Sample Originator: Martin B. Smitha.
Data Collection: Simon J. Colesb and Michael B. Hursthouseb
Structure Determination: Simon J. Colesb.
Loughborough Universitya
University of Southamptonb
C33H29I2NO3P2Pt
InChI=1/C27H25NO3P2.C8H14.4CH4.2HI.Pt.H2/c29-26-17-16-21(27(30)31)18-25(26)28(19-32-22-10-4-1-5-11-22)20-33(23-12-6-2-7-13-23)24-14-8-3-9-15-24;1-3-7-5-8(4-2)6-7;;;;;;;;/h1-18,29,32H,19-20H2,(H,30,31);3,7-8H,1,4-6H2,2H3;4*1H4;2*1H;;1H/q;;;;;;;;+1;/p-1/t;7-,8+;;;;;;;;
| Controlled Keywords: | polyphosphines |
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| Date Created: | 13 December 2002 |
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| Deposited On: | 16 Feb 2010 14:45 |
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| Deposited By: | Mr Steve Lamond |
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Data collection parameters
| Chemical formula | C33 H29 I2 N O3 P2 Pt |
| Crystal morphology | |
| Crystal system | monoclinic |
| Space group symbol | P2(1)/c |
| Cell length a | 16.4439(4) |
| Cell length b | 17.3353(3) |
| Cell length c | 15.1356(2) |
| Cell angle alpha | 90.00 |
| Cell angle beta | 109.9110(10) |
| Cell angle gamma | 90.00 |
| Data collection temperature | 120(2) |
Refinement results
| Solution figure of merit | |
| R Factor (Obs) | 0.0522 |
| R Factor (All) | 0.0713 |
| Weighted R Factor (Obs) | 0.1377 |
| Weighted R Factor (All) | 0.1521 |
Citation: Smith, Martin B. and Coles, Simon J. and Hursthouse, Michael B. (2002) University of Southampton, Crystal Structure Report Archive. (http://ecrystals.chem.soton.ac.uk/1146/)
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