7 0 309.97 385.08 39.56 o -5 7 0 0.92 -18.09 22.78 o -4 7 0 220.22 153.89 39.58 o -2 7 0 127.37 81.80 40.21 o -1 7 0 75.63 155.02 28.08 o 0 7 0 11.15 22.06 23.44 o 1 7 0 21.90 30.79 25.24 o 2 7 0 12.69 15.51 34.66 o 3 7 0 78.03 114.99 33.15 o 4 7 0 22.93 35.07 22.31 o 5 7 0 31.14 -18.58 33.91 o 6 7 0 407.59 466.12 44.08 o 7 7 0 25.04 76.09 39.40 o 8 7 0 56.52 32.09 34.06 o 9 7 0 103.77 134.47 32.60 o -10 8 0 44.43 130.80 69.13 o -9 8 0 11.87 7.31 41.55 o -8 8 0 1.56 183.62 47.38 o -7 8 0 253.67 464.10 58.81 o -6 8 0 98.40 147.39 46.18 o -5 8 0 208.58 178.22 25.66 o -4 8 0 370.92 322.94 39.72 o -3 8 0 42.15 100.28 55.65 o -2 8 0 35.82 52.95 29.27 o -1 8 0 609.12 608.11 31.61 o 0 8 0 798.76 652.08 52.82 o 1 8 0 80.64 137.32 33.36 o 2 8 0 137.19 88.99 36.53 o 3 8 0 86.64 51.40 22.58 o 4 8 0 4.89 14.33 25.10 o 5 8 0 0.65 27.60 33.26 o 6 8 0 2.59 -56.01 37.34 o 7 8 0 14.77 -2.56 46.19 o 8 8 0 114.09 154.09 55.00 o 9 8 0 0.52 26.85 34.47 o -9 9 0 178.67 211.94 55.99 o -8 9 0 34.88 120.37 38.09 o -7 9 0 41.56 33.28 40.55 o -6 9 0 2.99 -9.02 87.87 o -5 9 0 71.71 113.52 40.72 o -4 9 0 41.08 62.65 43.29 o -3 9 0 22.67 137.60 23.89 o -2 9 0 392.50 291.63 38.32 o -1 9 0 363.58 354.30 50.42 o 0 9 0 13.34 57.09 33.97 o 1 9 0 39.35 -6.72 49.36 o 2 9 0 499.79 387.05 59.66 o 3 9 0 62.88 41.35 31.79 o 4 9 0 44.63 38.82 32.75 o 5 9 0 83.09 62.77 36.20 o 6 9 0 3.85 96.70 63.16 o 7 9 0 7.90 153.84 59.99 o 8 9 0 39.68 16.85 47.44 o -9 10 0 4.32 -3.94 44.95 o -8 10 0 55.40 75.41 51.66 o -7 10 0 388.12 241.81 97.36 o -6 10 0 170.54 416.30 66.34 o -5 10 0 0.18 269.76 92.62 o -4 10 0 40.23 44.02 25.50 o -3 10 0 43.46 128.38 57.15 o -2 10 0 5.68 15.79 40.22 o -1 10 0 148.80 162.18 91.47 o 0 10 0 264.08 280.56 50.63 o 1 10 0 1115.39 1020.44 124.84 o 2 10 0 3.65 -28.09 41.50 o 3 10 0 7.28 -27.59 50.82 o 4 10 0 32.05 59.80 28.02 o 5 10 0 3.46 11.78 31.19 o 6 10 0 9.21 117.48 33.20 o 7 10 0 1.15 40.83 32.16 o 8 10 0 12.00 14.17 72.95 o -8 11 0 2.34 26.29 63.56 o -7 11 0 61.50 147.44 39.27 o -6 11 0 151.65 130.61 35.31 o -5 11 0 249.89 407.67 49.41 o -4 11 0 0.26 2.16 17.31 o -3 11 0 80.93 179.42 110.97 o -2 11 0 141.03 32.83 27.08 o -1 11 0 1.11 11.15 92.11 o 0 11 0 11.37 38.07 52.54 o 1 11 0 286.02 199.80 48.72 o 2 11 0 132.12 187.80 48.39 o 3 11 0 296.18 420.77 61.97 o 4 11 0 17.66 -118.56 97.25 o 5 11 0 6.29 -25.86 37.34 o 6 11 0 90.15 34.30 52.64 o 7 11 0 67.50 96.63 75.19 o -7 12 0 12.78 -67.89 45.26 o -6 12 0 61.59 98.53 40.44 o -5 12 0 8.54 77.17 47.95 o -4 12 0 36.55 32.58 80.14 o -3 12 0 23.62 -96.34 112.11 o -2 12 0 0.12 109.13 52.75 o -1 12 0 169.86 231.50 72.28 o 0 12 0 160.94 203.20 65.67 o 1 12 0 164.45 249.84 75.63 o 2 12 0 0.10 75.21 45.98 o 3 12 0 81.50 67.62 44.88 o 4 12 0 3.29 -34.72 71.04 o 5 12 0 29.66 166.33 87.98 o 6 12 0 4.06 2.15 61.52 o -6 13 0 46.75 -79.62 60.83 o -5 13 0 33.08 42.05 48.11 o -4 13 0 17.75 110.55 69.12 o -3 13 0 7.32 59.17 47.57 o -2 13 0 2.97 202.85 85.64 o 0 13 0 4.18 35.16 62.80 o 1 13 0 23.44 96.55 64.33 o 2 13 0 28.03 29.17 59.85 o 3 13 0 18.80 113.28 148.93 o 4 13 0 0.23 61.35 113.18 o -4 14 0 19.70 408.04 118.85 o -3 14 0 4.99 -59.53 96.72 o -2 14 0 3.45 -124.93 83.29 o -1 14 0 34.39 67.09 140.66 o 0 14 0 64.49 0.02 83.97 o 1 14 0 32.97 436.27 143.47 o 2 14 0 25.50 87.28 97.50 o 3 14 0 4.55 116.77 84.61 o -1 15 0 9.37 -81.95 54.63 o 0 15 0 2.98 24.51 97.54 o -2 -14 1 0.01 -40.19 65.48 o -1 -14 1 9.40 30.20 76.85 o 0 -14 1 60.00 28.28 76.43 o 1 -14 1 1.27 88.43 74.43 o 2 -14 1 7.12 -28.90 68.82 o 3 -14 1 3.44 308.57 109.63 o 4 -14 1 12.66 -18.69 111.71 o -4 -13 1 5.78 48.07 89.56 o -3 -13 1 0.00 -15.98 97.96 o -2 -13 1 3.38 133.56 169.71 o -1 -13 1 0.17 40.83 103.48 o 0 -13 1 9.29 114.25 78.64 o 1 -13 1 53.41 234.00 88.25 o 2 -13 1 48.10 103.49 74.38 o 3 -13 1 10.51 58.20 76.25 o 4 -13 1 21.43 116.63 190.98 o 5 -13 1 8.54 2.88 86.43 o 6 -13 1 0.01 -74.81 71.17 o -5 -12 1 7.96 154.97 67.81 o -4 -12 1 0.02 18.34 68.29 o -3 -12 1 25.07 93.01 117.10 o -2 -12 1 1.77 31.76 33.96 o -1 -12 1 27.87 27.39 31.59 o 0 -12 1 2.27 -36.07 63.94 o 1 -12 1 168.16 258.56 60.18 o 2 -12 1 12.27 -7.53 58.95 o 3 -12 1 48.71 35.64 55.89 o 4 -12 1 42.74 18.85 41.53 o 5 -12 1 19.83 135.52 45.29 o 6 -12 1 55.50 83.06 24.88 o 7 -12 1 99.92 144.40 74.80 o -7 -11 1 1.70 -14.24 140.01 o -6 -11 1 47.46 -81.53 73.80 o -5 -11 1 1.14 -16.67 31.28 o -4 -11 1 52.86 42.11 77.31 o -3 -11 1 72.51 198.00 45.20 o -2 -11 1 90.04 195.62 68.76 o -1 -11 1 86.30 125.51 58.45 o 0 -11 1 0.35 12.51 41.56 o 1 -11 1 439.62 533.05 86.88 o 2 -11 1 35.99 79.66 49.60 o 3 -11 1 55.50 11.47 36.46 o 4 -11 1 9.33 13.98 18.01 o 5 -11 1 49.16 -2.80 66.28 o 6 -11 1 99.39 132.99 29.35 o 7 -11 1 6.62 28.45 64.00 o 8 -11 1 28.83 70.20 48.88 o -7 -10 1 0.18 -78.61 97.76 o -6 -10 1 19.76 25.66 35.94 o -5 -10 1 0.78 69.22 61.29 o -4 -10 1 0.24 91.23 28.03 o -3 -10 1 19.86 17.28 40.16 o -2 -10 1 227.15 188.92 40.11 o -1 -10 1 2.25 -6.17 54.95 o 0 -10 1 166.14 209.31 53.78 o 2 -10 1 159.93 181.24 32.48 o 3 -10 1 251.23 225.26 40.53 o 4 -10 1 0.30 56.94 67.92 o 5 -10 1 16.53 -3.32 32.76 o 6 -10 1 6.18 106.72 41.16 o 7 -10 1 21.43 -14.22 30.74 o 8 -10 1 81.19 42.31 56.95 o 9 -10 1 18.65 11.61 40.01 o -8 -9 1 7.66 55.69 36.91 o -7 -9 1 11.09 52.02 39.96 o -6 -9 1 0.61 20.38 34.21 o -5 -9 1 43.92 48.64 39.77 o -4 -9 1 0.22 41.74 34.73 o -3 -9 1 12.49 -56.63 37.75 o -2 -9 1 35.28 137.87 54.78 o -1 -9 1 21.14 -25.04 33.25 o 0 -9 1 106.85 155.23 35.66 o 1 -9 1 108.58 63.54 36.70 o 2 -9 1 547.68 418.70 44.75 o 3 -9 1 74.65 0.42 68.32 o 4 -9 1 236.07 0.06 87.83 o 5 -9 1 392.13 403.13 88.00 o 6 -9 1 5.79 -17.39 25.71 o 7 -9 1 0.72 127.34 46.70 o 8 -9 1 0.64 132.10 54.23 o 9 -9 1 4.88 102.38 56.38 o -9 -8 1 29.30 12.62 70.63 o -8 -8 1 318.84 271.28 68.72 o -7 -8 1 83.87 87.02 39.67 o -6 -8 1 0.40 22.31 39.20 o -5 -8 1 24.52 -49.04 35.59 o -4 -8 1 218.83 154.94 32.99 o -3 -8 1 474.33 371.28 45.38 o -2 -8 1 40.13 60.91 20.66 o -1 -8 1 29.71 46.41 24.95 o 0 -8 1 433.30 455.17 43.67 o 1 -8 1 91.83 69.96 29.63 o 2 -8 1 5.52 23.41 26.16 o 3 -8 1 53.87 91.25 64.77 o 4 -8 1 869.79 732.60 47.22 o 5 -8 1 44.18 86.07 35.76 o 6 -8 1 391.51 198.15 165.56 o 7 -8 1 327.41 265.31 52.61 o 8 -8 1 105.36 243.23 44.58 o 9 -8 1 51.21 56.39 55.07 o 10 -8 1 1.66 101.40 48.14 o -9 -7 1 9.28 -22.26 37.60 o -8 -7 1 6.54 30.91 32.39 o -7 -7 1 6.81 69.61 37.16 o -6 -7 1 650.77 629.45 59.37 o -5 -7 1 160.00 146.82 24.61 o -4 -7 1 43.08 139.10 26.68 o -3 -7 1 45.08 51.30 27.71 o -2 -7 1 1649.52 1634.67 74.43 o -1 -7 1 221.49 141.12 35.19 o 0 -7 1 111.88 85.88 44.63 o 1 -7 1 0.31 -23.11 16.15 o 2 -7 1 107.08 112.65 33.82 o 3 -7 1 345.72 304.22 40.90 o 4 -7 1 17.52 61.39 30.08 o 5 -7 1 91.62 55.90 22.40 o 6 -7 1 962.51 828.17 66.12 o 7 -7 1 4.16 23.41 20.12 o 8 -7 1 41.23 103.62 90.29 o 9 -7 1 107.77 380.81 46.41 o 10 -7 1 24.07 96.38 75.80 o -10 -6 1 4.98 27.14 83.11 o -9 -6 1 4.84 174.26 77.94 o -8 -6 1 237.91 144.04 72.67 o -7 -6 1 16.79 17.84 45.82 o -6 -6 1 466.36 358.41 47.18 o -5 -6 1 27.25 8.15 53.33 o -4 -6 1 4.03 26.83 27.53 o -3 -6 1 31.19 97.99 34.31 o -2 -6 1 68.20 134.43 29.12 o -1 -6 1 1443.29 1502.65 83.23 o 0 -6 1 355.17 384.92 33.03 o 1 -6 1 249.65 195.40 18.98 o 2 -6 1 1040.79 1161.99 69.27 o 3 -6 1 489.98 370.73 95.82 o 4 -6 1 507.47 543.69 37.19 o 5 -6 1 252.54 204.24 28.83 o 6 -6 1 130.54 151.06 22.40 o 7 -6 1 0.80 -19.94 38.26 o 8 -6 1 721.94 1034.47 106.52 o 9 -6 1 1.85 -59.77 39.85 o 10 -6 1 72.74 257.47 69.19 o -10 -5 1 11.94 11.29 180.46 o -9 -5 1 86.10 324.38 107.48 o -8 -5 1 112.29 83.43 71.77 o -7 -5 1 31.81 55.76 32.03 o -6 -5 1 41.36 143.63 32.61 o -5 -5 1 1.88 25.65 22.74 o -4 -5 1 265.92 198.41 29.15 o -3 -5 1 59.98 70.29 20.65 o -2 -5 1 165.24 175.89 21.20 o -1 -5 1 49.00 63.87 33.66 o 0 -5 1 24.18 23.01 13.32 o 1 -5 1 169.64 135.04 38.62 o 2 -5 1 30.89 39.08 26.97 o 3 -5 1 34.44 81.17 22.07 o 4 -5 1 218.60 180.99 25.84 o 5 -5 1 7.10 143.75 30.09 o 6 -5 1 597.57 302.23 55.42 o 7 -5 1 17.30 3.61 31.90 o 8 -5 1 55.74 117.04 37.80 o 9 -5 1 64.74 133.43 32.01 o 10 -5 1 298.88 394.03 57.40 o 11 -5 1 50.60 95.43 84.61 o -10 -4 1 0.04 -56.91 140.96 o -9 -4 1 1.00 0.86 39.41 o -8 -4 1 229.86 104.26 60.65 o -7 -4 1 371.85 361.55 48.18 o -6 -4 1 5.73 -34.91 24.17 o -5 -4 1 888.47 723.23 53.66 o -4 -4 1 11.67 72.40 29.22 o -3 -4 1 201.29 127.08 27.76 o -2 -4 1 95.67 121.17 25.64 o -1 -4 1 10.31 12.90 21.53 o 0 -4 1 1412.22 1632.65 67.85 o 1 -4 1 2916.37 3275.19 167.56 o 2 -4 1 135.06 132.50 43.82 o 3 -4 1 760.59 716.20 60.08 o 4 -4 1 4.75 13.89 28.81 o 5 -4 1 15.73 99.63 20.68 o 6 -4 1 8.43 -3.46 21.08 o 7 -4 1 21.13 99.61 44.84 o 8 -4 1 85.50 173.81 47.15 o 9 -4 1 24.03 50.72 57.81 o 10 -4 1 2.73 176.75 44.00 o 11 -4 1 42.69 143.91 81.14 o -11 -3 1 1.08 -0.87 88.54 o -10 -3 1 110.08 3.50 67.47 o -9 -3 1 108.71 304.95 67.48 o -8 -3 1 10.40 117.02 35.68 o -7 -3 1 0.65 95.19 28.60 o -6 -3 1 1276.82 996.05 93.71 o -5 -3 1 1031.13 1090.86 82.83 o -4 -3 1 421.01 485.74 43.77 o -3 -3 1 1141.84 1136.91 55.84 o -2 -3 1 56.75 70.74 25.35 o -1 -3 1 61.83 102.74 16.95 o 0 -3 1 127.12 61.12 31.21 o 1 -3 1 670.25 679.65 47.62 o 2 -3 1 27.65 43.25 24.01 o 3 -3 1 838.57 803.71 51.13 o 4 -3 1 306.93 295.93 31.84 o 5 -3 1 39.81 114.40 28.51 o 6 -3 1 270.82 238.00 26.00 o 7 -3 1 18.28 123.40 46.01 o 8 -3 1 13.26 31.31 27.60 o 9 -3 1 93.67 95.42 40.08 o 10 -3 1 46.50 -30.90 36.82 o 11 -3 1 5.99 29.41 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