| Symmetry used in scalepack | c2 |
|---|---|
| a (Angstrom) | 19.0985 +/- 0.0006 |
| b (Angstrom) | 8.5350 +/- 0.0003 |
| c (Angstrom) | 16.7990 +/- 0.0007 |
| alpha (°) | 90.000 |
| beta (°) | 115.6478 +/- 0.0014 |
| gamma (°) | 90.000 |
| Volume (A**3) | 2468.53 +/- 0.16 |
| Mosaicity (°) | 0.354 +/- 0.003 |
| Total number of images collected | 98 |
|---|---|
| Total exposure time | 31.7 minutes |
| Data collection exposure time | 30.3 minutes |
| Data collection wall-clock time | 40.5 minutes |
| Wavelength | 0.71073 A |
|---|---|
| Generator setting | 50kV 90mA |
| Crystal to detector distance | 30.00 mm |
| Type | Name | # images | Total Rotation | Per frame Rotation | Exposure per frame | Used in scaling |
|---|---|---|---|---|---|---|
| data collection | s01f | 90 | 180.0° phi | 2.000° | 20 seconds | Yes |
| Phi/Chi | i01f - i08f | 8 | 10 seconds |
| Overload or incomplete profile | 116 |
|---|---|
| Sigma cutoff | 3 |
| Scale factor | 10.00 |
|---|---|
| Number of 'full' reflections | 1017 |
| Number of 'partial' reflections | 9327 |
| Total number of integrated reflections | 7822 |
| Total number of unique reflections | 2946 |
| Data completeness | 97.5% |
| Resolution range | 7.00-0.77 A |
| Theta range | 2.91°-27.48° |
| Average Intensity | 33.8 |
| Average Sigma(I) | 2.6 |
| Overall R-merge (linear) | 0.045 |
| Collection Temperature | 120 K |
| Crystal Size | x x |
| Crystal Colour | |
| Crystal Shape |
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