# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_04src1116 _shelx_title ' 04src1116 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 315.50 _exptl_crystal_F_000 1110.00 _reflns_d_resolution_high 0.7700 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.1978 _cell_length_b 12.7114 _cell_length_c 18.0814 _cell_angle_alpha 88.343 _cell_angle_beta 80.737 _cell_angle_gamma 86.262 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5021.55 4565.88 130.99 o 3 0 0 1219.63 1743.94 51.60 o 4 0 0 246.67 362.91 36.71 o 5 0 0 5410.69 5260.64 161.43 o 6 0 0 419.29 361.83 24.55 o 7 0 0 2572.12 2427.79 89.47 o 8 0 0 391.17 366.17 43.00 o 9 0 0 519.88 546.83 70.59 o 10 0 0 75.37 71.40 45.55 o 11 0 0 5.90 39.00 52.11 o -11 1 0 210.67 126.07 51.35 o -10 1 0 91.81 140.81 46.11 o -9 1 0 3.49 -25.79 47.87 o -8 1 0 181.27 176.28 89.94 o -7 1 0 120.37 147.51 68.05 o -6 1 0 1.53 52.67 20.25 o -5 1 0 37.76 78.81 7.38 o -4 1 0 26.97 33.76 9.60 o -3 1 0 1309.39 1402.75 29.56 o -2 1 0 4080.90 3266.56 63.10 o 2 1 0 15764.75 15466.51 522.90 o 3 1 0 9415.68 8614.19 161.93 o 4 1 0 4608.16 4647.32 86.43 o 5 1 0 581.83 454.37 28.09 o 6 1 0 3.83 22.62 27.75 o 7 1 0 259.94 310.09 42.05 o 8 1 0 673.89 630.26 53.97 o 9 1 0 505.64 576.62 76.11 o 10 1 0 19.19 45.81 52.56 o 11 1 0 0.53 33.55 65.12 o -11 2 0 420.97 272.60 96.18 o -10 2 0 687.44 794.54 63.28 o -9 2 0 803.80 904.04 64.44 o -8 2 0 307.54 348.80 86.44 o -7 2 0 1736.25 1577.41 64.93 o -6 2 0 3013.80 3445.71 65.23 o -5 2 0 387.11 334.62 20.18 o -4 2 0 1617.11 1589.78 30.15 o -3 2 0 2.55 51.49 8.33 o -2 2 0 2688.60 2137.25 48.30 o -1 2 0 8431.14 7969.44 141.98 o 1 2 0 4602.08 4649.12 97.17 o 2 2 0 38550.44 42708.40 1032.69 o 3 2 0 746.99 1788.44 116.55 o 4 2 0 1755.20 2030.69 36.95 o 5 2 0 1874.77 1978.51 45.30 o 6 2 0 4032.31 3978.47 98.56 o 7 2 0 2070.22 1763.84 60.45 o 8 2 0 3.14 61.59 30.54 o 9 2 0 26.80 38.83 37.69 o 10 2 0 40.18 69.43 37.93 o 11 2 0 675.99 807.83 105.68 o -11 3 0 170.49 52.22 121.80 o -10 3 0 318.29 352.79 48.03 o -9 3 0 381.95 439.25 46.38 o -8 3 0 16.89 31.70 51.53 o -7 3 0 1351.09 1311.75 37.21 o -6 3 0 524.98 569.81 22.33 o -5 3 0 5769.25 5954.05 108.00 o -4 3 0 2741.77 2905.12 49.64 o -3 3 0 2.15 47.52 20.08 o -2 3 0 2583.53 2144.89 43.76 o -1 3 0 44.86 135.64 16.12 o 0 3 0 599.62 525.60 15.41 o 1 3 0 2213.72 3075.45 75.99 o 2 3 0 2278.99 2907.50 55.40 o 3 3 0 5335.24 5545.82 119.49 o 4 3 0 13285.95 14373.25 212.15 o 5 3 0 10.73 60.50 12.01 o 6 3 0 180.06 107.13 13.08 o 7 3 0 51.32 44.05 24.38 o 8 3 0 105.80 72.10 30.51 o 9 3 0 1071.53 1016.63 54.93 o 10 3 0 128.61 168.77 52.08 o 11 3 0 103.97 119.59 79.44 o -11 4 0 1.32 88.63 417.94 o -10 4 0 222.40 158.98 68.17 o -9 4 0 203.86 261.14 36.75 o -8 4 0 67.61 71.08 14.01 o -7 4 0 3.18 -6.23 14.30 o -6 4 0 394.05 300.10 18.09 o -5 4 0 3333.68 3387.74 65.60 o -4 4 0 1675.55 1413.35 28.92 o -3 4 0 160.85 91.82 15.38 o -2 4 0 123.68 99.46 12.46 o -1 4 0 6540.49 4277.87 90.68 o 0 4 0 10940.77 10937.64 221.39 o 1 4 0 815.12 1618.37 31.72 o 2 4 0 17.41 80.41 13.48 o 3 4 0 1391.00 1866.59 42.02 o 4 4 0 8335.28 11719.99 222.34 o 5 4 0 9965.74 10361.10 165.94 o 6 4 0 1164.47 769.78 23.16 o 7 4 0 4.39 58.72 17.97 o 8 4 0 950.24 902.40 85.08 o 9 4 0 43.44 150.11 37.61 o 10 4 0 0.14 -11.55 38.36 o 11 4 0 18.98 79.37 62.56 o -10 5 0 220.41 156.53 71.55 o -9 5 0 19.42 -9.92 20.05 o -8 5 0 9.37 32.10 16.93 o -7 5 0 583.91 708.90 31.38 o -6 5 0 71.78 81.55 12.68 o -5 5 0 475.23 522.85 17.93 o -4 5 0 428.28 614.73 26.65 o -3 5 0 1733.32 1872.96 41.36 o -2 5 0 7604.78 7352.89 149.37 o -1 5 0 65.57 19.38 17.46 o 0 5 0 3902.49 3788.10 73.37 o 1 5 0 378.71 383.16 23.27 o 2 5 0 1857.73 1964.79 63.92 o 3 5 0 106.17 255.42 21.69 o 4 5 0 498.72 386.31 16.01 o 5 5 0 39.30 72.20 12.22 o 6 5 0 2917.98 3159.27 58.05 o 7 5 0 182.34 176.32 16.52 o 8 5 0 92.28 109.98 13.65 o 9 5 0 3.32 -18.95 31.29 o 10 5 0 36.22 95.75 112.82 o 11 5 0 2.39 25.32 76.17 o -9 6 0 16.51 -7.17 30.59 o -8 6 0 730.63 678.78 52.83 o -7 6 0 2365.37 2400.92 89.37 o -6 6 0 625.36 649.75 29.73 o -5 6 0 17.96 18.65 16.81 o -4 6 0 173.01 134.50 13.31 o -3 6 0 1028.53 829.13 25.40 o -2 6 0 8371.82 7869.10 136.86 o -1 6 0 863.48 1094.12 70.31 o 0 6 0 730.93 787.59 25.33 o 1 6 0 7572.88 7938.77 141.32 o 2 6 0 8260.24 8852.92 167.20 o 3 6 0 261.70 371.63 22.05 o 4 6 0 214.65 549.57 34.03 o 5 6 0 2734.63 2677.90 59.82 o 6 6 0 1757.86 1640.86 59.02 o 7 6 0 1877.63 2014.24 52.62 o 8 6 0 0.39 25.85 14.99 o 9 6 0 0.39 -24.86 26.08 o 10 6 0 158.30 203.97 76.91 o 11 6 0 487.43 295.37 83.62 o -10 7 0 22.52 -42.14 106.22 o -9 7 0 517.56 701.28 87.89 o -8 7 0 9.71 40.77 69.75 o -7 7 0 712.27 765.33 54.08 o -6 7 0 41.15 46.44 48.82 o -5 7 0 269.23 240.03 26.16 o -4 7 0 1475.29 1289.28 59.81 o -3 7 0 254.40 270.61 18.73 o -2 7 0 547.86 649.16 22.91 o -1 7 0 15.16 37.93 19.14 o 0 7 0 520.86 841.61 33.54 o 1 7 0 506.21 629.43 26.17 o 2 7 0 266.70 456.09 21.91 o 3 7 0 67.50 250.10 26.27 o 4 7 0 23.11 86.10 17.60 o 5 7 0 68.58 136.38 22.65 o 6 7 0 134.59 177.31 23.00 o 7 7 0 381.58 332.00 27.36 o 8 7 0 509.85 459.33 48.05 o 9 7 0 7.85 -0.57 56.87 o 10 7 0 114.43 174.80 84.62 o -9 8 0 313.40 239.99 52.76 o -8 8 0 381.93 391.58 91.34 o -7 8 0 0.75 4.36 43.59 o -6 8 0 62.63 49.63 27.07 o -5 8 0 686.24 679.74 27.11 o -4 8 0 68.03 -5.57 20.02 o -3 8 0 574.66 603.37 26.11 o -2 8 0 33.72 96.90 22.93 o -1 8 0 2812.39 2942.74 61.55 o 0 8 0 2933.74 3194.95 84.07 o 1 8 0 19.16 67.79 20.66 o 2 8 0 1555.39 2052.05 63.15 o 3 8 0 555.86 780.45 43.56 o 4 8 0 505.69 445.06 29.42 o 5 8 0 777.37 904.95 46.73 o 6 8 0 16.67 111.30 31.26 o 7 8 0 796.51 888.90 53.94 o 8 8 0 39.36 59.36 41.25 o 9 8 0 246.38 222.86 44.23 o 10 8 0 23.02 78.50 96.07 o -9 9 0 0.25 -23.61 37.82 o -8 9 0 86.71 147.77 61.98 o -7 9 0 145.58 176.18 37.74 o -6 9 0 0.96 18.99 38.61 o -5 9 0 1.02 -3.82 14.84 o -4 9 0 435.51 492.17 28.59 o -3 9 0 225.30 242.55 22.99 o -2 9 0 134.70 116.89 19.95 o -1 9 0 3081.44 2817.05 62.49 o 0 9 0 1504.08 1301.45 42.66 o 1 9 0 668.38 809.67 40.28 o 2 9 0 3609.71 3914.67 95.26 o 3 9 0 320.45 339.46 22.67 o 4 9 0 522.81 735.83 47.76 o 5 9 0 27.21 66.74 40.89 o 6 9 0 149.75 158.37 40.92 o 7 9 0 324.42 385.50 47.70 o 8 9 0 10.02 17.70 34.63 o 9 9 0 83.54 5.29 46.20 o 10 9 0 173.96 262.35 88.68 o -8 10 0 78.60 169.45 55.33 o -7 10 0 1.72 -11.72 36.51 o -6 10 0 347.54 356.37 50.78 o -5 10 0 9.80 39.40 27.16 o -4 10 0 276.83 275.84 30.80 o -3 10 0 3871.40 3756.03 100.28 o -2 10 0 283.75 374.75 47.99 o -1 10 0 3508.47 3504.16 88.73 o 0 10 0 1447.76 1770.21 54.51 o 1 10 0 414.37 585.60 40.59 o 2 10 0 106.49 220.25 37.92 o 3 10 0 64.48 159.55 28.80 o 4 10 0 99.03 193.58 39.05 o 5 10 0 373.38 294.38 43.38 o 6 10 0 1176.94 1342.20 140.69 o 7 10 0 3.20 2.87 41.85 o 8 10 0 0.36 9.76 46.34 o 9 10 0 43.15 106.20 51.43 o -8 11 0 6.23 4.20 134.47 o -7 11 0 80.31 99.59 42.17 o -6 11 0 0.30 -23.11 38.22 o -5 11 0 504.39 402.84 46.13 o -4 11 0 175.88 135.51 29.04 o -3 11 0 20.07 -23.52 19.40 o -2 11 0 612.11 748.17 41.41 o -1 11 0 267.45 238.33 49.16 o 0 11 0 2.28 -14.46 29.94 o 1 11 0 104.60 1050.06 572.77 o 2 11 0 70.79 87.58 24.19 o 3 11 0 65.83 117.24 34.96 o 4 11 0 98.85 294.94 109.05 o 5 11 0 331.30 511.40 48.11 o 6 11 0 169.16 112.93 34.87 o 7 11 0 5.07 13.27 35.47 o 8 11 0 30.95 84.80 73.20 o 9 11 0 72.18 33.79 55.79 o -7 12 0 0.82 25.45 55.56 o -6 12 0 61.39 83.73 34.12 o -5 12 0 85.41 62.93 42.28 o -4 12 0 1015.53 819.30 57.17 o -3 12 0 6.42 38.54 50.28 o -2 12 0 21.83 62.10 29.07 o -1 12 0 771.22 911.26 69.80 o 0 12 0 43.86 7.82 37.72 o 1 12 0 352.88 409.15 48.16 o 2 12 0 468.04 463.84 61.99 o 3 12 0 157.16 176.35 34.12 o 4 12 0 1200.89 1245.68 109.49 o 5 12 0 52.39 75.76 39.98 o 6 12 0 64.57 47.07 35.94 o 7 12 0 3.11 16.06 49.29 o 8 12 0 154.85 66.16 85.05 o -6 13 0 131.30 100.27 75.75 o -5 13 0 54.75 15.23 43.08 o -4 13 0 22.53 21.00 38.37 o -3 13 0 1.73 3.69 35.86 o -2 13 0 0.53 13.09 32.66 o -1 13 0 331.95 241.97 47.08 o 0 13 0 372.78 439.26 51.78 o 1 13 0 912.54 1029.37 58.89 o 2 13 0 40.09 -22.50 31.14 o 3 13 0 315.11 264.85 52.93 o 4 13 0 452.44 421.94 57.43 o 5 13 0 36.92 24.79 50.06 o 6 13 0 45.06 53.76 40.35 o 7 13 0 0.96 27.62 83.91 o -5 14 0 0.05 -28.13 73.89 o -4 14 0 9.61 -20.91 39.26 o -3 14 0 88.82 98.32 37.92 o -2 14 0 232.53 308.93 62.25 o -1 14 0 88.12 36.55 39.37 o 0 14 0 3.11 46.23 44.76 o 1 14 0 486.10 377.53 45.26 o 2 14 0 176.96 122.07 46.98 o 3 14 0 62.87 105.84 98.81 o 5 14 0 4.11 -34.52 45.50 o 6 14 0 1.37 102.39 89.78 o -4 15 0 20.40 -66.91 64.71 o -3 15 0 49.78 87.92 52.56 o -2 15 0 32.61 90.21 39.18 o -1 15 0 63.61 97.47 59.65 o 0 15 0 195.67 158.12 47.14 o 1 15 0 18.95 3.51 46.27 o 2 15 0 49.28 85.79 52.13 o 4 15 0 212.62 301.27 62.26 o 5 15 0 20.81 59.40 54.37 o -2 16 0 19.13 53.73 50.07 o 0 16 0 56.41 15.05 65.19 o 1 16 0 9.36 14.80 57.07 o 2 16 0 81.70 16.88 36.72 o 3 16 0 87.39 16.22 117.78 o -3 -16 1 132.06 155.48 94.66 o -2 -16 1 0.43 18.66 47.68 o -1 -16 1 0.85 -3.29 52.42 o 0 -16 1 1.94 42.69 53.67 o 1 -16 1 103.94 129.47 62.02 o 2 -16 1 18.36 -17.64 57.26 o -5 -15 1 86.69 35.33 55.92 o -4 -15 1 0.78 -36.58 60.84 o -3 -15 1 372.32 353.45 74.82 o -2 -15 1 141.23 132.76 43.35 o -1 -15 1 65.68 30.89 42.84 o 0 -15 1 52.50 -7.16 29.24 o 1 -15 1 143.82 39.32 53.40 o 2 -15 1 120.46 224.93 45.64 o 3 -15 1 11.34 96.53 127.11 o 4 -15 1 9.34 66.65 73.65 o -6 -14 1 160.10 122.36 71.90 o -5 -14 1 51.43 13.59 40.50 o -4 -14 1 13.28 26.81 40.49 o -3 -14 1 252.24 322.98 70.39 o -2 -14 1 0.73 -63.63 45.29 o -1 -14 1 238.62 390.80 44.72 o 0 -14 1 224.71 294.32 50.26 o 1 -14 1 15.13 113.71 46.20 o 2 -14 1 4.42 -35.09 38.53 o 3 -14 1 0.79 55.42 38.80 o 4 -14 1 3.69 -31.86 38.43 o 5 -14 1 10.67 29.87 40.72 o -7 -13 1 23.64 -74.15 49.43 o -6 -13 1 106.87 45.39 110.02 o -5 -13 1 805.76 683.94 57.95 o -4 -13 1 264.39 294.62 44.12 o -3 -13 1 122.47 124.55 79.37 o -2 -13 1 8.47 11.25 28.22 o -1 -13 1 492.95 403.80 42.59 o 0 -13 1 469.08 355.46 44.77 o 1 -13 1 0.94 14.14 28.18 o 2 -13 1 689.78 653.25 49.66 o 3 -13 1 100.48 126.87 62.24 o 4 -13 1 214.17 119.95 42.21 o 5 -13 1 62.26 25.96 33.00 o 6 -13 1 1.01 57.91 87.43 o -8 -12 1 35.44 5.98 61.99 o -7 -12 1 172.82 123.54 48.18 o -6 -12 1 90.78 78.79 37.14 o -5 -12 1 360.30 419.82 45.09 o -4 -12 1 53.26 53.89 110.99 o -3 -12 1 377.37 413.11 47.26 o -2 -12 1 150.41 201.86 33.52 o -1 -12 1 7.49 68.99 30.94 o 0 -12 1 186.59 292.93 67.37 o 1 -12 1 135.67 190.88 72.42 o 2 -12 1 354.76 311.59 33.56 o 3 -12 1 444.60 399.87 54.36 o 4 -12 1 65.36 50.78 34.16 o 5 -12 1 11.59 38.51 55.55 o 6 -12 1 7.45 78.93 41.10 o 7 -12 1 3.05 24.34 49.92 o -9 -11 1 9.62 39.43 107.91 o -8 -11 1 44.04 33.15 78.00 o -7 -11 1 0.93 36.25 39.56 o -6 -11 1 20.60 57.59 99.05 o -5 -11 1 11.62 50.30 32.51 o -4 -11 1 1822.03 2080.57 105.38 o -3 -11 1 700.90 653.89 53.64 o -2 -11 1 799.50 656.08 39.92 o -1 -11 1 148.82 235.68 216.58 o 0 -11 1 2.04 13.35 24.25 o 1 -11 1 1868.62 1953.28 128.46 o 2 -11 1 919.26 921.74 71.65 o 3 -11 1 42.17 -3.14 20.31 o 4 -11 1 106.57 97.95 22.12 o 5 -11 1 36.06 16.43 24.68 o 6 -11 1 341.28 288.88 33.67 o 7 -11 1 7.38 43.68 43.31 o 8 -11 1 24.67 67.47 57.78 o -9 -10 1 2.00 21.44 64.71 o -8 -10 1 81.79 118.18 48.25 o -7 -10 1 3.92 54.60 40.23 o -6 -10 1 500.41 514.86 49.46 o -5 -10 1 490.59 578.25 37.11 o -4 -10 1 103.39 47.74 33.16 o -3 -10 1 674.34 742.21 37.85 o -2 -10 1 99.53 75.26 20.79 o -1 -10 1 2465.57 2313.11 72.09 o 0 -10 1 67.31 73.82 32.79 o 1 -10 1 190.76 303.88 39.00 o 2 -10 1 926.80 976.80 47.26 o 3 -10 1 7.31 -32.64 21.76 o 4 -10 1 848.79 758.52 42.12 o 5 -10 1 280.46 159.50 30.66 o 6 -10 1 20.65 48.49 41.94 o 7 -10 1 22.17 23.10 36.94 o 8 -10 1 37.31 40.15 50.54 o -10 -9 1 93.38 85.74 97.01 o -9 -9 1 687.73 494.46 57.82 o -8 -9 1 89.42 84.72 58.36 o -7 -9 1 9.00 -5.60 34.39 o -6 -9 1 92.34 190.03 26.34 o -5 -9 1 1014.77 1092.90 51.72 o -4 -9 1 354.35 524.50 45.51 o -3 -9 1 361.16 321.50 23.60 o -2 -9 1 527.81 635.60 36.47 o -1 -9 1 2384.20 2583.18 64.21 o 0 -9 1 2.06 12.65 22.56 o 1 -9 1 1596.50 1497.82 71.75 o 2 -9 1 2634.73 2428.52 56.79 o 3 -9 1 3292.20 3258.60 83.35 o 4 -9 1 8.94 13.05 17.49 o 5 -9 1 231.57 247.64 30.20 o 6 -9 1 60.05 71.76 36.36 o 7 -9 1 1313.35 1479.58 87.19 o 8 -9 1 939.36 901.77 91.86 o 9 -9 1 12.95 -37.47 47.62 o -10 -8 1 137.68 90.81 140.54 o -9 -8 1 211.12 174.33 39.62 o -8 -8 1 324.98 319.87 46.83 o -7 -8 1 1058.78 1116.98 62.94 o -6 -8 1 74.99 73.54 24.87 o -5 -8 1 1602.15 1978.87 66.66 o -4 -8 1 114.86 131.56 24.25 o -3 -8 1 2135.81 2212.47 62.76 o -2 -8 1 5.66 36.76 21.85 o -1 -8 1 1083.83 953.40 40.28 o 0 -8 1 120.15 124.79 26.03 o 1 -8 1 18.45 52.75 20.20 o 2 -8 1 2443.50 2619.14 56.22 o 3 -8 1 16.32 6.51 13.90 o 4 -8 1 224.27 136.69 19.75 o 5 -8 1 1013.19 1052.06 49.85 o 6 -8 1 804.22 828.71 54.20 o 7 -8 1 746.37 678.17 56.59 o 8 -8 1 26.11 63.15 43.90 o 9 -8 1 80.16 221.20 82.52 o 10 -8 1 1.16 225.51 116.73 o -10 -7 1 104.91 147.98 79.40 o -9 -7 1 159.00 170.12 39.22 o -8 -7 1 1765.89 1572.47 58.39 o -7 -7 1 1521.49 1598.83 40.07 o -6 -7 1 78.50 55.60 20.07 o -5 -7 1 224.52 411.67 24.83 o -4 -7 1 73.62 138.73 19.73 o -3 -7 1 3656.49 4043.01 75.38 o -2 -7 1 25.82 26.46 15.47 o -1 -7 1 615.83 442.33 20.22 o 0 -7 1 3342.44 3079.02 58.12 o 1 -7 1 1851.01 1844.95 44.68 o 2 -7 1 3610.03 3598.79 60.38 o 3 -7 1 1121.84 1171.99 35.87 o 4 -7 1 637.70 638.39 21.64 o 5 -7 1 28.17 94.48 36.72 o 6 -7 1 70.67 112.46 27.69 o 7 -7 1 214.46 171.97 38.11 o 8 -7 1 125.55 174.91 40.63 o 9 -7 1 1517.80 1759.23 158.28 o 10 -7 1 19.43 27.20 76.81 o -11 -6 1 22.35 341.89 160.85 o -10 -6 1 34.79 475.31 188.40 o -9 -6 1 724.30 656.45 60.70 o -8 -6 1 284.86 284.76 22.07 o -7 -6 1 2366.90 2161.25 57.19 o -6 -6 1 265.98 255.76 13.52 o -5 -6 1 1.12 28.64 11.41 o -4 -6 1 339.39 367.37 21.04 o -3 -6 1 607.60 891.32 27.01 o -2 -6 1 2454.24 2494.12 48.47 o -1 -6 1 1063.82 1074.01 46.90 o 0 -6 1 994.69 1089.32 25.57 o 1 -6 1 3050.49 3144.20 72.11 o 2 -6 1 1764.41 1985.64 39.96 o 3 -6 1 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