Alert level A
PLAT222_ALERT_3_A Large Non-Solvent H Ueq(max)/Ueq(min) ... 5.33 Ratio
Alert level B
PLAT213_ALERT_2_B Atom C232 has ADP max/min Ratio ..... 4.40 oblat
PLAT220_ALERT_2_B Large Non-Solvent C Ueq(max)/Ueq(min) ... 4.28 Ratio
PLAT242_ALERT_2_B Check Low Ueq as Compared to Neighbors for P203
PLAT413_ALERT_2_B Short Inter XH3 .. XHn H22C .. H24B .. 1.94 Ang.
Alert level C
PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for P3
PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds (x 1000) Ang .. 13
PLAT234_ALERT_4_C Large Hirshfeld Difference P203 -- C225 .. 0.20 Ang.
Alert level G
REFLT03_ALERT_4_G Please check that the estimate of the number of Friedel pairs is
correct. If it is not, please give the correct count in the
_publ_section_exptl_refinement section of the submitted CIF.
From the CIF: _diffrn_reflns_theta_max 27.48
From the CIF: _reflns_number_total 11396
Count of symmetry unique reflns 6299
Completeness (_total/calc) 180.92%
TEST3: Check Friedels for noncentro structure
Estimate of Friedel pairs measured 5097
Fraction of Friedel pairs measured 0.809
Are heavy atom types Z>Si present yes
PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 27.71
PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 20.00 Perc.
PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 504
PLAT811_ALERT_5_G No ADDSYM Analysis: Too Many Excluded Atoms .... !
1 ALERT level A = In general: serious problem 4 ALERT level B = Potentially serious problem 3 ALERT level C = Check and explain 5 ALERT level G = General alerts; check 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 6 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check
