# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_s92 _shelx_title ' 03src0086 in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 376.64 _exptl_crystal_F_000 2088.00 _reflns_d_resolution_high 0.8107 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 30.5860 _cell_length_b 9.6595 _cell_length_c 18.4491 _cell_angle_alpha 90.000 _cell_angle_beta 94.599 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 5 0 0 204.39 97.12 48.56 o 6 0 0 548.92 918.30 194.47 o 7 0 0 1660.54 1504.00 170.43 o 8 0 0 14526.83 9973.06 831.19 o 9 0 0 392.80 501.70 170.67 o 10 0 0 4141.26 4653.51 463.94 o 11 0 0 16106.84 12183.17 1930.28 o 12 0 0 1174.12 805.49 220.19 o 13 0 0 944.25 683.94 122.36 o 14 0 0 1893.59 1793.40 139.38 o 15 0 0 1460.58 1566.15 171.63 o 16 0 0 25.78 49.28 104.37 o 17 0 0 12.24 196.79 104.54 o 18 0 0 2608.87 1942.95 443.03 o 19 0 0 2143.53 2791.40 616.10 o 20 0 0 1441.09 1087.50 198.08 o 21 0 0 791.34 544.71 198.08 o 22 0 0 14559.31 15166.79 950.96 o 23 0 0 460.81 546.15 248.08 o 24 0 0 4182.36 4074.99 399.04 o 25 0 0 135.21 -99.52 199.04 o 26 0 0 9849.96 10510.07 1001.44 o 27 0 0 395.83 498.56 199.52 o 28 0 0 328.93 50.00 199.52 o 29 0 0 21.21 349.52 200.00 o 30 0 0 266.40 100.00 200.00 o 31 0 0 150.06 50.00 200.00 o 32 0 0 169.25 50.00 200.48 o 33 0 0 46.99 0.00 200.48 o 36 0 0 18.41 250.96 300.96 o 37 0 0 60.87 300.96 200.96 o 3 1 0 14886.96 12603.34 1285.57 o 4 1 0 195.38 183.45 31.46 o 5 1 0 19010.86 22887.02 1560.53 o 6 1 0 381.65 225.44 80.05 o 7 1 0 8092.77 9495.65 695.02 o 8 1 0 152.55 214.54 70.74 o 9 1 0 19487.92 16295.63 1008.67 o 10 1 0 0.82 81.09 63.70 o 11 1 0 3776.53 3136.95 211.01 o 12 1 0 281.65 130.71 66.50 o 13 1 0 2702.94 2837.71 180.64 o 14 1 0 977.14 808.37 86.03 o 15 1 0 329.65 308.43 74.09 o 16 1 0 6280.00 6454.85 324.05 o 17 1 0 322.87 479.10 132.54 o 18 1 0 1177.82 1520.28 112.92 o 19 1 0 213.24 148.60 85.76 o 20 1 0 797.36 1037.22 139.88 o 21 1 0 5461.63 6003.17 332.35 o 22 1 0 1385.76 1436.32 175.07 o 23 1 0 263.22 418.84 295.19 o 24 1 0 27.01 154.16 154.89 o 25 1 0 8498.51 9624.65 907.45 o 26 1 0 0.90 120.61 198.32 o 27 1 0 429.18 472.42 272.11 o 28 1 0 16.31 -99.52 140.74 o 29 1 0 153.00 94.10 155.59 o 30 1 0 45.31 332.55 155.94 o 31 1 0 281.05 244.11 274.04 o 32 1 0 137.65 210.96 155.94 o 33 1 0 611.54 250.00 300.00 o 34 1 0 35.00 -33.33 156.17 o 35 1 0 178.39 200.48 250.48 o 36 1 0 5.69 -300.48 250.48 o 37 1 0 49.74 600.96 300.48 o 0 2 0 7837.65 7330.34 373.86 o 1 2 0 34049.13 39328.24 1528.98 o 2 2 0 7735.27 6990.59 307.80 o 3 2 0 23075.51 20379.94 902.77 o 4 2 0 1447.04 1217.89 61.14 o 5 2 0 168.89 235.00 53.75 o 6 2 0 3418.51 3236.76 208.79 o 7 2 0 2013.86 2136.91 294.71 o 8 2 0 12604.77 12590.84 1375.48 o 9 2 0 352.40 48.56 97.60 o 10 2 0 15142.37 12328.55 917.75 o 11 2 0 1684.89 1646.43 260.34 o 12 2 0 17811.10 18167.02 1360.98 o 13 2 0 2318.52 1239.33 156.37 o 14 2 0 10127.49 8610.52 541.79 o 15 2 0 257.65 579.87 159.37 o 16 2 0 0.34 65.53 124.84 o 17 2 0 203.72 347.76 86.01 o 18 2 0 758.42 421.01 129.18 o 19 2 0 64.57 0.00 146.15 o 20 2 0 547.83 828.76 361.30 o 21 2 0 102.38 123.10 104.52 o 22 2 0 163.71 394.43 139.36 o 23 2 0 1965.45 2452.87 225.34 o 24 2 0 1622.39 1892.03 225.14 o 25 2 0 370.54 842.10 174.55 o 26 2 0 27.07 253.45 269.71 o 27 2 0 386.96 123.51 174.73 o 28 2 0 460.18 420.09 175.00 o 29 2 0 51.56 222.69 223.56 o 30 2 0 243.17 38.73 321.63 o 31 2 0 50.39 214.88 155.01 o 32 2 0 7.75 -149.04 248.56 o 33 2 0 0.00 184.36 122.24 o 34 2 0 275.98 746.63 298.56 o 35 2 0 2.51 298.56 249.04 o 36 2 0 14.55 249.04 348.56 o 37 2 0 1.09 14.48 167.80 o 1 3 0 77.41 114.62 37.87 o 2 3 0 16513.71 15915.36 722.81 o 3 3 0 748.90 853.84 150.96 o 4 3 0 313.99 150.48 100.48 o 8 3 0 3577.72 3293.74 395.19 o 9 3 0 4889.43 4344.69 314.12 o 10 3 0 372.79 -9.84 172.84 o 11 3 0 713.55 883.49 119.52 o 12 3 0 4806.97 5654.46 422.90 o 13 3 0 5549.68 4648.71 383.17 o 14 3 0 1822.62 2162.81 210.99 o 15 3 0 596.14 648.28 119.78 o 16 3 0 949.56 579.74 119.43 o 17 3 0 1059.50 897.38 155.87 o 18 3 0 62.10 130.23 195.67 o 19 3 0 44.05 121.87 170.91 o 20 3 0 521.73 696.60 138.02 o 21 3 0 406.48 292.31 116.99 o 22 3 0 966.54 1422.53 187.20 o 23 3 0 195.02 263.18 134.46 o 24 3 0 1001.32 1222.35 214.68 o 25 3 0 3.51 49.00 115.48 o 26 3 0 1055.17 995.60 149.39 o 27 3 0 233.98 154.21 120.77 o 28 3 0 394.50 621.15 141.65 o 29 3 0 3.29 203.85 130.18 o 30 3 0 22.09 320.80 149.63 o 31 3 0 33.98 24.57 174.05 o 32 3 0 57.06 -99.04 197.60 o 33 3 0 17.94 -49.52 247.11 o 34 3 0 117.74 374.30 191.22 o 35 3 0 23.48 184.20 136.82 o 36 3 0 12.87 692.79 346.63 o 1 4 0 20169.53 22592.74 2212.01 o 11 4 0 1122.38 1049.04 200.00 o 12 4 0 396.77 561.70 76.03 o 13 4 0 65.98 -24.84 105.36 o 14 4 0 124.07 -49.51 148.56 o 15 4 0 249.24 285.87 45.41 o 16 4 0 1361.04 1129.73 100.96 o 18 4 0 2.05 -98.56 148.08 o 19 4 0 1149.39 714.56 139.38 o 20 4 0 1.65 49.04 139.04 o 21 4 0 684.06 1045.13 188.36 o 22 4 0 36.49 65.15 152.82 o 23 4 0 2505.07 2750.52 305.53 o 24 4 0 34.60 22.28 112.74 o 25 4 0 282.37 436.39 251.08 o 26 4 0 25.12 226.36 129.95 o 27 4 0 430.13 358.99 141.27 o 28 4 0 43.73 110.33 250.49 o 29 4 0 124.67 308.38 166.29 o 30 4 0 79.05 84.91 188.41 o 31 4 0 335.66 240.81 188.41 o 32 4 0 15.73 49.04 246.15 o 33 4 0 22.01 442.79 295.19 o 34 4 0 68.04 0.00 246.15 o 35 4 0 132.67 344.23 295.19 o 12 5 0 345.39 700.48 150.00 o 13 5 0 377.85 0.00 150.48 o 19 5 0 1059.94 1155.12 191.24 o 20 5 0 458.15 892.79 248.08 o 21 5 0 608.62 1123.88 209.92 o 22 5 0 713.33 974.06 209.41 o 23 5 0 219.58 411.56 189.05 o 24 5 0 514.70 1148.14 208.39 o 25 5 0 118.77 274.21 162.93 o 26 5 0 97.31 231.45 149.78 o 27 5 0 5.75 73.67 173.87 o 28 5 0 0.53 216.19 163.79 o 29 5 0 142.13 217.23 158.57 o 30 5 0 10.20 0.00 197.11 o 31 5 0 24.17 -98.56 245.67 o 32 5 0 226.82 244.95 207.71 o 33 5 0 254.83 122.30 207.88 o 34 5 0 23.31 116.40 269.71 o 18 6 0 377.59 452.40 251.44 o 19 6 0 0.05 -31.90 192.87 o 20 6 0 43.85 125.48 375.48 o 21 6 0 21.19 190.77 191.93 o 22 6 0 28.91 -45.26 224.04 o 23 6 0 14.65 189.23 372.35 o 24 6 0 166.46 445.43 197.84 o 26 6 0 40.63 114.89 153.86 o 27 6 0 2.93 -368.51 245.67 o 28 6 0 3.18 109.71 154.31 o 29 6 0 17.21 -49.52 198.08 o 30 6 0 146.81 -246.63 197.60 o 31 6 0 47.02 -70.61 152.82 o 32 6 0 24.38 24.52 138.36 o 20 7 0 297.56 453.56 178.31 o 21 7 0 36.66 351.71 226.44 o 22 7 0 106.88 401.20 177.29 o 23 7 0 75.52 100.00 300.00 o 24 7 0 2.74 -22.74 191.58 o 25 7 0 20.41 248.56 155.36 o 29 7 0 17.05 -21.78 153.63 o 30 7 0 0.40 319.47 173.72 o 20 8 0 24.82 -101.08 71.56 o 21 8 0 1.12 0.00 84.00 o 22 8 0 1.73 0.00 125.96 o 23 8 0 33.85 130.50 83.65 o 24 8 0 70.22 10.08 83.29 o 26 8 0 30.39 0.00 199.52 o 18 9 0 0.08 0.00 101.44 o 19 9 0 23.70 220.00 90.78 o 20 9 0 109.43 -20.37 84.45 o 21 9 0 0.19 60.65 84.09 o 22 9 0 26.26 50.48 151.44 o 23 9 0 2.29 100.96 151.44 o 24 9 0 69.92 150.96 200.96 o 19 10 0 16.68 50.96 152.88 o 20 10 0 2.68 -101.92 152.40 o -37 1 1 3.84 0.00 250.00 o -36 1 1 15.13 -49.90 176.44 o -35 1 1 42.64 408.19 173.47 o -34 1 1 510.82 689.98 227.03 o -33 1 1 2.53 0.00 198.56 o -32 1 1 918.44 1396.15 299.52 o -31 1 1 232.75 39.99 173.80 o -30 1 1 1.02 -74.46 140.40 o -29 1 1 87.25 -24.94 140.40 o -28 1 1 4.16 -82.50 154.68 o -27 1 1 50.47 -74.10 222.60 o -26 1 1 21.00 -24.61 173.32 o -25 1 1 1072.93 997.89 174.90 o -24 1 1 4.73 35.33 118.35 o -23 1 1 55.38 -98.56 104.70 o -22 1 1 392.76 302.92 118.43 o -21 1 1 2169.66 2200.55 189.79 o -20 1 1 808.42 519.48 114.08 o -19 1 1 206.87 315.74 78.48 o -18 1 1 855.57 817.66 90.29 o -17 1 1 5.41 115.18 64.59 o -16 1 1 261.49 29.57 76.89 o -15 1 1 46.64 153.56 64.69 o -14 1 1 7.16 184.19 80.93 o -13 1 1 120.27 398.60 80.78 o -12 1 1 1234.05 1309.51 130.68 o -11 1 1 98.05 92.72 72.61 o -10 1 1 1197.07 1140.11 117.67 o -9 1 1 455.39 183.84 62.73 o -8 1 1 4843.68 6209.84 387.07 o -7 1 1 40667.42 34686.20 2841.04 o -6 1 1 141854.33 134495.86 15648.04 o -5 1 1 73962.34 77667.13 8423.54 o -4 1 1 4967.26 3364.20 150.71 o -3 1 1 6082.28 6421.62 581.82 o 3 1 1 7272.13 5173.54 474.23 o 4 1 1 2344.10 1390.02 103.02 o 5 1 1 25960.90 25995.67 1996.10 o 6 1 1 33111.66 27603.73 2253.70 o 7 1 1 82853.54 74531.80 6026.92 o 8 1 1 1253.79 1547.10 124.50 o 9 1 1 5228.18 4088.74 288.12 o 10 1 1 73.95 131.41 64.35 o 11 1 1 109.28 112.47 64.11 o 12 1 1 244.82 1016.18 93.66 o 13 1 1 941.76 1025.32 84.40 o 14 1 1 959.44 442.58 85.01 o 15 1 1 1855.85 2103.20 200.06 o 16 1 1 952.97 770.30 78.61 o 17 1 1 811.30 694.40 169.37 o 18 1 1 258.03 84.25 78.55 o 19 1 1 42.25 268.86 195.19 o 20 1 1 625.91 1272.36 387.50 o 21 1 1 1206.74 1525.28 336.06 o 22 1 1 1941.19 2065.98 175.75 o 23 1 1 242.65 156.02 118.91 o 24 1 1 1.97 -24.88 140.74 o 25 1 1 7.03 -49.64 140.91 o 26 1 1 425.82 348.79 198.08 o 27 1 1 0.20 -49.88 141.08 o 28 1 1 108.68 349.70 141.25 o 29 1 1 505.85 566.45 156.28 o 30 1 1 54.32 100.00 200.48 o 31 1 1 1.74 222.73 250.24 o 32 1 1 87.62 400.96 250.48 o 33 1 1 460.19 799.64 192.74 o 34 1 1 14.50 -200.48 200.48 o 35 1 1 140.88 701.92 250.96 o 36 1 1 1.16 100.29 177.46 o 37 1 1 0.11 -200.96 251.44 o -37 2 1 90.05 -99.40 210.94 o -36 2 1 16.39 130.04 160.44 o -35 2 1 12.56 153.44 190.86 o -34 2 1 303.78 49.76 175.41 o -33 2 1 1322.74 1044.71 298.56 o -32 2 1 18.99 277.99 126.57 o -31 2 1 160.14 144.23 130.68 o -30 2 1 150.67 -16.58 154.21 o -29 2 1 98.54 276.98 220.43 o -28 2 1 169.16 411.04 153.87 o -27 2 1 507.42 786.38 154.31 o -26 2 1 48.43 221.83 269.71 o -25 2 1 528.10 320.11 139.37 o -24 2 1 281.06 492.40 139.37 o -23 2 1 5.51 147.53 139.20 o -22 2 1 0.41 -98.39 104.53 o -21 2 1 46.98 98.39 104.53 o -20 2 1 343.87 373.03 109.81 o -19 2 1 26.83 -32.99 85.85 o -18 2 1 960.33 936.12 148.57 o -17 2 1 990.73 911.10 122.37 o -16 2 1 1282.20 1164.29 114.33 o -15 2 1 1061.36 1104.34 141.21 o -14 2 1 47.31 -24.87 70.69 o -13 2 1 11527.45 11093.72 852.94 o -12 2 1 12718.24 14009.57 1067.54 o -11 2 1 1010.22 1807.94 157.91 o -10 2 1 427.81 442.60 143.03 o -9 2 1 12294.79 12800.48 960.34 o -8 2 1 15073.47 11686.99 1289.42 o -7 2 1 10397.10 9527.26 586.84 o -6 2 1 503.83 530.29 49.04 o -5 2 1 984.03 780.12 56.21 o -4 2 1 8.81 129.06 47.86 o -3 2 1 59916.28 57851.87 2475.38 o -2 2 1 13909.79 14794.34 628.07 o -1 2 1 4518.43 4140.67 161.57 o 0 2 1 33581.41 34868.09 1280.21 o 1 2 1 5112.34 5669.49 222.19 o 2 2 1 28837.72 28279.99 1175.75 o 3 2 1 2415.31 2131.97 83.65 o 4 2 1 495.43 506.28 49.58 o 5 2 1 717.17 196.38 99.52 o 6 2 1 51.17 -48.56 97.12 o 7 2 1 2129.64 1884.61 195.19 o 8 2 1 14657.57 11491.32 1265.86 o 9 2 1 21561.39 22591.29 2433.17 o 10 2 1 3594.44 4258.39 333.61 o 11 2 1 86.27 147.51 128.12 o 12 2 1 3374.42 2357.75 231.49 o 13 2 1 4705.61 4233.93 331.27 o 14 2 1 3740.11 4429.93 323.16 o 15 2 1 3.63 197.09 104.62 o 16 2 1 2873.88 2523.65 197.57 o 17 2 1 0.01 20.88 71.81 o 18 2 1 337.97 188.28 169.71 o 19 2 1 2.14 29.69 82.53 o 20 2 1 1123.84 1619.13 152.40 o 21 2 1 801.00 638.94 117.90 o 22 2 1 80.65 98.55 104.69 o 23 2 1 981.59 1079.77 355.05 o 24 2 1 745.44 906.96 180.29 o 25 2 1 61.75 197.47 146.87 o 26 2 1 397.87 271.77 139.88 o 27 2 1 0.91 248.56 248.56 o 28 2 1 29.69 0.00 140.06 o 29 2 1 97.41 49.46 140.23 o 30 2 1 489.43 497.11 248.56 o 31 2 1 525.12 348.08 199.04 o 32 2 1 158.65 323.08 175.76 o 34 2 1 350.65 187.40 151.57 o 36 2 1 5.11 -149.52 249.04 o -36 3 1 112.70 -99.04 297.60 o -35 3 1 8.70 446.15 248.08 o -34 3 1 144.14 99.04 297.11 o -33 3 1 133.34 252.96 195.80 o -32 3 1 400.27 435.41 143.05 o -31 3 1 162.09 175.28 153.96 o -30 3 1 32.69 297.11 247.60 o -29 3 1 60.86 202.00 153.52 o -28 3 1 312.52 603.77 216.83 o -27 3 1 25.49 147.03 113.24 o -26 3 1 47.30 98.39 153.72 o -25 3 1 3.80 171.82 125.71 o -24 3 1 668.52 624.07 136.26 o -23 3 1 4.04 31.44 120.98 o -22 3 1 617.53 1179.17 236.19 o -21 3 1 138.90 313.35 122.81 o -20 3 1 1767.13 1401.26 162.77 o -19 3 1 91.85 118.23 101.33 o -18 3 1 1165.43 1210.50 138.83 o -17 3 1 44.78 100.96 151.44 o -16 3 1 78.84 174.36 127.16 o -15 3 1 477.96 669.59 165.38 o -14 3 1 1.41 224.59 105.86 o -13 3 1 682.12 531.24 142.31 o -12 3 1 4219.37 3682.87 263.43 o -11 3 1 3070.01 3349.91 282.46 o -10 3 1 1697.09 1324.14 114.72 o -9 3 1 65.08 395.19 99.04 o -6 3 1 3063.34 2445.19 199.52 o -5 3 1 116.76 449.04 100.00 o -3 3 1 24.42 176.26 75.96 o -2 3 1 11502.50 9962.87 393.86 o -1 3 1 5077.36 4810.07 291.82 o 0 3 1 6509.57 6082.98 294.89 o 1 3 1 3350.62 3284.44 143.80 o 2 3 1 1820.04 1616.44 105.87 o 3 3 1 393.82 452.40 100.48 o 5 3 1 113.12 347.60 99.52 o 9 3 1 465.24 145.91 68.84 o 10 3 1 1359.19 1018.27 146.15 o 11 3 1 60.76 419.07 104.65 o 12 3 1 4286.08 3779.47 280.80 o 13 3 1 230.64 49.38 69.81 o 14 3 1 446.10 369.59 104.62 o 15 3 1 1937.17 1746.72 290.38 o 16 3 1 184.69 52.03 129.65 o 17 3 1 213.86 -177.57 200.72 o 18 3 1 129.60 49.04 146.63 o 19 3 1 130.57 180.97 116.99 o 20 3 1 0.40 0.08 86.91 o 21 3 1 414.70 326.60 116.64 o 22 3 1 133.78 315.86 137.34 o 23 3 1 21.88 283.29 158.22 o 24 3 1 628.27 356.44 120.64 o 25 3 1 2277.42 2025.23 296.83 o 26 3 1 28.07 3.39 184.60 o 27 3 1 30.47 30.06 166.06 o 28 3 1 994.33 1136.42 187.09 o 29 3 1 34.57 316.77 198.08 o 30 3 1 130.95 0.00 245.19 o 31 3 1 1.14 0.00 189.14 o 32 3 1 195.68 542.79 296.15 o 33 3 1 275.88 838.94 345.67 o 34 3 1 260.02 246.63 296.15 o 35 3 1 37.54 -246.63 296.15 o 36 3 1 6.64 99.01 126.87 o -35 4 1 3.24 -76.28 153.17 o -34 4 1 46.84 109.85 165.42 o -33 4 1 265.75 357.44 391.59 o -32 4 1 40.20 -4.50 188.76 o -31 4 1 33.23 147.35 208.38 o -30 4 1 6.29 0.00 197.60 o -29 4 1 22.80 99.04 247.11 o -28 4 1 4.33 180.92 203.78 o -27 4 1 8.96 -20.97 120.82 o -26 4 1 143.77 260.40 210.84 o -25 4 1 67.94 257.24 130.31 o -24 4 1 402.93 743.24 381.88 o -23 4 1 206.15 146.63 342.31 o -22 4 1 76.99 -24.52 173.04 o -21 4 1 253.88 337.82 153.17 o -20 4 1 1050.60 1200.74 94.70 o -19 4 1 394.69 377.40 47.60 o -18 4 1 122.43 139.90 46.63 o -17 4 1 57.70 11.89 73.80 o -16 4 1 742.56 515.61 80.30 o -15 4 1 878.66 604.81 201.92 o -14 4 1 77.00 74.75 225.00 o -13 4 1 102.13 331.10 83.15 o -12 4 1 32.09 79.50 98.80 o 0 4 1 2365.70 1705.28 200.96 o 1 4 1 544.59 602.88 100.48 o 10 4 1 841.22 786.06 147.60 o 11 4 1 2080.99 2087.72 246.63 o 12 4 1 2532.84 2190.52 225.73 o 13 4 1 645.94 1033.97 335.82 o 14 4 1 1180.72 805.77 251.92 o 15 4 1 197.76 0.00 151.44 o 17 4 1 138.82 0.00 148.56 o 18 4 1 1.65 176.38 118.50 o 19 4 1 503.96 295.19 139.04 o 20 4 1 30.76 -21.02 196.15 o 21 4 1 235.17 59.60 152.71 o 22 4 1 340.92 381.46 187.33 o 23 4 1 11.61 239.09 187.20 o 24 4 1 15.79 -81.00 151.79 o 25 4 1 612.97 1345.76 363.94 o 26 4 1 19.31 97.87 112.78 o 27 4 1 28.57 284.83 289.48 o 28 4 1 119.90 195.25 140.91 o 29 4 1 1.79 244.80 173.03 o 30 4 1 37.28 195.83 207.54 o 31 4 1 20.92 245.67 196.63 o 32 4 1 84.74 98.08 245.19 o 33 4 1 319.60 687.02 245.67 o 34 4 1 185.45 147.12 294.23 o 35 4 1 2.26 -294.23 294.23 o -34 5 1 39.66 98.16 208.39 o -33 5 1 10.94 147.60 246.15 o 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