Symmetry used in scalepack | c2 |
---|---|
a (Angstrom) | 14.6339 +/- 0.0010 |
b (Angstrom) | 7.7463 +/- 0.0006 |
c (Angstrom) | 35.875 +/- 0.003 |
alpha (°) | 90.000 |
beta (°) | 91.066 +/- 0.003 |
gamma (°) | 90.000 |
Volume (A**3) | 4066.1 +/- 0.6 |
Mosaicity (°) | 0.915 +/- 0.005 |
Total number of images collected | 233 |
---|---|
Total exposure time | 59.7 minutes |
Data collection exposure time | 57.0 minutes |
Data collection wall-clock time | 83.3 minutes |
Wavelength | 0.71073 A |
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Generator setting | 50kV 90mA |
Crystal to detector distance | 45.50 mm |
Type | Name | # images | Total Rotation | Per frame Rotation | Exposure per frame | Used in scaling |
---|---|---|---|---|---|---|
data collection | s01f | 183 | 183.0° phi | 1.000° | 15 seconds | Yes |
data collection | s02f | 42 | 42.0° omega | 1.000° | 15 seconds | Yes |
Phi/Chi | i01f - i08f | 8 | 20 seconds |
Zero sigma or profile test | 46 |
---|---|
Overload or incomplete profile | 288 |
Sigma cutoff | 23 |
High resolution limit | 3 |
Scale factor | 10.00 |
---|---|
Number of 'full' reflections | 245 |
Number of 'partial' reflections | 21064 |
Total number of integrated reflections | 7547 |
Total number of unique reflections | 3602 |
Data completeness | 83.2% |
Resolution range | 7.00-0.81 A |
Theta range | 2.91°-26.02° |
Average Intensity | 10.6 |
Average Sigma(I) | 2.2 |
Overall R-merge (linear) | 0.110 |
Collection Temperature | 120 K |
Crystal Size | x x |
Crystal Colour | |
Crystal Shape |
R(merge) on F2 |
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R |
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Rw |
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Max Transmission Factor |
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Min Transmission Factor |
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