Alert level A
PLAT432_ALERT_2_A Short Inter X...Y Contact C128 .. C128 .. 2.86 Ang.
PLAT432_ALERT_2_A Short Inter X...Y Contact C131 .. C136 .. 2.66 Ang.
Alert level B
PLAT222_ALERT_3_B Large Non-Solvent H Ueq(max)/Ueq(min) ... 4.47 Ratio
PLAT242_ALERT_2_B Check Low Ueq as Compared to Neighbors for C22
PLAT413_ALERT_2_B Short Inter XH3 .. XHn H3C .. H24C .. 1.99 Ang.
PLAT413_ALERT_2_B Short Inter XH3 .. XHn H6 .. H24B .. 2.04 Ang.
Alert level C
PLAT213_ALERT_2_C Atom C120 has ADP max/min Ratio ..... 3.10 prola
PLAT213_ALERT_2_C Atom C128 has ADP max/min Ratio ..... 3.50 oblat
PLAT220_ALERT_2_C Large Non-Solvent C Ueq(max)/Ueq(min) ... 3.46 Ratio
PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C10
PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C25
PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C30
PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C34
PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C114
PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C122
PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for P103
PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds (x 1000) Ang .. 13
PLAT360_ALERT_2_C Short C(sp3)-C(sp3) Bond C10 - C12 ... 1.37 Ang.
PLAT413_ALERT_2_C Short Inter XH3 .. XHn H2 .. H24B .. 2.11 Ang.
PLAT432_ALERT_2_C Short Inter X...Y Contact C3 .. C24 .. 3.13 Ang.
PLAT601_ALERT_2_C Structure Contains Solvent Accessible VOIDS of . 82.00 A**3
PLAT234_ALERT_4_C Large Hirshfeld Difference P3 -- C33 .. 0.17 Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference C2 -- C3 .. 0.16 Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference C10 -- C11 .. 0.19 Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference C10 -- C12 .. 0.20 Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference C26 -- C28 .. 0.23 Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference C122 -- C124 .. 0.19 Ang.
Alert level G
REFLT03_ALERT_4_G Please check that the estimate of the number of Friedel pairs is
correct. If it is not, please give the correct count in the
_publ_section_exptl_refinement section of the submitted CIF.
From the CIF: _diffrn_reflns_theta_max 27.48
From the CIF: _reflns_number_total 11537
Count of symmetry unique reflns 6595
Completeness (_total/calc) 174.94%
TEST3: Check Friedels for noncentro structure
Estimate of Friedel pairs measured 4942
Fraction of Friedel pairs measured 0.749
Are heavy atom types Z>Si present yes
PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 17.52
PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 34.00 Perc.
PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 946
PLAT811_ALERT_5_G No ADDSYM Analysis: Too Many Excluded Atoms .... !
2 ALERT level A = In general: serious problem 4 ALERT level B = Potentially serious problem 21 ALERT level C = Check and explain 5 ALERT level G = General alerts; check 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 20 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 7 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check
