 data_global
 
_publ_contact_author               'Coles, Simon J.'
_publ_contact_author_email          s.j.coles@soton.ac.uk
 
loop_
_publ_author_name
 
'Coles, Simon J.'
'Hursthouse, Michael B.'
 
_journal_name_full                 'private communication'

data_03src0073
 
_audit_creation_method            SHELXL-97
_chemical_name_systematic
;
 ?
;
_chemical_name_common             ?
_chemical_melting_point           ?
_chemical_formula_moiety          ?
_chemical_formula_sum
 'C10 H22 Cl8 N10 O0 P6'
_chemical_formula_weight          751.80
 
loop_
 _atom_type_symbol
 _atom_type_description
 _atom_type_scat_dispersion_real
 _atom_type_scat_dispersion_imag
 _atom_type_scat_source
 'C'  'C'   0.0033   0.0016
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'H'  'H'   0.0000   0.0000
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'N'  'N'   0.0061   0.0033
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'O'  'O'   0.0106   0.0060
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'P'  'P'   0.1023   0.0942
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Cl'  'Cl'   0.1484   0.1585
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 
_symmetry_cell_setting            Triclinic
_symmetry_space_group_name_H-M    P-1
 
loop_
 _symmetry_equiv_pos_as_xyz
 'x, y, z'
 '-x, -y, -z'
 
_cell_length_a                    10.0230(4)
_cell_length_b                    10.8755(5)
_cell_length_c                    15.3970(7)
_cell_angle_alpha                 79.211(2)
_cell_angle_beta                  77.133(2)
_cell_angle_gamma                 69.254(2)
_cell_volume                      1519.28(12)
_cell_formula_units_Z             2
_cell_measurement_temperature     120(2)
_cell_measurement_reflns_used     15566
_cell_measurement_theta_min       2.91
_cell_measurement_theta_max       27.48
 
_exptl_crystal_description        blade
_exptl_crystal_colour             colourless
_exptl_crystal_size_max           0.35
_exptl_crystal_size_mid           0.14
_exptl_crystal_size_min           0.12
_exptl_crystal_density_meas       ?
_exptl_crystal_density_diffrn     1.643
_exptl_crystal_density_method     'not measured'
_exptl_crystal_F_000              756
_exptl_absorpt_coefficient_mu     1.081
_exptl_absorpt_correction_type    multi-scan
_exptl_absorpt_correction_T_min   0.7036
_exptl_absorpt_correction_T_max   0.8813
_exptl_absorpt_process_details    'SORTAV (Blessing, 1997)'
 
_exptl_special_details
;
 ?
;
 
_diffrn_ambient_temperature       120(2)
_diffrn_radiation_wavelength      0.71073
_diffrn_radiation_type            MoK\a
_diffrn_radiation_source         'Bruker-Nonius FR591 rotating anode'
_diffrn_radiation_monochromator   graphite
_diffrn_measurement_device_type    'Bruker-Nonius KappaCCD'
_diffrn_measurement_method         'φ & ω scans'
_diffrn_detector_area_resol_mean  9.091
_diffrn_standards_decay_%         negligible
_diffrn_reflns_number             23087
_diffrn_reflns_av_R_equivalents   0.1145
_diffrn_reflns_av_sigmaI/netI     0.0842
_diffrn_reflns_limit_h_min        -12
_diffrn_reflns_limit_h_max        12
_diffrn_reflns_limit_k_min        -14
_diffrn_reflns_limit_k_max        14
_diffrn_reflns_limit_l_min        -19
_diffrn_reflns_limit_l_max        19
_diffrn_reflns_theta_min          3.10
_diffrn_reflns_theta_max          27.41
_reflns_number_total              6805
_reflns_number_gt                 4657
_reflns_threshold_expression      >2sigma(I)
 
_computing_data_collection        
'DENZO (Otwinowski & Minor, 1997) & COLLECT (Hooft, 1998)'
_computing_cell_refinement        'DENZO & COLLECT'
_computing_data_reduction          'DENZO & COLLECT'
_computing_structure_solution      'SHELXS-97 (Sheldrick, 1997)'
_computing_structure_refinement   'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics     ?
_computing_publication_material   ?
 
_refine_special_details
;
 Refinement of F² against ALL reflections.  The weighted R-factor wR and
 goodness of fit S are based on F², conventional R-factors R are based
 on F, with F set to zero for negative F². The threshold expression of
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is
 not relevant to the choice of reflections for refinement.  R-factors based
 on F² are statistically about twice as large as those based on F, and R-
 factors based on ALL data will be even larger.
;
 
_refine_ls_structure_factor_coef  Fsqd
_refine_ls_matrix_type            full
_refine_ls_weighting_scheme       calc
_refine_ls_weighting_details
 'calc w=1/[σ²(Fo²)+(0.0959P)²+3.8325P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary      direct
_atom_sites_solution_secondary    difmap
_atom_sites_solution_hydrogens    geom
_refine_ls_hydrogen_treatment     mixed
_refine_ls_extinction_method      none
_refine_ls_extinction_coef        ?
_refine_ls_number_reflns          6805
_refine_ls_number_parameters      315
_refine_ls_number_restraints      206
_refine_ls_R_factor_all           0.1087
_refine_ls_R_factor_gt            0.0742
_refine_ls_wR_factor_ref          0.2184
_refine_ls_wR_factor_gt           0.1960
_refine_ls_goodness_of_fit_ref    1.049
_refine_ls_restrained_S_all       1.033
_refine_ls_shift/su_max           0.121
_refine_ls_shift/su_mean          0.008
 
loop_
 _atom_site_label
 _atom_site_type_symbol
 _atom_site_fract_x
 _atom_site_fract_y
 _atom_site_fract_z
 _atom_site_U_iso_or_equiv
 _atom_site_adp_type
 _atom_site_occupancy
 _atom_site_symmetry_multiplicity
 _atom_site_calc_flag
 _atom_site_refinement_flags
 _atom_site_disorder_assembly
 _atom_site_disorder_group
H4N H 0.544(3) 0.382(5) 0.165(3) 0.052(17) Uiso 1 1 d D . .
H7N H -0.508(6) 1.353(2) 0.342(4) 0.060(19) Uiso 1 1 d D . .
C1 C 0.4023(6) 0.3889(6) 0.0894(4) 0.0491(14) Uani 1 1 d U . .
H1A H 0.4697 0.3020 0.0724 0.059 Uiso 1 1 calc R . .
H1B H 0.3884 0.4506 0.0336 0.059 Uiso 1 1 calc R . .
C2 C 0.2608(7) 0.3733(7) 0.1340(5) 0.068(2) Uani 1 1 d U . .
H2A H 0.2774 0.2805 0.1618 0.082 Uiso 1 1 calc R . .
H2B H 0.1995 0.3902 0.0879 0.082 Uiso 1 1 calc R . .
C3 C 0.1810(6) 0.4629(5) 0.2041(4) 0.0468(13) Uani 1 1 d U . .
H3A H 0.0757 0.4845 0.2067 0.056 Uiso 1 1 calc R . .
H3B H 0.2048 0.4161 0.2631 0.056 Uiso 1 1 calc R . .
C4 C 0.0947(6) 0.7108(5) 0.1836(4) 0.0464(13) Uani 1 1 d U . .
H4A H 0.0317 0.7053 0.1442 0.056 Uiso 1 1 calc R . .
H4B H 0.1340 0.7833 0.1555 0.056 Uiso 1 1 calc R . .
C5 C 0.0041(6) 0.7456(5) 0.2724(4) 0.0436(12) Uani 1 1 d U . .
H5A H 0.0653 0.7543 0.3117 0.052 Uiso 1 1 calc R . .
H5B H -0.0349 0.6732 0.3014 0.052 Uiso 1 1 calc R . .
C6 C -0.1205(6) 0.8739(5) 0.2627(4) 0.0453(13) Uani 1 1 d U . .
H6A H -0.0812 0.9454 0.2320 0.054 Uiso 1 1 calc R . .
H6B H -0.1827 0.8640 0.2246 0.054 Uiso 1 1 calc R . .
C7 C -0.2113(6) 0.9132(5) 0.3517(4) 0.0469(13) Uani 1 1 d U . .
H7A H -0.2507 0.8416 0.3819 0.056 Uiso 1 1 calc R . .
H7B H -0.1481 0.9214 0.3899 0.056 Uiso 1 1 calc R . .
C8 C -0.4668(7) 1.0374(6) 0.3253(5) 0.0610(17) Uani 1 1 d U . .
H8A H -0.4643 0.9447 0.3294 0.073 Uiso 1 1 calc R . .
H8B H -0.4769 1.0792 0.2631 0.073 Uiso 1 1 calc R . .
C9 C -0.5964(7) 1.1110(7) 0.3897(6) 0.076(2) Uani 1 1 d U . .
H9A H -0.6800 1.1525 0.3578 0.091 Uiso 1 1 calc R . .
H9B H -0.6217 1.0465 0.4393 0.091 Uiso 1 1 calc R . .
C10 C -0.5723(6) 1.2147(6) 0.4282(5) 0.0533(15) Uani 1 1 d U . .
H10A H -0.6659 1.2853 0.4426 0.064 Uiso 1 1 calc R . .
H10B H -0.5340 1.1758 0.4847 0.064 Uiso 1 1 calc R . .
N1 N 0.4052(5) 0.7057(4) 0.1254(3) 0.0395(10) Uani 1 1 d U . .
N2 N 0.5161(7) 0.7686(5) 0.2491(3) 0.0557(14) Uani 1 1 d U . .
N3 N 0.4291(4) 0.5536(4) 0.2830(3) 0.0320(8) Uani 1 1 d U . .
N4 N 0.4680(5) 0.4380(4) 0.1443(3) 0.0366(9) Uani 1 1 d DU . .
N5 N 0.2156(4) 0.5861(4) 0.1874(3) 0.0377(9) Uani 1 1 d U . .
N6 N -0.3325(4) 1.0384(4) 0.3450(3) 0.0408(10) Uani 1 1 d U . .
N7 N -0.4710(4) 1.2726(4) 0.3665(3) 0.0335(9) Uani 1 1 d DU . .
N8 N -0.2711(4) 1.2436(4) 0.2273(3) 0.0391(10) Uani 1 1 d U . .
N9 N -0.0035(5) 1.2293(6) 0.2454(4) 0.0634(15) Uani 1 1 d U . .
N10 N -0.1902(4) 1.1690(5) 0.3881(3) 0.0409(10) Uani 1 1 d U . .
P1 P 0.38145(13) 0.57521(11) 0.18592(8) 0.0299(3) Uani 1 1 d U . .
P2 P 0.46704(18) 0.79978(14) 0.15522(9) 0.0445(4) Uani 1 1 d U . .
P3 P 0.49220(15) 0.64634(12) 0.31445(9) 0.0359(3) Uani 1 1 d U . .
P4 P -0.30964(12) 1.18198(11) 0.32989(8) 0.0297(3) Uani 1 1 d U . .
P5 P -0.12305(16) 1.26337(16) 0.18554(11) 0.0510(4) Uani 1 1 d U . .
P6 P -0.03956(14) 1.18236(15) 0.34777(12) 0.0473(4) Uani 1 1 d U . .
Cl1 Cl 0.3246(3) 0.98255(16) 0.14935(14) 0.0831(6) Uani 1 1 d U . .
Cl2 Cl 0.6375(3) 0.8196(3) 0.06755(14) 0.1045(9) Uani 1 1 d U . .
Cl3 Cl 0.37395(19) 0.70985(16) 0.42965(10) 0.0576(4) Uani 1 1 d U . .
Cl4 Cl 0.68049(18) 0.54071(17) 0.35593(14) 0.0667(5) Uani 1 1 d U . .
Cl5 Cl -0.0355(2) 1.1638(3) 0.07733(15) 0.0972(7) Uani 1 1 d U . .
Cl6 Cl -0.1634(2) 1.4516(2) 0.12470(18) 0.0934(8) Uani 1 1 d U . .
Cl7 Cl -0.0034(2) 1.2873(3) 0.4306(2) 0.1142(10) Uani 1 1 d U . .
Cl8 Cl 0.11259(15) 1.00939(16) 0.37626(12) 0.0584(4) Uani 1 1 d U . .
 
 
_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
 
loop_
 _geom_bond_atom_site_label_1
 _geom_bond_atom_site_label_2
 _geom_bond_distance
 _geom_bond_site_symmetry_2
 _geom_bond_publ_flag
C1 N4 1.449(6) . ?
C1 C2 1.484(8) . ?
C1 H1A 0.9900 . ?
C1 H1B 0.9900 . ?
C2 C3 1.486(8) . ?
C2 H2A 0.9900 . ?
C2 H2B 0.9900 . ?
C3 N5 1.464(6) . ?
C3 H3A 0.9900 . ?
C3 H3B 0.9900 . ?
C4 N5 1.465(7) . ?
C4 C5 1.496(8) . ?
C4 H4A 0.9900 . ?
C4 H4B 0.9900 . ?
C5 C6 1.516(7) . ?
C5 H5A 0.9900 . ?
C5 H5B 0.9900 . ?
C6 C7 1.509(8) . ?
C6 H6A 0.9900 . ?
C6 H6B 0.9900 . ?
C7 N6 1.474(7) . ?
C7 H7A 0.9900 . ?
C7 H7B 0.9900 . ?
C8 N6 1.449(7) . ?
C8 C9 1.516(10) . ?
C8 H8A 0.9900 . ?
C8 H8B 0.9900 . ?
C9 C10 1.479(9) . ?
C9 H9A 0.9900 . ?
C9 H9B 0.9900 . ?
C10 N7 1.458(7) . ?
C10 H10A 0.9900 . ?
C10 H10B 0.9900 . ?
N1 P2 1.547(4) . ?
N1 P1 1.607(4) . ?
N2 P3 1.567(5) . ?
N2 P2 1.569(5) . ?
N3 P3 1.557(4) . ?
N3 P1 1.620(4) . ?
N4 P1 1.607(4) . ?
N4 H4N 0.8702(13) . ?
N5 P1 1.619(4) . ?
N6 P4 1.624(4) . ?
N7 P4 1.606(4) . ?
N7 H7N 0.8702(14) . ?
N8 P5 1.553(4) . ?
N8 P4 1.615(4) . ?
N9 P6 1.566(6) . ?
N9 P5 1.572(6) . ?
N10 P6 1.546(4) . ?
N10 P4 1.601(4) . ?
P2 Cl2 1.978(3) . ?
P2 Cl1 1.994(2) . ?
P3 Cl3 1.9926(19) . ?
P3 Cl4 2.004(2) . ?
P5 Cl5 2.017(3) . ?
P5 Cl6 2.024(2) . ?
P6 Cl8 2.003(2) . ?
P6 Cl7 2.026(3) . ?
 
loop_
 _geom_angle_atom_site_label_1
 _geom_angle_atom_site_label_2
 _geom_angle_atom_site_label_3
 _geom_angle
 _geom_angle_site_symmetry_1
 _geom_angle_site_symmetry_3
 _geom_angle_publ_flag
N4 C1 C2 114.1(5) . . ?
N4 C1 H1A 108.7 . . ?
C2 C1 H1A 108.7 . . ?
N4 C1 H1B 108.7 . . ?
C2 C1 H1B 108.7 . . ?
H1A C1 H1B 107.6 . . ?
C1 C2 C3 114.0(5) . . ?
C1 C2 H2A 108.8 . . ?
C3 C2 H2A 108.8 . . ?
C1 C2 H2B 108.8 . . ?
C3 C2 H2B 108.8 . . ?
H2A C2 H2B 107.6 . . ?
N5 C3 C2 112.8(5) . . ?
N5 C3 H3A 109.0 . . ?
C2 C3 H3A 109.0 . . ?
N5 C3 H3B 109.0 . . ?
C2 C3 H3B 109.0 . . ?
H3A C3 H3B 107.8 . . ?
N5 C4 C5 114.8(5) . . ?
N5 C4 H4A 108.6 . . ?
C5 C4 H4A 108.6 . . ?
N5 C4 H4B 108.6 . . ?
C5 C4 H4B 108.6 . . ?
H4A C4 H4B 107.5 . . ?
C4 C5 C6 111.7(5) . . ?
C4 C5 H5A 109.3 . . ?
C6 C5 H5A 109.3 . . ?
C4 C5 H5B 109.3 . . ?
C6 C5 H5B 109.3 . . ?
H5A C5 H5B 107.9 . . ?
C7 C6 C5 112.7(5) . . ?
C7 C6 H6A 109.0 . . ?
C5 C6 H6A 109.0 . . ?
C7 C6 H6B 109.0 . . ?
C5 C6 H6B 109.0 . . ?
H6A C6 H6B 107.8 . . ?
N6 C7 C6 114.3(5) . . ?
N6 C7 H7A 108.7 . . ?
C6 C7 H7A 108.7 . . ?
N6 C7 H7B 108.7 . . ?
C6 C7 H7B 108.7 . . ?
H7A C7 H7B 107.6 . . ?
N6 C8 C9 111.5(5) . . ?
N6 C8 H8A 109.3 . . ?
C9 C8 H8A 109.3 . . ?
N6 C8 H8B 109.3 . . ?
C9 C8 H8B 109.3 . . ?
H8A C8 H8B 108.0 . . ?
C10 C9 C8 113.8(5) . . ?
C10 C9 H9A 108.8 . . ?
C8 C9 H9A 108.8 . . ?
C10 C9 H9B 108.8 . . ?
C8 C9 H9B 108.8 . . ?
H9A C9 H9B 107.7 . . ?
N7 C10 C9 111.9(5) . . ?
N7 C10 H10A 109.2 . . ?
C9 C10 H10A 109.2 . . ?
N7 C10 H10B 109.2 . . ?
C9 C10 H10B 109.2 . . ?
H10A C10 H10B 107.9 . . ?
P2 N1 P1 124.5(3) . . ?
P3 N2 P2 119.1(3) . . ?
P3 N3 P1 124.6(2) . . ?
C1 N4 P1 120.5(4) . . ?
C1 N4 H4N 117(4) . . ?
P1 N4 H4N 121(4) . . ?
C4 N5 C3 117.4(4) . . ?
C4 N5 P1 124.5(4) . . ?
C3 N5 P1 117.7(3) . . ?
C8 N6 C7 119.3(4) . . ?
C8 N6 P4 116.1(4) . . ?
C7 N6 P4 122.3(4) . . ?
C10 N7 P4 120.9(4) . . ?
C10 N7 H7N 116(4) . . ?
P4 N7 H7N 122(4) . . ?
P5 N8 P4 123.7(3) . . ?
P6 N9 P5 118.9(3) . . ?
P6 N10 P4 124.2(3) . . ?
N4 P1 N1 115.9(2) . . ?
N4 P1 N3 105.3(2) . . ?
N1 P1 N3 112.0(2) . . ?
N4 P1 N5 101.0(2) . . ?
N1 P1 N5 106.6(2) . . ?
N3 P1 N5 116.0(2) . . ?
N1 P2 N2 120.3(2) . . ?
N1 P2 Cl2 110.57(19) . . ?
N2 P2 Cl2 105.0(2) . . ?
N1 P2 Cl1 109.3(2) . . ?
N2 P2 Cl1 107.0(2) . . ?
Cl2 P2 Cl1 103.27(13) . . ?
N3 P3 N2 119.5(2) . . ?
N3 P3 Cl3 109.93(17) . . ?
N2 P3 Cl3 108.3(2) . . ?
N3 P3 Cl4 110.10(17) . . ?
N2 P3 Cl4 107.4(2) . . ?
Cl3 P3 Cl4 99.74(9) . . ?
N7 P4 N10 115.1(2) . . ?
N7 P4 N8 105.8(2) . . ?
N10 P4 N8 112.1(2) . . ?
N7 P4 N6 100.1(2) . . ?
N10 P4 N6 106.7(2) . . ?
N8 P4 N6 116.7(2) . . ?
N8 P5 N9 119.9(3) . . ?
N8 P5 Cl5 109.1(2) . . ?
N9 P5 Cl5 108.2(3) . . ?
N8 P5 Cl6 107.65(19) . . ?
N9 P5 Cl6 110.2(2) . . ?
Cl5 P5 Cl6 99.89(13) . . ?
N10 P6 N9 119.9(3) . . ?
N10 P6 Cl8 108.77(19) . . ?
N9 P6 Cl8 108.0(2) . . ?
N10 P6 Cl7 105.4(2) . . ?
N9 P6 Cl7 114.7(2) . . ?
Cl8 P6 Cl7 97.72(11) . . ?
 
loop_
 _geom_torsion_atom_site_label_1
 _geom_torsion_atom_site_label_2
 _geom_torsion_atom_site_label_3
 _geom_torsion_atom_site_label_4
 _geom_torsion
 _geom_torsion_site_symmetry_1
 _geom_torsion_site_symmetry_2
 _geom_torsion_site_symmetry_3
 _geom_torsion_site_symmetry_4
 _geom_torsion_publ_flag
N4 C1 C2 C3 26.6(9) . . . . ?
C1 C2 C3 N5 27.9(9) . . . . ?
N5 C4 C5 C6 -178.7(5) . . . . ?
C4 C5 C6 C7 -178.4(5) . . . . ?
C5 C6 C7 N6 179.3(5) . . . . ?
N6 C8 C9 C10 26.5(9) . . . . ?
C8 C9 C10 N7 30.4(9) . . . . ?
C2 C1 N4 P1 -55.9(7) . . . . ?
C5 C4 N5 C3 74.1(6) . . . . ?
C5 C4 N5 P1 -98.6(6) . . . . ?
C2 C3 N5 C4 124.8(6) . . . . ?
C2 C3 N5 P1 -62.1(7) . . . . ?
C9 C8 N6 C7 131.1(6) . . . . ?
C9 C8 N6 P4 -66.0(7) . . . . ?
C6 C7 N6 C8 83.0(7) . . . . ?
C6 C7 N6 P4 -78.8(6) . . . . ?
C9 C10 N7 P4 -58.3(7) . . . . ?
C1 N4 P1 N1 -90.9(5) . . . . ?
C1 N4 P1 N3 144.8(4) . . . . ?
C1 N4 P1 N5 23.8(5) . . . . ?
P2 N1 P1 N4 -120.4(3) . . . . ?
P2 N1 P1 N3 0.4(4) . . . . ?
P2 N1 P1 N5 128.2(3) . . . . ?
P3 N3 P1 N4 126.0(3) . . . . ?
P3 N3 P1 N1 -0.7(4) . . . . ?
P3 N3 P1 N5 -123.3(3) . . . . ?
C4 N5 P1 N4 -153.7(4) . . . . ?
C3 N5 P1 N4 33.7(4) . . . . ?
C4 N5 P1 N1 -32.3(5) . . . . ?
C3 N5 P1 N1 155.1(4) . . . . ?
C4 N5 P1 N3 93.1(5) . . . . ?
C3 N5 P1 N3 -79.5(4) . . . . ?
P1 N1 P2 N2 1.9(5) . . . . ?
P1 N1 P2 Cl2 124.6(3) . . . . ?
P1 N1 P2 Cl1 -122.4(3) . . . . ?
P3 N2 P2 N1 -3.9(6) . . . . ?
P3 N2 P2 Cl2 -129.2(4) . . . . ?
P3 N2 P2 Cl1 121.5(3) . . . . ?
P1 N3 P3 N2 -1.3(5) . . . . ?
P1 N3 P3 Cl3 124.7(3) . . . . ?
P1 N3 P3 Cl4 -126.3(3) . . . . ?
P2 N2 P3 N3 3.6(5) . . . . ?
P2 N2 P3 Cl3 -123.2(3) . . . . ?
P2 N2 P3 Cl4 129.9(3) . . . . ?
C10 N7 P4 N10 -92.0(5) . . . . ?
C10 N7 P4 N8 143.6(4) . . . . ?
C10 N7 P4 N6 22.0(5) . . . . ?
P6 N10 P4 N7 -134.3(3) . . . . ?
P6 N10 P4 N8 -13.2(4) . . . . ?
P6 N10 P4 N6 115.6(3) . . . . ?
P5 N8 P4 N7 136.9(3) . . . . ?
P5 N8 P4 N10 10.6(4) . . . . ?
P5 N8 P4 N6 -112.9(3) . . . . ?
C8 N6 P4 N7 39.2(5) . . . . ?
C7 N6 P4 N7 -158.5(4) . . . . ?
C8 N6 P4 N10 159.5(4) . . . . ?
C7 N6 P4 N10 -38.2(5) . . . . ?
C8 N6 P4 N8 -74.4(5) . . . . ?
C7 N6 P4 N8 88.0(5) . . . . ?
P4 N8 P5 N9 -3.1(5) . . . . ?
P4 N8 P5 Cl5 122.4(3) . . . . ?
P4 N8 P5 Cl6 -130.1(3) . . . . ?
P6 N9 P5 N8 -3.0(6) . . . . ?
P6 N9 P5 Cl5 -129.0(4) . . . . ?
P6 N9 P5 Cl6 122.7(3) . . . . ?
P4 N10 P6 N9 8.3(5) . . . . ?
P4 N10 P6 Cl8 -116.6(3) . . . . ?
P4 N10 P6 Cl7 139.5(3) . . . . ?
P5 N9 P6 N10 0.6(6) . . . . ?
P5 N9 P6 Cl8 125.8(3) . . . . ?
P5 N9 P6 Cl7 -126.4(3) . . . . ?
 
_diffrn_measured_fraction_theta_max    0.987
_diffrn_reflns_theta_full              27.41
_diffrn_measured_fraction_theta_full   0.987
_refine_diff_density_max    1.676
_refine_diff_density_min   -1.443
_refine_diff_density_rms    0.121
