Sample Originator: Martin B. Smitha.

Data Collection: Mark E. Lightb and Michael B. Hursthouseb

Structure Determination: Mark E. Lightb.

Loughborough Universitya
University of Southamptonb



Identification Number:10.5258/ecrystals/1014
Controlled Keywords:phosphorus compounds, metal ligands, palladium compounds
Date Created:16 January 2001
Deposited On:17 Dec 2009 15:35
Deposited By:Mr Steve Lamond

Depositor Comments

All hydrogen atoms were placed in idealised positions and refiend using a riding model.

Data collection parameters

Chemical formulaC20 H17 Cl2 N2 P Pd S
Crystal morphology
Crystal systemMonoclinic
Space group symbolP2(1)/c
Cell length a21.0715(3)
Cell length b8.19620(10)
Cell length c35.2981(7)
Cell angle alpha90.00
Cell angle beta95.2190(10)
Cell angle gamma90.00
Data collection temperature150(2)

Refinement results

Solution figure of merit
R Factor (Obs)0.0452
R Factor (All)0.0835
Weighted R Factor (Obs)0.0883
Weighted R Factor (All)0.0988

Citation: Smith, Martin B. and Light, Mark E. and Hursthouse, Michael B. (2001) University of Southampton, Crystal Structure Report Archive. (doi:10.5258/ecrystals/1014)
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