# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_2008sjc0013 _shelx_title ' 2008sjc0013 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 208.06 _exptl_crystal_F_000 936.00 _reflns_d_resolution_high 0.7696 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.9590 _cell_length_b 11.4830 _cell_length_c 14.0360 _cell_angle_alpha 96.445 _cell_angle_beta 111.731 _cell_angle_gamma 97.318 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1683.39 1772.00 51.27 o 3 0 0 332.74 306.42 8.07 o 4 0 0 173.63 144.16 7.01 o 5 0 0 1572.96 1691.54 29.75 o 6 0 0 5379.74 6136.79 96.17 o 7 0 0 7985.79 7639.19 141.79 o 8 0 0 6600.20 6554.01 130.16 o 9 0 0 978.54 1000.77 26.62 o 10 0 0 75.03 72.28 8.60 o 11 0 0 3.01 7.13 6.21 o 12 0 0 102.19 91.41 25.92 o 13 0 0 18.99 -61.83 91.99 o -13 1 0 1193.87 1223.09 81.69 o -12 1 0 2852.36 2783.99 144.21 o -11 1 0 1814.61 1724.46 66.35 o -10 1 0 170.19 164.16 15.71 o -9 1 0 125.72 134.07 8.34 o -8 1 0 87.46 91.43 7.55 o -7 1 0 2305.88 2311.47 42.13 o -6 1 0 10884.99 10556.52 165.69 o -5 1 0 11359.54 11299.87 173.85 o -4 1 0 7665.28 7132.28 127.50 o -3 1 0 10.66 24.23 3.57 o -2 1 0 54.47 80.99 4.47 o 2 1 0 493.34 593.64 15.23 o 3 1 0 5211.91 4212.53 87.48 o 4 1 0 424.93 314.03 8.98 o 5 1 0 1715.00 1371.05 26.58 o 6 1 0 4066.64 3938.25 73.69 o 7 1 0 3528.68 3479.57 75.02 o 8 1 0 277.70 268.79 11.55 o 9 1 0 103.20 95.25 8.79 o 10 1 0 35.12 28.27 20.80 o 11 1 0 115.39 87.33 12.88 o 12 1 0 103.02 71.17 13.44 o -13 2 0 2.35 8.65 19.11 o -12 2 0 674.97 581.28 36.39 o -11 2 0 2279.69 2126.53 69.56 o -10 2 0 83.71 83.38 7.48 o -9 2 0 1355.46 1499.78 40.40 o -8 2 0 3777.48 3779.23 79.65 o -7 2 0 6138.47 6887.39 117.76 o -6 2 0 1474.55 1430.47 25.90 o -5 2 0 766.72 842.73 18.14 o -4 2 0 75.95 125.00 7.10 o -3 2 0 2601.14 2349.54 44.02 o -2 2 0 14999.30 15685.04 359.51 o -1 2 0 13146.52 13682.04 349.95 o 0 2 0 3620.06 3893.22 174.89 o 1 2 0 43013.29 37994.18 1239.98 o 2 2 0 23252.63 20964.09 512.27 o 3 2 0 238.74 182.17 7.55 o 4 2 0 868.35 789.76 16.75 o 5 2 0 7227.09 7516.28 141.81 o 6 2 0 3458.83 3294.39 62.29 o 7 2 0 3087.28 2871.18 54.65 o 8 2 0 4280.23 4284.01 107.54 o 9 2 0 5119.58 5131.93 149.00 o 10 2 0 1712.40 1636.20 51.12 o 11 2 0 81.87 49.17 9.61 o 12 2 0 0.07 -3.34 41.01 o -13 3 0 1914.66 1912.68 109.64 o -12 3 0 1111.49 1086.65 57.01 o -11 3 0 434.13 434.58 27.77 o -10 3 0 1046.84 1106.95 34.82 o -9 3 0 182.59 215.36 10.06 o -8 3 0 325.78 338.40 12.47 o -7 3 0 3338.04 3346.88 56.09 o -6 3 0 11623.50 11806.28 177.63 o -5 3 0 12957.30 13878.33 208.04 o -4 3 0 8480.14 8898.77 141.84 o -3 3 0 6071.13 5528.23 137.48 o -2 3 0 3803.76 4178.45 101.88 o -1 3 0 172.84 192.85 11.98 o 0 3 0 292.97 248.41 11.17 o 1 3 0 9992.29 9262.34 436.65 o 2 3 0 13475.61 12434.77 380.49 o 3 3 0 2700.84 2658.00 62.41 o 4 3 0 14881.42 14468.58 291.63 o 5 3 0 2017.86 1853.01 39.42 o 6 3 0 540.07 579.25 15.76 o 7 3 0 574.52 580.85 24.58 o 8 3 0 1897.54 2015.18 54.73 o 9 3 0 534.98 550.28 21.65 o 10 3 0 608.50 532.89 27.32 o 11 3 0 124.29 146.61 27.55 o 12 3 0 35.48 10.90 52.62 o -13 4 0 1.98 -9.93 14.89 o -12 4 0 616.96 588.45 37.67 o -11 4 0 349.41 296.58 18.65 o -10 4 0 1858.94 1825.58 57.39 o -9 4 0 1155.80 1171.56 31.29 o -8 4 0 372.75 343.36 13.32 o -7 4 0 622.87 591.30 18.85 o -6 4 0 4594.68 4797.87 78.29 o -5 4 0 1291.07 1331.36 26.13 o -4 4 0 0.74 19.73 7.15 o -3 4 0 278.65 252.90 8.99 o -2 4 0 3024.66 2729.84 62.55 o -1 4 0 27.84 15.32 7.51 o 0 4 0 3200.46 2970.86 89.17 o 1 4 0 17953.20 18098.97 526.18 o 2 4 0 1967.90 2036.10 55.73 o 3 4 0 11106.28 11729.45 289.19 o 4 4 0 1688.94 1575.11 48.18 o 5 4 0 2878.84 2919.58 60.70 o 6 4 0 221.42 229.42 12.15 o 7 4 0 3870.81 4016.95 98.07 o 8 4 0 4009.51 4047.47 117.20 o 9 4 0 2049.59 2134.96 70.89 o 10 4 0 550.53 513.49 37.21 o 11 4 0 432.17 491.44 35.03 o -13 5 0 521.22 425.17 43.57 o -12 5 0 1127.59 1121.27 62.19 o -11 5 0 1460.54 1355.22 54.28 o -10 5 0 721.08 721.20 27.37 o -9 5 0 994.85 1006.47 30.40 o -8 5 0 0.16 19.58 7.25 o -7 5 0 716.48 808.40 22.89 o -6 5 0 26.27 53.05 7.35 o -5 5 0 22950.55 23024.61 407.04 o -4 5 0 19665.36 20261.96 357.80 o -3 5 0 17479.03 17008.56 349.84 o -2 5 0 579.73 472.59 13.53 o -1 5 0 1099.11 1123.91 30.54 o 0 5 0 49.23 33.55 9.10 o 1 5 0 3.27 -3.94 6.23 o 2 5 0 3898.76 3831.37 118.63 o 3 5 0 18139.40 18375.91 440.16 o 4 5 0 3441.99 3376.86 73.47 o 5 5 0 1924.26 1857.16 42.32 o 6 5 0 73.65 58.72 10.02 o 7 5 0 121.74 90.30 10.05 o 8 5 0 3.62 2.74 6.55 o 9 5 0 46.80 44.17 7.43 o 10 5 0 1038.55 1020.91 75.00 o 11 5 0 757.06 597.32 56.45 o -12 6 0 79.33 57.81 18.88 o -11 6 0 561.10 624.55 57.72 o -10 6 0 2224.26 2283.97 74.33 o -9 6 0 3192.76 3336.92 96.30 o -8 6 0 1388.71 1430.45 36.46 o -7 6 0 0.04 -0.36 7.18 o -6 6 0 1656.95 1769.93 34.66 o -5 6 0 2492.33 2638.42 48.60 o -4 6 0 3967.03 4214.59 73.25 o -3 6 0 6306.41 6610.98 125.93 o -2 6 0 265.06 184.55 15.23 o -1 6 0 8.42 9.28 8.39 o 0 6 0 435.34 494.30 26.60 o 1 6 0 7668.46 7889.92 216.77 o 2 6 0 7092.87 7135.23 191.94 o 3 6 0 266.15 399.25 18.86 o 4 6 0 2276.53 2266.67 53.98 o 5 6 0 2.61 16.75 9.29 o 6 6 0 632.12 725.09 25.77 o 7 6 0 489.35 462.93 20.97 o 8 6 0 52.42 41.33 9.33 o 9 6 0 1387.60 1428.27 71.94 o 10 6 0 848.32 760.67 46.28 o -12 7 0 672.32 684.56 56.39 o -11 7 0 2080.86 2164.56 151.65 o -10 7 0 1473.08 1460.47 70.24 o -9 7 0 7.06 -8.39 7.82 o -8 7 0 656.30 647.03 26.19 o -7 7 0 15.77 6.01 8.49 o -6 7 0 3199.25 3408.94 69.23 o -5 7 0 2877.05 2883.69 53.65 o -4 7 0 11705.05 12235.68 229.45 o -3 7 0 4988.22 5307.32 113.25 o -2 7 0 6771.49 6504.04 144.79 o -1 7 0 178.92 207.66 11.89 o 0 7 0 50.64 41.71 11.46 o 1 7 0 759.85 759.74 28.02 o 2 7 0 1659.01 1866.39 53.13 o 3 7 0 4236.67 4422.40 123.15 o 4 7 0 8080.14 8379.27 221.89 o 5 7 0 910.70 1036.47 35.01 o 6 7 0 6.84 23.78 9.84 o 7 7 0 237.91 230.54 14.06 o 8 7 0 405.29 454.74 25.76 o 9 7 0 65.41 36.54 37.74 o 10 7 0 441.30 360.77 34.90 o -12 8 0 28.86 39.34 17.80 o -11 8 0 1675.68 1708.18 105.93 o -10 8 0 941.97 932.27 53.84 o -9 8 0 1934.90 2093.96 92.49 o -8 8 0 896.27 979.95 38.13 o -7 8 0 15.74 26.95 8.80 o -6 8 0 7.48 18.75 8.69 o -5 8 0 871.10 881.68 27.67 o -4 8 0 219.07 274.48 17.00 o -3 8 0 1224.95 1261.06 44.56 o -2 8 0 9941.40 10530.67 225.56 o -1 8 0 3113.07 3264.16 83.36 o 0 8 0 62.36 71.85 10.68 o 1 8 0 196.89 212.69 16.90 o 2 8 0 293.72 282.61 19.46 o 3 8 0 2731.70 2818.95 91.20 o 4 8 0 474.60 478.44 22.36 o 5 8 0 109.13 100.49 11.32 o 6 8 0 1978.59 1954.40 67.11 o 7 8 0 14.77 15.24 12.78 o 8 8 0 356.08 329.44 31.18 o 9 8 0 25.53 -8.97 27.82 o -11 9 0 359.37 355.91 43.36 o -10 9 0 114.65 95.79 19.17 o -9 9 0 226.65 239.43 17.64 o -8 9 0 0.18 12.10 11.70 o -7 9 0 9.57 8.84 9.29 o -6 9 0 142.48 137.23 12.11 o -5 9 0 1217.67 1224.89 46.52 o -4 9 0 3146.08 3141.93 89.37 o -3 9 0 1744.32 1915.19 63.91 o -2 9 0 1156.96 1108.22 39.20 o -1 9 0 2091.49 2000.91 58.01 o 0 9 0 81.12 64.79 12.07 o 1 9 0 528.32 497.35 42.20 o 2 9 0 1656.43 1632.98 67.02 o 3 9 0 3639.30 3763.16 124.19 o 4 9 0 4706.16 4835.92 177.72 o 5 9 0 3050.39 3133.98 123.90 o 6 9 0 1939.65 2155.73 80.89 o 7 9 0 51.71 42.42 18.52 o 8 9 0 252.97 201.24 27.97 o -11 10 0 262.87 317.26 42.88 o -10 10 0 3358.26 3349.15 183.72 o -9 10 0 3325.05 3450.47 140.23 o -8 10 0 2185.50 2227.83 105.71 o -7 10 0 794.63 765.01 33.01 o -6 10 0 1340.45 1331.21 52.62 o -5 10 0 55.99 73.39 11.10 o -4 10 0 147.07 216.23 18.56 o -3 10 0 501.41 545.32 27.80 o -2 10 0 1746.41 1881.05 66.73 o -1 10 0 4643.92 5025.26 127.61 o 0 10 0 6134.28 6223.40 201.46 o 1 10 0 61.79 46.50 40.66 o 2 10 0 518.38 512.39 35.67 o 3 10 0 25.43 46.87 15.18 o 4 10 0 141.25 139.84 17.17 o 5 10 0 209.29 199.58 20.32 o 6 10 0 250.13 236.67 42.15 o 7 10 0 793.82 906.15 59.27 o -10 11 0 1297.71 1144.82 64.74 o -9 11 0 53.67 48.03 14.36 o -8 11 0 490.42 507.71 28.65 o -7 11 0 958.88 934.31 82.89 o -6 11 0 597.74 511.92 32.44 o -5 11 0 280.11 328.21 35.99 o -4 11 0 1207.23 1172.30 55.31 o -3 11 0 9554.38 9778.06 330.79 o -2 11 0 2777.04 2767.86 86.96 o -1 11 0 150.81 142.10 17.16 o 0 11 0 31.94 24.16 12.61 o 1 11 0 101.67 59.09 40.75 o 2 11 0 33.28 28.56 13.75 o 3 11 0 28.76 22.92 13.55 o 4 11 0 1185.18 1168.17 68.00 o 5 11 0 2800.43 3114.75 226.92 o 6 11 0 502.81 573.89 51.02 o -9 12 0 1711.52 1824.62 140.92 o -8 12 0 2548.21 2307.54 203.62 o -7 12 0 1188.74 1125.54 71.78 o -6 12 0 62.17 80.71 20.38 o -5 12 0 408.41 288.24 36.86 o -4 12 0 72.83 38.18 31.00 o -3 12 0 396.04 390.28 38.81 o -2 12 0 2279.14 2049.93 133.11 o -1 12 0 3967.55 4028.51 207.45 o 0 12 0 2324.52 2372.76 122.77 o 1 12 0 1505.03 1558.86 83.27 o 2 12 0 166.20 207.79 29.13 o 3 12 0 1.87 36.24 18.63 o 4 12 0 33.18 7.48 14.22 o 5 12 0 429.69 468.87 60.70 o -8 13 0 56.20 25.32 78.24 o -7 13 0 1901.34 1889.63 178.25 o -6 13 0 3347.22 2980.70 303.68 o -5 13 0 706.63 573.18 45.76 o -4 13 0 3.93 7.57 20.29 o -3 13 0 15.25 51.12 24.88 o -2 13 0 449.33 502.19 44.66 o -1 13 0 415.72 427.83 37.90 o 0 13 0 11.23 -12.33 24.63 o 1 13 0 957.74 1084.01 82.68 o 2 13 0 235.13 245.58 48.38 o 3 13 0 83.01 124.40 29.26 o 4 13 0 1.72 33.01 26.21 o -6 14 0 480.58 441.05 51.42 o -5 14 0 36.77 54.28 31.96 o -4 14 0 2.07 3.92 29.49 o -3 14 0 6.91 64.46 40.39 o -2 14 0 471.16 544.81 76.27 o -1 14 0 1418.32 1378.96 124.52 o 0 14 0 2097.59 1980.49 187.20 o 1 14 0 1645.73 1764.41 113.78 o -2 -14 1 17.44 45.86 31.84 o -1 -14 1 134.40 140.98 119.25 o 0 -14 1 0.12 35.99 36.66 o 1 -14 1 0.00 53.09 54.93 o 2 -14 1 0.44 0.89 23.16 o 3 -14 1 1655.01 1757.90 173.07 o 4 -14 1 2056.30 1988.32 150.01 o 5 -14 1 42.92 -29.32 68.54 o 6 -14 1 484.69 356.70 67.10 o -4 -13 1 181.15 237.22 41.18 o -3 -13 1 27.43 70.56 28.05 o -2 -13 1 134.08 109.97 23.89 o -1 -13 1 0.15 -9.30 25.48 o 0 -13 1 416.67 422.81 49.20 o 1 -13 1 2053.12 1950.08 184.60 o 2 -13 1 2682.99 2826.14 147.80 o 3 -13 1 1964.04 2015.38 159.70 o 4 -13 1 151.94 119.64 34.82 o 5 -13 1 2.58 76.71 90.01 o 6 -13 1 13.88 39.43 21.58 o 7 -13 1 152.78 79.78 44.17 o 8 -13 1 772.34 757.85 112.88 o -6 -12 1 776.67 782.51 112.58 o -5 -12 1 1231.07 1190.28 129.40 o -4 -12 1 689.52 752.92 63.85 o -3 -12 1 1956.71 2054.25 112.99 o -2 -12 1 3084.00 3042.99 202.34 o -1 -12 1 101.75 78.68 25.26 o 0 -12 1 545.95 433.84 67.22 o 1 -12 1 57.42 52.75 18.66 o 2 -12 1 2152.10 2149.25 121.41 o 3 -12 1 798.91 771.50 64.11 o 4 -12 1 222.62 319.52 48.76 o 5 -12 1 1198.70 1132.22 70.85 o 6 -12 1 1156.97 1066.05 80.77 o 7 -12 1 99.73 130.67 40.95 o 8 -12 1 195.17 145.50 34.94 o 9 -12 1 127.93 113.33 25.02 o -7 -11 1 84.35 104.64 27.89 o -6 -11 1 159.93 81.53 22.64 o -5 -11 1 612.14 527.36 35.50 o -4 -11 1 0.46 -9.56 13.78 o -3 -11 1 33.52 3.22 11.50 o -2 -11 1 787.31 767.54 48.40 o -1 -11 1 428.95 437.10 49.02 o 0 -11 1 1.28 13.63 14.49 o 1 -11 1 3066.03 3086.56 118.36 o 2 -11 1 948.98 878.25 44.21 o 3 -11 1 1462.93 1491.69 61.16 o 4 -11 1 353.71 412.88 33.40 o 5 -11 1 70.90 85.45 19.23 o 6 -11 1 139.06 117.46 17.55 o 7 -11 1 19.76 -8.10 23.73 o 8 -11 1 150.67 211.18 24.54 o 9 -11 1 1697.85 1663.45 86.41 o 10 -11 1 2164.11 2349.91 155.90 o -8 -10 1 250.68 308.42 60.10 o -7 -10 1 204.51 222.02 29.83 o -6 -10 1 36.25 64.45 17.75 o -5 -10 1 131.89 137.11 19.96 o -4 -10 1 2406.00 2592.45 113.62 o -3 -10 1 3313.44 3646.60 135.01 o -2 -10 1 3167.05 3309.68 124.48 o -1 -10 1 6436.06 6547.35 230.79 o 0 -10 1 2523.57 2476.74 82.63 o 1 -10 1 123.82 158.19 14.21 o 2 -10 1 316.42 305.22 18.52 o 3 -10 1 1362.88 1347.00 58.73 o 4 -10 1 14105.05 15223.14 422.34 o 5 -10 1 6061.66 6142.71 210.55 o 6 -10 1 897.36 944.09 39.56 o 7 -10 1 336.95 314.26 21.89 o 8 -10 1 170.78 130.44 22.98 o 9 -10 1 1166.22 1139.66 61.69 o 10 -10 1 126.36 81.14 17.33 o -9 -9 1 1119.89 1143.93 99.20 o -8 -9 1 2696.49 2946.94 163.72 o -7 -9 1 219.02 183.51 18.78 o -6 -9 1 314.03 311.25 20.82 o -5 -9 1 344.79 285.08 33.19 o -4 -9 1 20.70 40.11 10.22 o -3 -9 1 313.08 303.93 23.33 o -2 -9 1 911.66 830.33 57.50 o -1 -9 1 3589.08 3981.38 125.09 o 0 -9 1 1787.83 1857.01 54.24 o 1 -9 1 302.04 324.12 28.37 o 2 -9 1 2409.90 2285.54 66.63 o 3 -9 1 1001.29 962.31 35.39 o 4 -9 1 1239.33 1283.00 54.00 o 5 -9 1 1240.96 1332.00 40.70 o 6 -9 1 11.24 4.29 7.83 o 7 -9 1 862.93 948.86 35.00 o 8 -9 1 88.76 144.04 17.14 o 9 -9 1 672.72 634.86 36.43 o 10 -9 1 1705.58 1714.18 91.96 o 11 -9 1 871.22 846.88 74.63 o -9 -8 1 772.96 760.13 65.04 o -8 -8 1 187.36 179.44 18.42 o -7 -8 1 183.24 189.31 16.82 o -6 -8 1 5.33 -3.29 9.33 o -5 -8 1 290.73 274.05 15.78 o -4 -8 1 3773.16 3769.10 99.29 o -3 -8 1 5065.28 5308.13 150.17 o -2 -8 1 10831.10 10224.74 314.85 o -1 -8 1 1265.34 1330.31 49.83 o 0 -8 1 50.02 36.42 11.81 o 1 -8 1 24.82 16.12 9.75 o 2 -8 1 407.71 458.28 27.02 o 3 -8 1 1737.47 1686.64 44.95 o 4 -8 1 3345.28 3312.31 66.91 o 5 -8 1 12004.15 12799.91 264.43 o 6 -8 1 10509.08 10996.63 249.68 o 7 -8 1 279.85 324.13 18.93 o 8 -8 1 40.64 52.59 10.60 o 9 -8 1 504.66 547.38 28.43 o 10 -8 1 464.14 457.59 28.89 o 11 -8 1 54.01 68.08 19.39 o -10 -7 1 1432.52 1402.14 101.92 o -9 -7 1 1137.49 1041.46 65.24 o -8 -7 1 1155.64 1249.96 61.89 o -7 -7 1 4827.90 5050.59 150.23 o -6 -7 1 5083.24 5300.40 167.05 o -5 -7 1 25.43 18.72 9.66 o -4 -7 1 140.06 115.92 10.62 o -3 -7 1 3860.23 3874.20 113.11 o -2 -7 1 1293.04 1446.36 45.00 o -1 -7 1 7813.22 7623.45 280.68 o 0 -7 1 4319.42 4279.75 103.19 o 1 -7 1 4642.00 4635.71 122.53 o 2 -7 1 347.89 398.90 15.64 o 3 -7 1 8.28 4.03 11.02 o 4 -7 1 372.09 337.41 17.84 o 5 -7 1 725.49 743.79 23.12 o 6 -7 1 2086.51 2262.64 49.93 o 7 -7 1 90.43 113.73 9.85 o 8 -7 1 2644.07 2899.40 84.09 o 9 -7 1 169.23 189.78 19.72 o 10 -7 1 571.21 508.99 28.35 o 11 -7 1 1281.05 1297.35 91.15 o 12 -7 1 792.43 802.45 98.31 o -11 -6 1 0.16 11.24 15.34 o -10 -6 1 585.86 585.08 44.03 o -9 -6 1 342.71 307.92 32.70 o -8 -6 1 0.20 7.79 6.25 o -7 -6 1 1006.68 931.32 33.60 o -6 -6 1 2098.59 2188.75 57.74 o -5 -6 1 1809.97 1804.56 48.46 o -4 -6 1 1621.72 1661.16 38.37 o -3 -6 1 7161.60 6735.81 172.54 o -2 -6 1 5118.97 5054.14 129.99 o -1 -6 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