Alert level A
PLAT242_ALERT_2_A Check Low Ueq as Compared to Neighbors for P102
PLAT432_ALERT_2_A Short Inter X...Y Contact C119 .. C124 .. 2.55 Ang.
Alert level B
PLAT222_ALERT_3_B Large Non-Solvent H Ueq(max)/Ueq(min) ... 4.01 Ratio
PLAT242_ALERT_2_B Check Low Ueq as Compared to Neighbors for P2
PLAT413_ALERT_2_B Short Inter XH3 .. XHn H8B .. H35C .. 2.01 Ang.
PLAT234_ALERT_4_B Large Hirshfeld Difference P2 -- C21 .. 0.28 Ang.
Alert level C
PLAT213_ALERT_2_C Atom C123 has ADP max/min Ratio ..... 3.30 prola
PLAT220_ALERT_2_C Large Non-Solvent C Ueq(max)/Ueq(min) ... 3.44 Ratio
PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C10
PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C126
PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C134
PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for P3
PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C34
PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds (x 1000) Ang .. 16
PLAT360_ALERT_2_C Short C(sp3)-C(sp3) Bond C10 - C12 ... 1.42 Ang.
PLAT432_ALERT_2_C Short Inter X...Y Contact C24 .. C31 .. 3.14 Ang.
PLAT601_ALERT_2_C Structure Contains Solvent Accessible VOIDS of . 36.00 A**3
PLAT234_ALERT_4_C Large Hirshfeld Difference P2 -- O2 .. 0.16 Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference P2 -- C17 .. 0.22 Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference C9 -- C10 .. 0.20 Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference C18 -- C19 .. 0.21 Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference C134 -- C135 .. 0.22 Ang.
Alert level G
REFLT03_ALERT_4_G Please check that the estimate of the number of Friedel pairs is
correct. If it is not, please give the correct count in the
_publ_section_exptl_refinement section of the submitted CIF.
From the CIF: _diffrn_reflns_theta_max 27.48
From the CIF: _reflns_number_total 11524
Count of symmetry unique reflns 6585
Completeness (_total/calc) 175.00%
TEST3: Check Friedels for noncentro structure
Estimate of Friedel pairs measured 4939
Fraction of Friedel pairs measured 0.750
Are heavy atom types Z>Si present yes
PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 69.47
PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 34.00 Perc.
PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 970
PLAT811_ALERT_5_G No ADDSYM Analysis: Too Many Excluded Atoms .... !
2 ALERT level A = In general: serious problem 4 ALERT level B = Potentially serious problem 16 ALERT level C = Check and explain 5 ALERT level G = General alerts; check 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 15 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 7 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check
