C~34~H~32~MnN~14~O~2~, 2(C~2~H~3~N), 2(ClO~4~)

Sample Originator: Craig J. Matthewsa.

Data Collection: Peter N. Hortonb and Michael B. Hursthouseb

Structure Determination: Peter N. Hortonb.

Nottingham Trent Universitya
University of Southamptonb



Identification Number:10.5258/ecrystals/1065
Controlled Keywords:structures of transition-metal organic compounds
Date Created:02 December 2004
Deposited On:28 Mar 2012 12:54
Deposited By:Mr Steve Lamond

Depositor Comments

All hydrogen atoms were fixed. There was disorder of a perchlorate anion and the solvent acetonitrile.

Data collection parameters

Chemical formulaC38 H38 Cl2 Mn N16 O10
Crystal morphologyPlate
Crystal systemtriclinic
Space group symbolP-1
Cell length a11.0194(6)
Cell length b13.230(2)
Cell length c16.983(4)
Cell angle alpha110.038(11)
Cell angle beta93.940(10)
Cell angle gamma109.791(12)
Data collection temperature120(2)

Refinement results

Solution figure of merit0.1782
R Factor (Obs)0.0661
R Factor (All)0.0906
Weighted R Factor (Obs)0.1723
Weighted R Factor (All)0.1886

Citation: Matthews, Craig J. and Horton, Peter N. and Hursthouse, Michael B. (2004) University of Southampton, Crystal Structure Report Archive. (doi:10.5258/ecrystals/1065)
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