Sample Originator: Andrew Platta.
Data Collection: Peter N. Hortonb
Structure Determination: Peter N. Hortonb and Michael B. Hursthouseb.
Staffordshire Universitya
University of Southamptonb
C80H84Br3LaO8P4
InChI=1/4C18H16OP.4C2H6O.3BrH.La/c4*19-20(16-10-4-1-5-11-16,17-12-6-2-7-13-17)18-14-8-3-9-15-18;4*1-2-3;;;;/h4*1-15,20H;4*3H,2H2,1H3;3*1H;/q4*-1;;;;;;;;+6/p-2
| Identification Number: | 10.5258/ecrystals/1236 |
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| Controlled Keywords: | lanthanide coordination, organophosphorus ligands |
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| Date Created: | 05 October 2009 |
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| Deposited On: | 22 Jan 2010 16:26 |
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| Deposited By: | Dr Peter N Horton |
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Depositor Comments
User ref code:- La Br Ph
Data collection parameters
| Chemical formula | C80 H84 Br3 La O8 P4 |
| Crystal morphology | Slab |
| Crystal system | monoclinic |
| Space group symbol | P2(1)/c |
| Cell length a | 14.6651(5) |
| Cell length b | 17.6331(7) |
| Cell length c | 30.0183(11) |
| Cell angle alpha | 90.00 |
| Cell angle beta | 97.6680(10) |
| Cell angle gamma | 90.00 |
| Data collection temperature | 120(2) |
Refinement results
| Solution figure of merit | 0.0525 |
| R Factor (Obs) | 0.0670 |
| R Factor (All) | 0.1035 |
| Weighted R Factor (Obs) | 0.1397 |
| Weighted R Factor (All) | 0.1574 |
Citation: Platt, Andrew and Horton, Peter N. and Hursthouse, Michael B. (2009) University of Southampton, Crystal Structure Report Archive. (doi:10.5258/ecrystals/1236)
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