| Symmetry used in scalepack | p1 |
|---|---|
| a (Angstrom) | 10.0187 +/- 0.0004 |
| b (Angstrom) | 11.5792 +/- 0.0005 |
| c (Angstrom) | 11.5755 +/- 0.0005 |
| alpha (°) | 68.532 +/- 0.002 |
| beta (°) | 90.034 +/- 0.003 |
| gamma (°) | 89.990 +/- 0.003 |
| Volume (A**3) | 1249.69 +/- 0.09 |
| Mosaicity (°) | 0.633 +/- 0.004 |
| Total number of images collected | 186 |
|---|---|
| Total exposure time | 13.0 hours |
| Data collection exposure time | 12.9 hours |
| Data collection wall-clock time | 13.4 hours |
| Wavelength | 0.71073 A |
|---|---|
| Generator setting | 50kV 90mA |
| Crystal to detector distance | 30.00 mm |
| Type | Name | # images | Total Rotation | Per frame Rotation | Exposure per frame | Used in scaling |
|---|---|---|---|---|---|---|
| data collection | s01f | 178 | 356.0° phi | 2.000° | 260 seconds | Yes |
| Phi/Chi | i01f - i08f | 8 | 50 seconds |
| Zero sigma or profile test | 10 |
|---|---|
| Overload or incomplete profile | 721 |
| Sigma cutoff | 132 |
| Low resolution limit | 36 |
| High resolution limit | 1971 |
| Scale factor | 10.00 |
|---|---|
| Number of 'full' reflections | 2159 |
| Number of 'partial' reflections | 25085 |
| Total number of integrated reflections | 15663 |
| Total number of unique reflections | 5209 |
| Data completeness | 92.3% |
| Resolution range | 7.00-0.77 A |
| Theta range | 2.91°-27.48° |
| Average Intensity | 23.4 |
| Average Sigma(I) | 2.0 |
| Overall R-merge (linear) | 0.095 |
| Collection Temperature | 120 K |
| Crystal Size | x x |
| Crystal Colour | |
| Crystal Shape |
| Max Transmission Factor |
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