(4,4,6,6-tetrachloro-2-[(2,4-dimethylphenyl)thio]-N-[4-(2,2,4,4- tetrachloro-1,3,5,7,11-pentaaza-2λ5,4λ5,6λ5-triphosphaspiro[5.5] undeca-1,3,5-trien-7-yl)butyl]-1,3,5,2λ5,4λ5,6λ5- triazatriphosphinin-2-amine

Sample Originator: R. A. Shawa, David B. Daviesa, A. Kilicb and H Ibisoglub.

Data Collection: Simon J. Colesc

Structure Determination: Simon J. Colesc and Michael B. Hursthouse.

Birkbeck College, University of Londona
Gebze Institute of Technologyb
University of Southamptonc



Identification Number:10.5258/ecrystals/336
Date Created:21 November 2000
Deposited On:21 Jan 2008 15:30
Deposited By:Dr Simon J Coles

Depositor Comments

To be submitted to Acta E

Data collection parameters

Chemical formulaC15 H25 Cl8 N9 P6 S
Crystal morphology
Crystal systemOrthorhombic
Space group symbolP2(1)2(1)2(1)
Cell length a8.5829(17)
Cell length b15.587(3)
Cell length c25.277(5)
Cell angle alpha90.00
Cell angle beta90.00
Cell angle gamma90.00
Data collection temperature120(2)

Refinement results

Solution figure of merit0.0486
R Factor (Obs)0.0453
R Factor (All)0.0665
Weighted R Factor (Obs)0.1003
Weighted R Factor (All)0.1127

Citation: Shaw, R. A. and Davies, David B. and Kilic, A. and Ibisoglu, H and Coles, Simon J. and Hursthouse, Michael B. (2000) University of Southampton, Crystal Structure Report Archive. (doi:10.5258/ecrystals/336)
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