(3a-Methyl-1a-trimethylsilanyl-hexahydro-4,5-diaza-cyclopropa[c]pentalen-5-yl)-phenyl-methanone

Sample Originator: Lee Patient^a.

Data Collection: Thomas Gelbrich^a

Structure Determination: Thomas Gelbrich^a.

University of Southampton^a

C₁₈H₂₆N₂OSi

InChI=1/C18H26N2OSi/c1-16-10-11-18(22(2,3)4)12-17(16,18)13-20(19-16)15(21)14-8-6-5-7-9-14/h5-9,19H,10-13H2,1-4H3

Identification Number:	10.5258/ecrystals/532
Date Created:	15 February 2001
Deposited On:	21 Jul 2008 09:10
Deposited By:	Dr Thomas Gelbrich

Data collection parameters

Chemical formula	C18 H26 N2 O Si
Crystal morphology
Crystal system	monoclinic
Space group symbol	P21/c
Cell length a	21.2704(8)
Cell length b	7.5887(2)
Cell length c	11.2915(3)
Cell angle alpha	90.00
Cell angle beta	102.2340(10)
Cell angle gamma	90.00
Data collection temperature	150(2)

Refinement results

Solution figure of merit
R Factor (Obs)	0.0490
R Factor (All)	0.0889
Weighted R Factor (Obs)	0.1003
Weighted R Factor (All)	0.1115

Citation: Gelbrich, Thomas and Patient, Lee and Hursthouse, Michael B. and Kilburn, Jeremy D. (2001) University of Southampton, Crystal Structure Report Archive. (doi:10.5258/ecrystals/532)
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Available Files

Final Result

00sot134.cif	15k
00sot134.cml	7k
s92.fcf	127k

Validation

00sot134_checkcif.htm

Processing

s92.hkl

358k

Other Files

00sot134.mol	4k
00sot134_ellipsoid.gif	20k
pics.doc	94k
s92.ins	7k

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