2(C~24~H~28~Mn~2~N~11~O~5~), C~2~H~8~N~2~O~5#, 2(CH~3~NO~2~), 6(ClO~4~)

Sample Originator: Craig J. Matthewsa.

Data Collection: Peter N. Hortonb and Michael B. Hursthouseb

Structure Determination: Peter N. Hortonb.

Nottingham Trent Universitya
University of Southamptonb



Identification Number:10.5258/ecrystals/1067
Controlled Keywords:structures of transition-metal organic compounds
Date Created:01 December 2004
Deposited On:28 Mar 2012 12:54
Deposited By:Mr Steve Lamond

Depositor Comments

All hydrogen atoms were fixed. There was some disordered solvent, including a half occupied water molecule.

Data collection parameters

Chemical formulaC26 H35 Cl3 Mn2 N13 O21.50
Crystal morphologySlab
Crystal systemtriclinic
Space group symbolP-1
Cell length a9.1978(8)
Cell length b12.711(4)
Cell length c18.081(5)
Cell angle alpha88.34(2)
Cell angle beta80.737(12)
Cell angle gamma86.262(14)
Data collection temperature120(2)

Refinement results

Solution figure of merit0.1002
R Factor (Obs)0.0943
R Factor (All)0.1575
Weighted R Factor (Obs)0.2176
Weighted R Factor (All)0.2472

Citation: Matthews, Craig J. and Horton, Peter N. and Hursthouse, Michael B. (2004) University of Southampton, Crystal Structure Report Archive. (doi:10.5258/ecrystals/1067)
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