# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_s92 _shelx_title ' 95SRC296R P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 352.34 _exptl_crystal_F_000 1240.00 _reflns_d_resolution_high 0.8368 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.3528 _cell_length_b 12.3921 _cell_length_c 18.1099 _cell_angle_alpha 83.286 _cell_angle_beta 82.649 _cell_angle_gamma 74.120 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4126.07 4106.13 275.17 o 4 0 0 4107.93 4052.39 430.36 o 6 0 0 5848.27 4879.44 610.06 o 7 0 0 50.21 166.33 302.36 o 8 0 0 13.68 294.04 380.62 o 11 0 0 1776.66 1936.08 592.38 o 12 0 0 1068.60 613.98 454.37 o -12 1 0 8.57 198.43 442.24 o -11 1 0 6.88 126.74 693.97 o -10 1 0 42.64 318.41 383.13 o -9 1 0 7745.59 7939.58 966.92 o -8 1 0 3766.99 3457.25 598.81 o -7 1 0 2158.83 2003.03 503.84 o -6 1 0 163.13 195.18 292.26 o -5 1 0 978.34 733.61 257.77 o -4 1 0 5.99 89.47 316.41 o -2 1 0 19826.03 20844.83 645.12 o -1 1 0 4115.37 3649.73 847.89 o 1 1 0 12498.51 11439.07 324.12 o 2 1 0 29.32 28.36 29.98 o 3 1 0 15723.48 18687.71 753.62 o 4 1 0 1041.65 838.49 262.13 o 5 1 0 3296.96 3019.94 430.51 o 6 1 0 797.44 1154.39 318.42 o 7 1 0 6520.11 6187.24 716.63 o 8 1 0 632.82 809.34 331.00 o 9 1 0 3028.36 2644.91 596.88 o 10 1 0 157.00 414.28 424.02 o 11 1 0 4815.61 4790.67 843.46 o 12 1 0 385.57 302.56 387.10 o 13 1 0 276.61 351.86 396.77 o -12 2 0 1775.05 2235.35 718.83 o -11 2 0 15.72 377.35 424.41 o -10 2 0 659.35 870.72 457.19 o -9 2 0 644.88 1058.85 456.96 o -8 2 0 174.29 263.53 336.78 o -7 2 0 756.60 642.34 313.26 o -6 2 0 6262.36 6489.83 701.22 o -5 2 0 660.24 669.08 241.67 o -4 2 0 3326.20 3570.77 417.85 o -3 2 0 3.19 57.57 394.42 o -1 2 0 5322.47 5629.82 300.43 o 0 2 0 3027.66 3810.75 397.50 o 1 2 0 43242.89 47398.84 1203.23 o 2 2 0 12789.75 14869.44 753.15 o 3 2 0 781.91 582.29 86.19 o 4 2 0 2001.56 1856.65 97.93 o 5 2 0 177.87 233.81 210.74 o 6 2 0 186.80 129.55 53.70 o 7 2 0 1354.70 1163.34 107.05 o 8 2 0 6348.44 6892.88 290.02 o 9 2 0 2872.73 2625.74 156.62 o 10 2 0 452.18 661.60 338.08 o 11 2 0 188.17 202.96 412.55 o 12 2 0 3027.11 2857.94 752.29 o 13 2 0 295.75 388.70 374.11 o -11 3 0 1425.24 1981.02 556.60 o -10 3 0 7.03 437.02 389.41 o -9 3 0 918.40 830.95 375.54 o -8 3 0 5766.71 5144.40 753.35 o -7 3 0 507.82 762.18 354.05 o -6 3 0 458.27 401.97 225.13 o -5 3 0 10317.19 9436.45 772.28 o -3 3 0 5954.33 5680.01 494.20 o -1 3 0 2323.57 2093.25 179.82 o 0 3 0 1298.70 1578.13 124.43 o 1 3 0 2744.45 2236.97 179.69 o 2 3 0 789.31 959.34 174.34 o 3 3 0 2542.14 1968.13 288.33 o 4 3 0 43.23 99.94 50.67 o 5 3 0 4423.20 4355.22 499.76 o 6 3 0 301.61 428.57 233.66 o 7 3 0 2837.19 3049.50 369.90 o 8 3 0 11.79 260.72 323.73 o 9 3 0 3899.98 3853.56 626.80 o 10 3 0 1580.13 1782.23 537.73 o 11 3 0 2654.82 2744.31 671.83 o 12 3 0 4.22 67.66 1150.15 o 13 3 0 16.50 278.34 455.02 o -12 4 0 0.78 110.63 725.67 o -11 4 0 3901.35 3860.77 771.61 o -10 4 0 31.05 4.55 12645.25 o -9 4 0 826.10 606.10 320.01 o -8 4 0 306.64 421.99 348.08 o -6 4 0 284.37 27.73 1365.32 o -5 4 0 4710.99 4867.29 578.93 o -4 4 0 3614.50 4405.14 537.28 o -3 4 0 3084.51 3342.21 407.61 o -2 4 0 975.00 1142.59 249.11 o -1 4 0 596.14 400.45 100.07 o 0 4 0 5980.64 5637.75 1129.77 o 1 4 0 728.84 870.42 148.01 o 2 4 0 13621.68 14792.39 2854.70 o 3 4 0 6826.35 6593.08 492.39 o 4 4 0 635.65 786.40 227.01 o 5 4 0 1788.93 1453.55 296.46 o 6 4 0 10959.57 12767.57 1635.81 o 7 4 0 5881.90 5605.90 703.86 o 8 4 0 4965.50 4130.33 630.27 o 9 4 0 3343.59 2953.34 559.76 o 10 4 0 661.65 544.19 315.41 o 11 4 0 258.21 534.75 359.63 o 12 4 0 1894.24 1755.38 701.42 o 13 4 0 9.03 209.20 392.39 o -11 5 0 424.30 173.14 451.78 o -10 5 0 1.48 37.48 2261.70 o -9 5 0 683.00 558.50 389.47 o -8 5 0 111.68 177.75 513.03 o -7 5 0 4912.60 4774.62 701.71 o -6 5 0 7366.53 7916.33 831.26 o -5 5 0 1128.66 914.06 317.55 o -4 5 0 974.93 981.94 320.04 o -3 5 0 4160.90 3924.13 458.03 o -2 5 0 6376.05 6389.71 524.16 o -1 5 0 20477.01 27043.29 4897.09 o 0 5 0 716.97 1054.74 163.20 o 1 5 0 178.22 208.25 106.61 o 2 5 0 1834.34 1711.37 210.22 o 3 5 0 18.80 132.55 192.36 o 4 5 0 341.25 459.13 218.84 o 5 5 0 1328.40 1368.54 352.06 o 7 5 0 1363.00 1035.38 379.98 o 8 5 0 296.83 567.45 290.98 o 9 5 0 347.63 559.87 380.34 o 11 5 0 214.00 430.38 428.57 o 12 5 0 49.99 319.45 403.46 o 13 5 0 613.83 608.96 477.57 o -11 6 0 312.51 256.05 339.86 o -10 6 0 5831.01 5706.28 896.43 o -9 6 0 431.40 407.22 414.54 o -8 6 0 7.51 103.72 510.25 o -7 6 0 72.94 95.61 626.51 o -6 6 0 484.66 586.96 286.80 o -5 6 0 1604.10 1532.01 423.60 o -4 6 0 7828.04 8443.72 754.52 o -3 6 0 72.11 279.31 234.70 o -2 6 0 2805.39 2335.22 360.34 o -1 6 0 240.05 220.16 108.60 o 0 6 0 3444.39 3771.44 295.04 o 1 6 0 4002.85 3782.46 316.84 o 2 6 0 942.06 826.50 167.75 o 3 6 0 1658.73 1767.76 233.76 o 4 6 0 72.92 298.44 198.20 o 5 6 0 2320.78 1664.21 357.46 o 6 6 0 235.86 363.94 240.78 o 7 6 0 6118.88 5223.78 685.74 o 8 6 0 176.16 292.55 339.95 o 9 6 0 141.08 119.97 442.24 o 10 6 0 1775.82 1768.58 443.38 o 11 6 0 970.35 621.19 433.17 o 12 6 0 476.19 745.45 598.10 o 13 6 0 1093.31 831.78 537.23 o -10 7 0 29.67 14.56 2775.86 o -9 7 0 206.42 154.58 342.47 o -8 7 0 162.18 16.98 2300.89 o -7 7 0 415.31 364.49 236.53 o -6 7 0 0.57 7.76 4670.43 o -5 7 0 125.13 302.56 283.13 o -4 7 0 1161.73 1282.98 365.82 o -3 7 0 1380.74 1507.13 328.91 o -2 7 0 7515.60 7934.41 492.38 o -1 7 0 224.15 407.07 122.59 o 0 7 0 6111.07 5803.04 402.13 o 1 7 0 4874.24 4711.14 363.10 o 2 7 0 11590.05 12571.35 1475.74 o 3 7 0 11708.37 20554.18 8635.89 o 4 7 0 10322.84 9758.51 601.04 o 5 7 0 392.25 292.37 193.52 o 6 7 0 4090.34 3760.47 585.38 o 7 7 0 2320.97 2319.82 501.70 o 8 7 0 107.89 280.76 349.56 o 9 7 0 1048.67 1521.81 519.53 o 10 7 0 144.95 310.69 342.66 o 11 7 0 961.83 782.92 304.72 o 12 7 0 25.44 235.14 372.84 o 13 7 0 114.46 149.21 409.22 o -9 8 0 1272.28 815.96 543.70 o -7 8 0 698.38 651.19 305.05 o -6 8 0 5980.18 5825.25 761.79 o -5 8 0 2.76 55.39 576.21 o -4 8 0 294.35 350.78 219.54 o -3 8 0 1439.33 1748.10 411.25 o -2 8 0 2388.65 2481.59 312.19 o -1 8 0 4016.66 4123.26 391.62 o 0 8 0 6545.35 6786.85 456.94 o 1 8 0 40.96 123.79 186.40 o 2 8 0 815.15 701.79 189.21 o 3 8 0 376.63 335.41 135.85 o 4 8 0 2409.38 2732.99 360.66 o 5 8 0 12.66 246.40 393.05 o 6 8 0 2724.08 2736.11 377.27 o 7 8 0 4157.70 5057.37 728.38 o 8 8 0 3656.75 3450.43 669.80 o 9 8 0 18.15 121.88 471.17 o 10 8 0 525.35 320.49 367.75 o 11 8 0 1096.79 1314.35 551.19 o 12 8 0 0.53 166.71 381.49 o -7 9 0 1003.14 590.48 300.35 o -6 9 0 10.00 170.10 241.81 o -5 9 0 112.68 11.13 2747.83 o -4 9 0 76.73 325.18 258.47 o -3 9 0 4820.50 4862.95 473.88 o -2 9 0 570.57 906.38 406.19 o -1 9 0 2657.43 2867.47 388.28 o 0 9 0 1234.56 1386.31 237.70 o 1 9 0 6423.42 6614.23 491.95 o 2 9 0 182.25 319.91 179.07 o 3 9 0 176.53 356.35 176.31 o 4 9 0 6.52 67.19 707.00 o 5 9 0 11292.11 11642.91 736.79 o 6 9 0 3679.64 3530.78 461.70 o 7 9 0 496.03 555.53 288.54 o 8 9 0 569.03 562.30 220.04 o 9 9 0 173.34 92.79 575.22 o 11 9 0 1917.04 2233.98 604.78 o 12 9 0 411.82 195.85 303.45 o -5 10 0 5.63 27.58 627.54 o -4 10 0 2558.26 2895.71 430.68 o -3 10 0 430.55 551.10 217.00 o -2 10 0 1558.28 1499.25 458.37 o -1 10 0 1103.28 1273.93 261.01 o 0 10 0 111.24 252.35 297.75 o 1 10 0 131.52 173.52 253.40 o 2 10 0 382.04 361.83 169.91 o 3 10 0 5.21 144.98 223.34 o 4 10 0 1746.95 1461.98 287.03 o 5 10 0 0.90 194.77 356.75 o 6 10 0 550.37 373.36 223.40 o 7 10 0 9.61 232.04 377.89 o 8 10 0 462.57 418.55 293.50 o 9 10 0 53.35 53.04 1344.18 o 10 10 0 446.04 323.66 274.47 o 11 10 0 96.24 206.69 294.08 o 12 10 0 2665.95 2898.41 773.22 o -3 11 0 256.83 247.76 272.20 o -2 11 0 1079.95 1044.74 429.52 o -1 11 0 227.50 196.67 179.23 o 0 11 0 1219.32 1251.01 267.08 o 1 11 0 41.09 178.91 262.74 o 2 11 0 1913.85 1763.78 311.72 o 3 11 0 1443.51 1559.03 297.54 o 4 11 0 238.22 255.75 147.74 o 5 11 0 521.10 677.62 257.95 o 6 11 0 316.59 197.15 241.85 o 7 11 0 234.15 499.57 242.40 o 8 11 0 92.81 64.28 851.18 o 9 11 0 2822.25 2751.90 504.69 o 10 11 0 152.01 265.42 352.16 o 11 11 0 47.38 66.71 585.11 o 0 12 0 3977.14 4399.82 465.90 o 1 12 0 2053.74 1523.46 310.42 o 2 12 0 256.05 194.12 156.36 o 3 12 0 725.09 637.73 207.06 o 4 12 0 270.49 303.97 202.53 o 5 12 0 11.89 19.97 1537.49 o 6 12 0 1511.65 1305.35 316.16 o 7 12 0 457.70 528.84 239.31 o 8 12 0 431.69 275.90 409.98 o 9 12 0 289.49 370.61 341.29 o 10 12 0 339.62 344.29 315.48 o 11 12 0 449.70 253.27 297.37 o 0 13 0 101.89 130.35 243.81 o 1 13 0 1800.64 2315.63 585.02 o 3 13 0 134.43 107.59 485.53 o 4 13 0 3.04 84.60 270.74 o 5 13 0 1797.42 1684.65 353.96 o 6 13 0 225.01 179.33 184.33 o 7 13 0 968.35 612.27 230.53 o 8 13 0 162.36 146.93 291.22 o 9 13 0 12.96 32.84 731.20 o 3 14 0 744.19 546.22 360.76 o 5 14 0 112.16 240.51 316.78 o -7 -14 1 372.11 701.74 495.76 o -6 -14 1 104.97 146.04 285.06 o -5 -14 1 1340.11 1340.78 467.47 o -9 -13 1 256.37 230.27 368.08 o -8 -13 1 56.61 162.24 270.53 o -7 -13 1 15.91 144.29 473.85 o -6 -13 1 1577.47 1507.79 343.56 o -5 -13 1 179.33 263.53 341.96 o -4 -13 1 379.15 290.60 336.47 o -3 -13 1 402.41 279.03 213.24 o -2 -13 1 843.62 600.21 212.95 o -1 -13 1 344.62 366.71 297.81 o -10 -12 1 523.31 529.40 319.11 o -9 -12 1 412.91 148.86 552.81 o -8 -12 1 1344.44 1615.47 408.29 o -7 -12 1 1289.35 1024.06 333.42 o -6 -12 1 0.09 18.82 4094.85 o -5 -12 1 71.97 214.92 279.82 o -4 -12 1 212.91 298.73 186.20 o -3 -12 1 23.14 114.66 221.03 o -2 -12 1 571.02 562.01 203.86 o -1 -12 1 3078.46 3171.07 414.80 o 0 -12 1 57.27 254.27 217.85 o 1 -12 1 582.32 472.28 236.46 o -11 -11 1 153.77 223.28 309.99 o -10 -11 1 647.52 502.04 289.17 o -9 -11 1 473.61 666.59 318.08 o -8 -11 1 49.57 223.40 286.79 o -6 -11 1 124.21 23.48 1369.87 o -5 -11 1 9.78 177.86 214.52 o -4 -11 1 549.60 762.29 253.91 o -3 -11 1 58.53 134.38 209.94 o -2 -11 1 2076.99 1591.55 300.69 o -1 -11 1 2987.22 3119.71 394.75 o 0 -11 1 3429.94 2936.78 394.14 o 1 -11 1 1784.77 2167.01 353.51 o 3 -11 1 290.76 339.46 226.13 o 4 -11 1 1528.57 1577.88 293.22 o -11 -10 1 1182.48 1274.68 544.89 o -10 -10 1 756.58 795.37 464.79 o -9 -10 1 542.59 404.74 232.67 o -8 -10 1 616.99 580.38 265.18 o -7 -10 1 66.72 244.21 234.96 o -6 -10 1 68.17 172.65 242.77 o -5 -10 1 2714.23 3189.68 454.12 o -4 -10 1 328.34 341.15 212.68 o -3 -10 1 710.08 750.70 245.53 o -2 -10 1 54.97 91.96 567.38 o -1 -10 1 254.78 504.65 205.30 o 0 -10 1 504.00 505.24 198.46 o 1 -10 1 1229.88 984.87 321.58 o 2 -10 1 1.67 129.36 342.47 o 3 -10 1 3005.88 3041.13 402.36 o 4 -10 1 422.69 433.44 208.10 o 5 -10 1 299.33 282.22 300.75 o 6 -10 1 191.75 177.36 316.86 o -12 -9 1 1622.99 1547.95 680.37 o -11 -9 1 266.93 419.61 422.58 o -10 -9 1 104.10 158.20 475.64 o -9 -9 1 21.45 305.09 364.89 o -7 -9 1 148.66 341.38 253.00 o -6 -9 1 5233.94 4898.98 518.29 o -5 -9 1 166.99 361.20 246.18 o -4 -9 1 1963.93 1950.03 309.81 o -3 -9 1 63.63 240.61 184.93 o -2 -9 1 175.07 79.88 285.36 o -1 -9 1 373.43 398.67 171.54 o 0 -9 1 126.51 122.86 226.29 o 1 -9 1 1201.32 1079.54 342.51 o 2 -9 1 4758.56 5039.43 464.80 o 3 -9 1 222.43 395.23 207.89 o 4 -9 1 660.53 608.96 284.97 o 5 -9 1 337.87 308.14 219.52 o 7 -9 1 733.87 569.52 310.90 o -12 -8 1 83.41 134.48 358.01 o -11 -8 1 1698.75 1783.46 626.14 o -10 -8 1 1.16 86.21 849.95 o -9 -8 1 105.39 19.45 2506.04 o -7 -8 1 1419.95 1368.54 442.23 o -6 -8 1 3648.41 3288.17 449.07 o -5 -8 1 7128.29 7911.37 587.52 o -4 -8 1 12533.11 12661.37 705.61 o -3 -8 1 1183.53 1114.55 234.16 o -2 -8 1 3807.12 4603.57 411.39 o -1 -8 1 13660.33 12394.98 613.51 o 0 -8 1 379.45 290.34 148.53 o 1 -8 1 1449.60 1519.24 255.28 o 2 -8 1 154.92 239.35 127.26 o 3 -8 1 193.90 229.83 174.19 o 4 -8 1 38.47 117.76 305.55 o 6 -8 1 143.35 182.03 296.34 o 7 -8 1 1684.16 1772.44 480.06 o 8 -8 1 129.98 130.35 249.12 o 9 -8 1 4.94 4.30 4667.63 o -12 -7 1 56.02 250.05 378.52 o -10 -7 1 1417.42 1297.57 496.45 o -9 -7 1 509.71 408.39 357.09 o -8 -7 1 4868.19 4401.29 721.84 o -7 -7 1 77.11 160.77 374.31 o -6 -7 1 95.34 63.43 607.15 o -5 -7 1 2543.24 2765.63 469.97 o -4 -7 1 4327.39 4557.47 433.46 o -3 -7 1 174.18 176.65 212.31 o -2 -7 1 1984.33 1888.68 273.46 o -1 -7 1 119.38 138.40 162.18 o 0 -7 1 3049.31 2836.13 291.67 o 1 -7 1 28.09 151.60 125.86 o 2 -7 1 554.96 476.40 174.51 o 3 -7 1 2122.38 2632.98 470.47 o 4 -7 1 0.39 119.97 328.94 o 5 -7 1 925.33 952.17 321.42 o 6 -7 1 3277.40 3145.59 574.44 o 7 -7 1 726.02 1011.25 477.95 o 8 -7 1 234.98 271.12 321.05 o 9 -7 1 140.16 97.89 340.19 o 10 -7 1 2057.89 1816.69 686.36 o -12 -6 1 31.87 43.76 1391.22 o -11 -6 1 3265.99 3134.00 489.66 o -10 -6 1 230.90 362.28 292.14 o -9 -6 1 0.81 143.59 440.51 o -8 -6 1 642.34 919.33 390.60 o -7 -6 1 562.69 863.89 342.83 o -6 -6 1 216.60 197.62 296.94 o -5 -6 1 4.23 78.57 437.93 o -4 -6 1 1104.99 785.58 268.37 o -3 -6 1 20781.59 19558.81 3819.65 o -1 -6 1 526.33 576.50 155.92 o 0 -6 1 8596.99 9447.92 816.40 o 1 -6 1 3.57 57.20 237.03 o 2 -6 1 92.03 257.91 256.75 o 3 -6 1 10271.88 10354.03 847.34 o 4 -6 1 0.40 89.74 262.70 o 5 -6 1 687.15 699.44 316.92 o 6 -6 1 155.43 146.39 256.97 o 7 -6 1 1131.52 1276.75 477.94 o 8 -6 1 163.47 45.51 1397.35 o 9 -6 1 1442.50 1607.88 606.15 o 10 -6 1 704.70 916.69 489.31 o 11 -6 1 768.44 611.82 378.22 o -13 -5 1 81.57 312.23 418.36 o -12 -5 1 1573.79 1267.44 584.65 o -10 -5 1 82.26 182.12 270.31 o -9 -5 1 5444.70 5240.57 775.06 o -8 -5 1 719.54 546.22 298.37 o -7 -5 1 108.13 387.56 379.85 o -6 -5 1 7786.07 7131.37 744.87 o -5 -5 1 5982.69 5354.61 605.10 o -4 -5 1 572.82 722.65 269.87 o -3 -5 1 1401.65 1522.94 321.57 o -2 -5 1 2311.81 2127.86 248.50 o -1 -5 1 671.62 560.02 123.86 o 0 -5 1 16895.56 20976.64 1501.88 o 1 -5 1 3788.48 3398.12 231.36 o 2 -5 1 4124.70 3835.57 443.84 o 3 -5 1 3634.04 3265.50 450.99 o 4 -5 1 6958.25 6968.15 685.43 o 5 -5 1 638.33 745.45 305.78 o 6 -5 1 248.35 83.80 497.36 o 7 -5 1 312.38 317.38 342.19 o 8 -5 1 1624.91 1618.37 479.73 o 9 -5 1 656.20 813.48 423.70 o 10 -5 1 1532.08 1909.36 664.35 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