Alert level A
PLAT432_ALERT_2_A Short Inter X...Y Contact C215 .. C219 .. 2.54 Ang.
Alert level B
PLAT222_ALERT_3_B Large Non-Solvent H Ueq(max)/Ueq(min) ... 4.56 Ratio
PLAT242_ALERT_2_B Check Low Ueq as Compared to Neighbors for C18
PLAT242_ALERT_2_B Check Low Ueq as Compared to Neighbors for C22
Alert level C
PLAT220_ALERT_2_C Large Non-Solvent C Ueq(max)/Ueq(min) ... 3.69 Ratio
PLAT230_ALERT_2_C Hirshfeld Test Diff for C9 -- C10 .. 5.63 su
PLAT230_ALERT_2_C Hirshfeld Test Diff for C10 -- C11 .. 5.79 su
PLAT230_ALERT_2_C Hirshfeld Test Diff for C22 -- C24 .. 5.30 su
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X) Gd1 -- O12 .. 5.07 su
PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for P2
PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C10
PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C14
PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C26
PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C30
PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for P202
PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C226
PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds (x 1000) Ang .. 11
PLAT601_ALERT_2_C Structure Contains Solvent Accessible VOIDS of . 35.00 A**3
PLAT234_ALERT_4_C Large Hirshfeld Difference P2 -- C17 .. 0.23 Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference C14 -- C15 .. 0.22 Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference C30 -- C31 .. 0.18 Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference C30 -- C32 .. 0.20 Ang.
PLAT234_ALERT_4_C Large Hirshfeld Difference C34 -- C35 .. 0.21 Ang.
Alert level G
REFLT03_ALERT_4_G Please check that the estimate of the number of Friedel pairs is
correct. If it is not, please give the correct count in the
_publ_section_exptl_refinement section of the submitted CIF.
From the CIF: _diffrn_reflns_theta_max 27.48
From the CIF: _reflns_number_total 11383
Count of symmetry unique reflns 6583
Completeness (_total/calc) 172.92%
TEST3: Check Friedels for noncentro structure
Estimate of Friedel pairs measured 4800
Fraction of Friedel pairs measured 0.729
Are heavy atom types Z>Si present yes
PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 15.02
PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 34.00 Perc.
PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 976
PLAT811_ALERT_5_G No ADDSYM Analysis: Too Many Excluded Atoms .... !
1 ALERT level A = In general: serious problem 3 ALERT level B = Potentially serious problem 19 ALERT level C = Check and explain 5 ALERT level G = General alerts; check 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 17 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 6 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check
